-
公开(公告)号:US4619777A
公开(公告)日:1986-10-28
申请号:US491718
申请日:1983-05-05
申请人: Milena Melzer , Helmut Jakusch , Werner Grau , Eberhard Koster , Werner Loser , Reinhard Polke , Gunter Schadel , Manfred Ohlinger , Gunter Vath
发明人: Milena Melzer , Helmut Jakusch , Werner Grau , Eberhard Koster , Werner Loser , Reinhard Polke , Gunter Schadel , Manfred Ohlinger , Gunter Vath
IPC分类号: G11B5/70 , C09D5/23 , G11B5/68 , G11B5/706 , G11B5/84 , H01F1/11 , H01F1/113 , H01F1/44 , H01F1/26 , C04B35/04
CPC分类号: G11B5/84 , G11B5/70663 , Y10S428/906 , Y10T428/25 , Y10T428/256 , Y10T428/257
摘要: A magnetic dispersion which can be applied to a non-magnetic base to produce a recording medium is prepared by dispersing a magnetically anisotropic material in a polymer binder and in an organic solvent by a method wherein the magnetically anisotropic material is worked in a jet mill before and/or during dispersing.
摘要翻译: 通过将磁各向异性材料分散在聚合物粘合剂和有机溶剂中,可以通过将磁各向异性材料在喷射磨中加工的方法制备可用于非磁性基底以产生记录介质的磁性分散体 和/或在分散期间。
-
公开(公告)号:US4497723A
公开(公告)日:1985-02-05
申请号:US508168
申请日:1983-06-27
申请人: Manfred Ohlinger , Guenter Vaeth , Peter Rudolf , Wilhelm Sarnecki , Helmut Jakusch , Eberhard Koester , Milena Melzer
发明人: Manfred Ohlinger , Guenter Vaeth , Peter Rudolf , Wilhelm Sarnecki , Helmut Jakusch , Eberhard Koester , Milena Melzer
CPC分类号: B82Y30/00 , C01G49/06 , G11B5/70694 , C01P2002/60 , C01P2004/10 , C01P2004/64 , C01P2006/12 , C01P2006/42
摘要: A process for the preparation of acicular ferrimagnetic iron oxides by reducing gamma-iron(III) oxide hydroxide to magnetite, at from 280.degree. to 620.degree. C., by means of an organic compound which is decomposable at this temperature in the presence of iron oxide, and, optionally, a stream of reducing gas, and, if desired, then oxidizing the magnetite with oxygen-containing gases, at from 150.degree. to 450.degree. C., to acicular ferrimagnetic iron oxide of the formula FeO.sub.x, where x is from above 1.33 to 1.50, wherein the organic compound used for the reduction is a non-polar glycerol ester of a fatty acid which is introduced into the aqueous reaction suspension during the preparation of the gamma-iron(III) oxide hydroxide.
摘要翻译: 一种制备针状亚铁磁性氧化铁的方法,该方法是通过在这种温度下在铁存在下可分解的有机化合物将280℃至620℃的氧化氢氧化物还原成磁铁矿 氧化物和任选的还原气体流,并且如果需要,然后用含氧气体在150℃至450℃下将磁铁矿氧化成式FeO x的针状亚铁磁性氧化铁,其中x为 从1.33到1.50,其中用于还原的有机化合物是在制备γ-铁(III)氧化物氢氧化物期间引入到水性反应悬浮液中的非极性甘油酯脂肪酸酯。
-
3.
公开(公告)号:US4169912A
公开(公告)日:1979-10-02
申请号:US848437
申请日:1977-11-03
申请人: Eduard Schonafinger , Paul Deigner , Manfred Ohlinger , Helmut Jakusch , Jurgen Amort , Heinz Nestler , Claus-Dietrich Seiler , Otto Ambros
发明人: Eduard Schonafinger , Paul Deigner , Manfred Ohlinger , Helmut Jakusch , Jurgen Amort , Heinz Nestler , Claus-Dietrich Seiler , Otto Ambros
CPC分类号: C09C3/12 , C09C1/24 , G11B5/71 , C01P2004/10 , C01P2004/80 , C01P2006/22 , C01P2006/42 , C01P2006/90 , Y10S428/90 , Y10T428/24388 , Y10T428/24413 , Y10T428/24421 , Y10T428/266 , Y10T428/31663
摘要: An iron oxide pigment having a coating of a silane of the formulaR.sub.n Si(OR').sub.4-nwhereinR is an, in some cases, branched or oxygen-bridge-containing alkyl or alkenyl moiety of 1 to 18 carbon atoms, or an aryl moiety,R' is an, in some cases, branched and, in some cases, oxygen-bridge-containing alkyl moiety of 1 to 8,N=1 to 3,Or a hydrolysis product thereof; a magnetic tape containing such coated iron oxide pigment and a process for coating such iron oxide pigment. There is particularly disclosed the treatment of iron oxide magnetic pigments to thereby improve their wear resistance and dispersibility in organic mediums.
