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1.发明授权
公开(公告)号：US4970163A
公开(公告)日：1990-11-13
申请号：US399826
申请日：1989-08-28
IPC分类号： C12P17/04
CPC分类号： C12R1/645 , C12P17/04 , Y10S435/911
摘要： Described is a microbilogical method for producing the lactone, sclareolide and a diol having the chemical structure: ##STR1## using sclareol having the structure: ##STR2## as a substrate and using one of the microorganisms: Cryptococcus albidus (saito [skinner var. albidus]), ATCC 20918Bensingtonia ciliata, ATCC 20919Cryptococcus laurentii, ATCC 20920Cryptococcus albidus, ATCC 20921.
摘要翻译： 描述了一种用于生产具有以下化学结构的内酯，香紫苏内酯和二醇的微生物学方法：使用具有以下结构的香叶介体作为底物并使用其中一种微生物：白垩纪（Saito [skinner var。albidus ]），ATCC 20918 Bensingtonia ciliata，ATCC 20919月桂树隐球菌，ATCC 20920隐球菌，ATCC 20921。
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2.发明授权
公开(公告)号：US5188129A
公开(公告)日：1993-02-23
申请号：US759992
申请日：1991-09-13
摘要： Described are smoking tobacco compositions comprising smoking tobacco and intimately admixed therewith an aroma or taste augmenting, enhancing or imparting quantity of a tricyclic ether-substituted acetic acid having the structure: ##STR1##
摘要翻译： 描述了吸烟烟草组合物，其包括吸烟烟草并且与其充分混合增加，增强或赋予量的具有以下结构的三环醚取代的乙酸的香味或味道：
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公开(公告)号：US5155029A
公开(公告)日：1992-10-13
申请号：US555195
申请日：1990-07-20
CPC分类号： C12R1/645 , C12P17/04 , C12P17/06 , C12P7/02 , Y10S435/911
摘要： Described is a microbiological method for producing the cyclic ether having the chemical structure: ##STR1## using a sclareol derivative having one of the structures: ##STR2## and using the microorganism: Cryptococcus laurentii, ATCC 20920.
摘要翻译： 描述了具有以下化学结构的环醚的微生物学方法：使用具有以下结构之一的香紫苏醇衍生物：
或 并使用微生物：月桂葡萄球菌ATCC 20920。 -
公开(公告)号：US5212078A
公开(公告)日：1993-05-18
申请号：US513789
申请日：1990-04-25
CPC分类号： C12R1/645 , C12P17/04 , C12P17/06 , C12P7/02 , Y10S435/911
摘要： Described is a microbiological method for producing the lactone, sclareolide having the structure: ##STR1## and a diol having the chemical structure: ##STR2## using a sclareol derivative having one of the structures: ##STR3## wherein a combination of two or more of the compounds as a substrate and using one of the microorganisms:Cryptococcus albidus, ATCC 20918Bensingtonia ciliata, ATCC 20919Cryptococcus laurentii, ATCC 20920 orCryptococcus albidus, ATCC 20921.
摘要翻译： 描述了具有以下结构的内酯，香紫苏内酯的微生物学方法：具有以下结构的化学结构：具有以下结构之一的香紫苏衍生物的化学结构：
其中两种或更多种化合物作为底物并使用微生物之一的组合：隐球菌，ATCC 20918 Bensingtonia ciliata，ATCC 20919月桂树，ATCC 20920或白化隐球菌ATCC 20921。 -
5.发明授权Octalactone-containing composition, fermentation process for producing same and organoleptic uses thereof 失效含有十八碳烯酮的组合物，用于生产其的发酵方法及其有机酸用途
公开(公告)号：US5166366A
公开(公告)日：1992-11-24
申请号：US797055
申请日：1992-01-23
CPC分类号： C12P17/04 , A23L27/24 , A24B15/403 , A24B15/406 , C11B9/0076 , C11D3/50 , C12P7/42
摘要： Described is a process for the preparation of compositions of matter containing octalactones defined according to the structure: ##STR1## which includes the stereoisomers having the structures: ##STR2## by means of the sequential steps of (i) fermentation of caprylic acid or the ethyl ester of caprylic acid defined according to the generic structure: ##STR3## wherein R is hydrogen or ethyl using a microorganism selected from the group consisting of:Mortierella isabellina, ATCC 44583;Mortierella isabellina, ATCC 38063;Syncephalastrum racemosum, NRRL A-5889;Mortierella isabellina, IFO 7884;Mortierella ramanniana var. angulispora, IFO 8187;Mortierella isabellina, CBS 221.29; andMortierella isabellina, IFO 7873whereby gamma hydroxy octanoic acid or ester thereof defined according to the structure: ##STR4## is formed; and (ii) lactonization of the resulting gamma hydroxy octanoic acid by means of simultaneous acidification and heating according to the reaction sequence: ##STR5##
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公开(公告)号：US5110953A
公开(公告)日：1992-05-05
申请号：US623522
申请日：1990-12-07
申请人： Mohamad I. Farbood , James A. Morris , Mark A. Sprecker , Lynda J. Bienkowski , Kevin P. Miller , Manfred H. Vock , Myrna L. Hagedorn
发明人： Mohamad I. Farbood , James A. Morris , Mark A. Sprecker , Lynda J. Bienkowski , Kevin P. Miller , Manfred H. Vock , Myrna L. Hagedorn
CPC分类号： C12P7/42 , A24B15/403 , C11B9/0073 , C12P17/02 , C12P7/40
摘要： Described is a process for the preparation of compositions of matter containing unsaturated lactones defined according to the generic structure: ##STR1## wherein R represents C.sub.6 alkyl or alkenyl; and X represents C.sub.2, C.sub.4 or C.sub.6 alkylene or alkenylene; with the provisos that R is C.sub.6 alkyl when X is alkenylene and R is C.sub.6 alkenyl when X is alkylene by means of the sequential steps of (i) fermentation of castor oil or ricinoleic acid using a microorganism selected from the group consisting of:Candida petrophilum, ATCC 20226;Candida oleophila, ATCC 20177;Candida sp., ATCC 20504; andCandida sake, ATCC 28137whereby gamma hydroxydecanoic acid and a mixture of other acids defined according to the generic structure: ##STR2## is formed wherein Y represents an oxo-saturated, oxo-unsaturated or di-unsaturated C.sub.9, C.sub.11 or C.sub.13 moiety according to the reaction: ##STR3## (ii) lactonization of the resulting gamma hydroxydecanoic acid by means of simultaneous acidification and heating according to the reaction: ##STR4## and (iii) lactonization (via distillation) of one or more of the resulting acids defined according to the structure: ##STR5## to form one or more lactones defined according to the generic structure: ##STR6## according to the reaction: ##STR7## wherein the sum of the number of carbon atoms in the X moiety and in the R moiety is equal to the number of carbon atoms in the Y moiety minus 1.Also described are the products produced according to such process as well as their organoleptic utilities for augmenting or enhancing the aroma or taste of consumable materials selected from the group consisting of perfume compositions, colognes, perfumed articles, perfumed polymers, foodstuffs, chewing gums, medicinal products, toothpastes, chewing tobaccos and smoking tobaccos.