-
公开(公告)号:US06231963B1
公开(公告)日:2001-05-15
申请号:US08913808
申请日:1998-03-17
申请人: August Lehner , Helmut Jakusch , Volker Koch , Manfred Ohlinger , Albert Kohl , Werner Lenz , Norbert Schneider , Peter Heilmann , Werner Hübner , Erich Hoffmann , Ronald John Veitch , Rudi Lehnert , Harald Jachow
发明人: August Lehner , Helmut Jakusch , Volker Koch , Manfred Ohlinger , Albert Kohl , Werner Lenz , Norbert Schneider , Peter Heilmann , Werner Hübner , Erich Hoffmann , Ronald John Veitch , Rudi Lehnert , Harald Jachow
IPC分类号: G11B5733
CPC分类号: G11B5/708 , G11B5/733 , G11B5/738 , Y10S428/90 , Y10T428/256 , Y10T428/257
摘要: Described are tape-type magnetic recording media (I) including a non-magnetic substrate (III), at least one film applied to the substrate and, in at least one of these films, an inorganic acicular pigment (II) suitable for use as a supporting pigment, the ratio of the mean length to the mean diameter of the pigment (II) being at least 3 and the mean modulus of elasticity of the films being not less than 15 GPa in the longitudinal direction of the tape-type recording medium (I).
摘要翻译: 描述了包括非磁性基板(III)的带式磁记录介质(I),至少一个施加到基板的膜,并且在这些膜中的至少一个膜中,适合用作 支撑颜料,颜料(II)的平均长度与平均直径的比率至少为3,膜的平均弹性模量在带式记录介质的纵向方向上不小于15GPa (一世)。
-
5.
公开(公告)号:US4271234A
公开(公告)日:1981-06-02
申请号:US8146
申请日:1979-01-31
申请人: Eduard Schonafinger , Paul Deigner , Manfred Ohlinger , Helmut Jakusch , Jurgen Amort , Heinz Nestler , Claus-Dietrich Seiler , Otto Ambros
发明人: Eduard Schonafinger , Paul Deigner , Manfred Ohlinger , Helmut Jakusch , Jurgen Amort , Heinz Nestler , Claus-Dietrich Seiler , Otto Ambros
IPC分类号: C09C1/22 , C01G49/02 , C01G49/06 , C09C1/00 , C09C1/24 , C09C3/12 , G11B5/71 , B32B5/16 , B32B9/04
CPC分类号: C09C1/24 , C09C3/12 , G11B5/71 , C01P2004/10 , C01P2004/80 , C01P2006/22 , C01P2006/42 , C01P2006/90 , Y10S428/90 , Y10T428/24388 , Y10T428/24413 , Y10T428/257 , Y10T428/2995 , Y10T428/31663 , Y10T428/31667
摘要: An iron oxide pigment having a coating of a silane of the formulaR.sub.n Si(OR').sub.4-nwhereinR is an, in some cases, branched or oxygen-bridge-containing alkyl or alkenyl moiety of 1 to 18 carbon atoms, or an aryl moiety,R' is an, in some cases, branched and, in some cases, oxygen-bridge-containing alkyl moiety of 1 to 8,n=1 to 3,or a hydrolysis product thereof; a magnetic tape containing such coated iron oxide pigment and a process for coating such iron oxide pigment. There is particularly disclosed the treatment of iron oxide magnetic pigments to thereby improve their wear resistance and dispersibility in organic mediums.
摘要翻译: 具有式RnSi(OR')4-n的硅烷的涂层的氧化铁颜料,其中R是在一些情况下是含有1至18个碳原子的支链或含氧桥的烷基或烯基部分,或 芳基部分,R'在某些情况下是支链的,在一些情况下,含1-8个碳原子的含氧桥烷基部分,n = 1-3,或其水解产物。 含有这种涂覆的氧化铁颜料的磁带和用于涂覆这种氧化铁颜料的方法。 特别公开了氧化铁磁性颜料的处理,从而提高其在有机介质中的耐磨性和分散性。
-
公开(公告)号:US4213959A
公开(公告)日:1980-07-22
申请号:US930513
申请日:1978-08-03
申请人: Rudolf Brodt , Helmut Jakusch , Eberhard Koester , Werner Loeser , Manfred Ohlinger , Wilhelm Sarnecki , Werner Steck
发明人: Rudolf Brodt , Helmut Jakusch , Eberhard Koester , Werner Loeser , Manfred Ohlinger , Wilhelm Sarnecki , Werner Steck
CPC分类号: G11B5/70663 , C01G49/06 , G11B5/62 , G11B5/70647 , G11B5/70652 , C01P2004/10 , C01P2004/54 , C01P2004/61 , C01P2004/62 , C01P2006/42
摘要: A process for the manufacture of acicular ferrimagnetic iron oxide by dehydrating acicular iron(III) oxide hydroxides to give acicular iron(III) oxides, then reducing these iron(III) oxides at from 300.degree. to 650.degree. C. by means of an organic compound which decomposes in this temperature range, and oxidizing the reduced product with an oxygen-containing gas at from 200.degree. to 500.degree. C., wherein the acicular iron(III) oxide hydroxides employed consist of a mixture of goethite and lepidocrocite, containing at least 60% of the latter, and the dehydration is carried out at from 250.degree. to 700.degree. C.
摘要翻译: 通过将针状铁(III)氧化物氢氧化物脱水制成针状亚铁磁性氧化铁,得到针状氧化铁(III),然后通过有机物在300℃至650℃还原这些氧化铁(III) 化合物,其在该温度范围内分解,并在200℃至500℃下用含氧气体氧化还原产物,其中所用的针状(III)氧化物氢氧化物由针铁矿和氯铁矿混合物组成, 最少为60%,脱水为250〜700℃。
-
公开(公告)号:US4178171A
公开(公告)日:1979-12-11
申请号:US888508
申请日:1978-03-20
申请人: Werner Steck , Rudolf Brodt , Wilhelm Sarnecki , Helmut Jakusch , Manfred Ohlinger , Eberhard Koester
发明人: Werner Steck , Rudolf Brodt , Wilhelm Sarnecki , Helmut Jakusch , Manfred Ohlinger , Eberhard Koester
IPC分类号: G11B5/706 , B22F9/22 , C09D5/23 , C09D7/12 , C21B15/00 , G11B5/712 , G11B5/714 , H01F1/06 , B22F9/00
摘要: A process for the manufacture of acicular ferromagnetic iron particles by reducing acicular iron(III) oxide hydroxides which consist of pure synthetic lepidocrocite or a mixture of synthetic goethite and at least 70% by weight of synthetic lepidocrocite.The iron(III) oxide hydroxides used carry, on their surface, an alkaline earth metal cation and an anion of a monobasic, dibasic or tribasic aliphatic carboxylic acid of up to 6 carbon atoms or an organic compound containing at least two groups capable of chelating the alkaline earth metal cation, and are produced in such a way that they consist of at least 70 percent by weight of lepidocrocite and have a length-to-width ratio of not less than 15:1.Reduction of such iron(III) oxide hydroxides gives iron particles with pronounced shape anisotropy, which exhibit both good magnetic properties and a narrow field strength distribution.
摘要翻译: 通过还原针状铁(III)氢氧化物来制造针状铁磁性铁粒子的方法,该针状铁氧化物由纯合成锂铁矿石或合成针铁矿和至少70%重量的合成锂铁矿石混合物组成。 所用的氧化铁(III)氢氧化物在其表面上带有至多6个碳原子的一元,二元或三元脂肪族羧酸的碱土金属阳离子和阴离子,或含至少两个能够螯合的基团的有机化合物 碱土金属阳离子,并且以这样的方式制备,使得它们由至少70重量%的氯铁矿石组成,并且具有不小于15:1的长宽比。 这种氧化还原铁(III)氢氧化物的还原产生具有显着形状各向异性的铁颗粒,其具有良好的磁性能和窄的场强分布。
-
公开(公告)号:US5569409A
公开(公告)日:1996-10-29
申请号:US341962
申请日:1994-11-16
申请人: Harald Jachow , Reinhard K orner , Ronald J. Veitch , Ekkehard Schwab , Helmut Jakusch , Bernd H oppner , Rudi Lehnert , Manfred Ohlinger
发明人: Harald Jachow , Reinhard K orner , Ronald J. Veitch , Ekkehard Schwab , Helmut Jakusch , Bernd H oppner , Rudi Lehnert , Manfred Ohlinger
IPC分类号: C01G37/027 , C09D5/23 , C09D7/12 , G11B5/706 , H01F1/11
CPC分类号: C01G37/027 , G11B5/70636 , C01P2004/10 , C01P2004/62 , C01P2006/12 , C01P2006/42 , Y10S428/90 , Y10T428/256 , Y10T428/26
摘要: A finely divided acicular CrO.sub.2 modified with iron, tellurium and/or antimony and having a high coercive force possesses improved heat stability of the residual induction and a relatively narrow distribution of the particle size and of the coercive force. This CrO.sub.2 pigment is obtained by a method in which the iron compound used for the modification is iron oxalate, which is employed in an amount of 1-10% by weight, based on the theoretical CrO.sub.2 yield.