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公开(公告)号：US4960597A
公开(公告)日：1990-10-02
申请号：US279065
申请日：1988-12-02
申请人： Mohamad I. Farbood , James A. Morris , Mark A. Sprecker , Lynda J. Bienkowski , Kevin P. Miller , Manfred H. Vock , Myrna L. Hagedorn
发明人： Mohamad I. Farbood , James A. Morris , Mark A. Sprecker , Lynda J. Bienkowski , Kevin P. Miller , Manfred H. Vock , Myrna L. Hagedorn
CPC分类号： C11B9/0073 , A24B15/403 , C12P17/02 , C12P7/40 , C12P7/42
摘要： Described is a process for the preparation of compositions of matter containing unsaturated lactones defined according to the generic structure: ##STR1## wherein R represents C.sub.6 alkyl or alkenyl; and X represents C.sub.2, C.sub.4 or C.sub.6 alkylene or alkenylene; with the provisos that R is C.sub.6 alkyl when X is alkenylene and R is C.sub.6 alkenyl when X is alkylene by means of the sequential steps of (i) fermentation of castor oil or ricinoleic acid using a microorganism selected from the group consisting of:Candida petrophilum, ATCC 20226;Candida oleophila, ATCC 20177;Candida sp., ATCC 20504; andCandida sake, ATCC 28137whereby gamma hydroxydecanoic acid and a mixture of other acids defined according to the generic structure: ##STR2## is formed wherein Y represents an oxo-saturated, oxo-unsaturated or di-unsaturated C.sub.9, C.sub.11 or C.sub.13 moiety according to the reaction: ##STR3## (ii) lactonization of the resulting gamma hydroxydecanoic acid by means of simultaneous acidification and heating according to the reaction: ##STR4## and (iii) lactonization (via distillation) of one or more of the resulting acids defined according to the structure: ##STR5## to form one or more lactones defined according to the generic structure: ##STR6## according to the reaction: ##STR7## wherein the sum of the number of carbon atoms in the X moiety and in the R moiety is equal to the number of carbon atoms in the Y moiety minus 1.Also described are the products produced according to such process as well as their organoleptic utilities for augmenting or enhancing the aroma or taste of consumable materials selected from the group consisting of perfume compositions, colognes, perfumed articles, perfumed polymers, foodstuffs, chewing gums, medicinal products, toothpastes, chewing tobaccos and smoking tobaccos.
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8.发明授权Octalactone-containing composition, fermentation process for producing same and organoleptic uses thereof 失效含有八聚内酯的组合物，用于生产其的发酵方法及其感官用途
公开(公告)号：US5274128A
公开(公告)日：1993-12-28
申请号：US887144
申请日：1992-05-22
CPC分类号： C12P17/04 , A23L27/24 , A24B15/403 , A24B15/406 , C11B9/0076 , C11D3/50 , C12P7/42 , Y10S435/911
摘要： Described is a process for the preparation of compositions of matter containing octalactones defined according to the structure: ##STR1## which includes the stereoisomers having the structures: ##STR2## by means of the sequential steps of (i) fermentation of caprylic acid or the ethyl ester of caprylic acid defined according to the generic structure: ##STR3## wherein R is hydrogen or ethyl using a microorganism selected from the group consisting of:Mortierella ramanniana var. ramanniana--CBS 112.08Mortierella ramanniana var. ramanniana--CBS 478.63Choanephora cucurbitarum--NRRL 2744Mortierella isabellina--IFO 8183Mortierella isabellina--IFO 8309Mortierella nana--IFO 8794Mortierella isabellina--IFO 7824Mortierella vinacea--IFO 6738whereby a gamma hydroxy octanoic acid defined according to the structure: ##STR4## is formed; and (ii) lactonization of the resulting gamma hydroxy octanoic acid by means of simultaneous acidification and heating according to the reaction sequence: ##STR5##