摘要翻译: 用铁,碲和/或锑改性并具有高矫顽力的精细分开的针状CrO 2具有改善的热稳定性,并且具有相对较窄的粒度分布和矫顽力的分布。 该CrO 2颜料通过以下方法获得:其中用于改性的铁化合物是草酸铁,其用量为1-10重量%,基于理论上的CrO 2收率。
-
公开(公告)号:US5378383A
公开(公告)日:1995-01-03
申请号:US109425
申请日:1993-08-20
申请人: Harald Jachow , Ekkehard Schwab , Reinhard Koerner , Norbert Mueller , Rudi Lehnert , Manfred Ohlinger , Helmut Auweter , Helmut Jakusch , Ronald J. Veitch , Michael Bobrich
发明人: Harald Jachow , Ekkehard Schwab , Reinhard Koerner , Norbert Mueller , Rudi Lehnert , Manfred Ohlinger , Helmut Auweter , Helmut Jakusch , Ronald J. Veitch , Michael Bobrich
IPC分类号: C01G37/027 , C09D5/23 , G11B5/706 , G11B5/73
CPC分类号: G11B5/70636
摘要: A magnetic recording medium comprising a nonmagnetic substrate and at least one magnetic layer applied thereon and containing an acicular chromium dioxide uniformly distributed in a polymeric binder and additives and having a coercive force of at least 60 kA/m, a mean particle length of the chromium dioxide of less than 300 nm, whose factor HD according to the formula ##EQU1## where KT is the coercive force of the magnetic layer in [kA/m], measured in an external field of 380 kA/m, L is the mean particle length and .DELTA.L is the range of the particle size distribution, determined from the numerical distribution of the particle length, both measured in [nm], is greater than 1.85, and a process for the preparation of this chromium dioxide.
摘要翻译: 一种磁记录介质,包括非磁性基底和至少一个施加在其上的磁性层,并含有均匀分布在聚合物粘合剂中的针状二氧化铬和添加剂,并具有至少60kA / m的矫顽力,铬的平均粒子长度 在380 kA / m的外场测量的小于300nm的二氧化物,其中KT是以[kA / m]表示的磁性层的矫顽力的公式
的因子HD是平均粒子 长度和DELTA L是根据粒度长度的数值分布确定的,粒度分布的范围,均以[nm]测量,大于1.85,以及制备该二氧化铬的方法。 -
公开(公告)号:US4059716A
公开(公告)日:1977-11-22
申请号:US586346
申请日:1975-06-12
CPC分类号: G11B5/70663 , C01G49/06 , G11B5/70657 , C01P2004/03 , C01P2004/10 , C01P2006/10 , C01P2006/42 , Y10T428/2991
摘要: A process for the manufacture of acicular gamma-iron(III) oxide which, because of its improved dispersibility in organic binders, is suitable for the manufacture of magnetic recording media exhibiting a particularly high orientation ratio. For this purpose, the non-magnetic acicular .alpha.-iron(III) oxide or goethite pigment is treated with from 0.5 to 10% by weight, based on the pigment, of a compound of the formula I: ##STR1## where R.sup.1, R.sup.2 and R.sup.3 are hydrogen, alkyl of 1 to 24 carbon atoms or alkenyl of 1 to 24 carbon atoms and (RX).sup.- is selected from the group consisting of an aliphatic carboxylic acid of 1 to 18 carbon atoms, an aromatic carboxylic acid of 1 to 18 carbon atoms, a sulfonic acid and an ester of phosphoric acid and is then further processed by conventional methods to give gamma-iron(III) oxide.
摘要翻译: 用于制造针状γ-氧化铁(III)的方法,其由于其在有机粘合剂中的分散性的改善而适用于制造表现出特别高取向比的磁记录介质。 为此,非磁性针状α-铁(III)氧化物或针铁矿颜料以基于颜料的0.5至10重量%的式I化合物处理:其中 R 1,R 2和R 3是氢,1至24个碳原子的烷基或1至24个碳原子的链烯基和(RX) - 选自1至18个碳原子的脂族羧酸,芳族羧酸 1至18个碳原子,磺酸和磷酸酯,然后通过常规方法进一步加工,得到γ-铁(III)氧化物。
-
-
-
-
-
-
-
-
-