摘要翻译： 描述了根据以下结构定义的含有八聚核苷酸的物质组合物的方法：其包括具有以下结构的立体异构体：其中包括具有以下结构的顺式步骤：（i）辛酸发酵 酸或根据通用结构定义的辛酸的乙酯：其中R是氢或乙基，使用选自以下的微生物：高山被孢霉（Mortierella ramanniana var。 ramanniana-CBS 112.08 Mortierella ramanniana var。 苎麻 - CBS 478.63葫芦巴-RNRL 2744高山被孢霉-IFO 8183高山被孢霉-IFO 8309高山被孢霉nana-IFO 8794被孢霉被孢霉-IFO 7824高山被孢霉Vinacea-IFO 6738，由此根据以下结构定义的γ-羟基辛酸：
形成 和（ii）通过根据反应顺序的同时酸化和加热来对所得的γ-羟基辛酸进行内酯化： 和 -
9.发明授权Octalactone-containing composition, fermentation process for producing same and organoleptic uses thereof 失效含有八聚内酯的组合物，用于生产其的发酵方法及其感官用途
公开(公告)号：US5112803A
公开(公告)日：1992-05-12
申请号：US719154
申请日：1991-06-21
CPC分类号： C11B9/0076 , A24B15/406 , C11D3/50 , C12P17/04
摘要： Described is a process for the preparation of compositions of matter containing octalactones defined according to the structure: ##STR1## which includes the stereoisomers having the structures: ##STR2## by means of the sequential steps of (i) fermentation of caprylic acid or the ethyl ester of caprylic acid defined according to the generic structure: ##STR3## wherein R is hydrogen or ethyl using a microorganism selected from the group consisting of:Mortierella isabellina, ATCC 44583;Mortierella isabellina, ATCC 38063;Syncephalastrum racemosum, NRRL A-5889;Mortierella isabellina, IFO 7884;Mortierella ramanniana var. angulispora, IFO 8187;Mortierella isabellina, CBS 221.29; andMortierella isabellina, IFO 7873whereby gamma hydroxy octanoic acid or ester thereof defined according to the structure: ##STR4## is formed; and (ii) lactonization of the resulting gamma hydroxy octanoic acid by means of simultaneous acidification and heating according to the reaction sequence:
摘要翻译： 描述了根据以下结构定义的含有八聚核苷酸的物质组合物的方法：其包括具有以下结构的立体异构体：其中包括具有以下结构的顺式步骤：（i）辛酸发酵 酸或根据通用结构定义的辛酸乙酯：其中R是氢或乙基，使用选自以下的微生物：高山被孢霉（Mortierella isabellina），ATCC 44583; 被孢霉（Mortierella isabellina），ATCC 38063; 沙门氏菌，NRRL A-5889; 高山被孢霉，IFO 7884; 高山被孢霉 angulispora，IFO 8187; 高山被孢霉，CBS 221.29; 和高山被孢霉（Mortierella isabellina），IFO 7873，由此形成根据以下结构定义的γ羟基辛酸或其酯： 和（ii）通过根据反应顺序的同时酸化和加热来对所得的γ-羟基辛酸进行内酯化：
和 -
10.发明授权Process for preparing compositions containing unsaturated lactones, products produced thereby and organoleptic uses of said products 失效制备含有不饱和内酯的组合物，由此生产的产品和所述产品的感官用途的方法
公开(公告)号：US4946782A
公开(公告)日：1990-08-07
申请号：US228512
申请日：1988-08-05
申请人： Mohamad I. Farbood , James A. Morris , Mark A. Sprecker , Lynda J. Bienkowski , Kevin P. Miller , Manfred H. Vock , Myrna L. Hagedorn
发明人： Mohamad I. Farbood , James A. Morris , Mark A. Sprecker , Lynda J. Bienkowski , Kevin P. Miller , Manfred H. Vock , Myrna L. Hagedorn
CPC分类号： C12P17/02 , A24B15/403 , C11B9/0073 , C12P7/40 , C12P7/42
摘要： Described is a process for the preparation of compositions of matter containing unsaturated lactones defined according to the generic structure: ##STR1## wherein R represents C.sub.6 alkyl or alkenyl; and X represents C.sub.2, C.sub.4 or C.sub.6 alkylene or alkenylene; with the provisos that R is C.sub.6 alkyl when X is alkenylene and R is C.sub.6 alkenyl when X is alkylene by means of the sequential steps of (i) fermentation of castor oil or ricinoleic acid using a microorganism selected from the group consisting of:Candida petrophilum, ATCC 20226;Candida oleophila, ATCC 20177;Candida sp., ATCC 20504; andCandida sake, ATCC 28137whereby gamma hydroxydecanoic acid and a mixture of other acids defined according to the generic structure: ##STR2## is formed wherein Y represents an oxo-saturated, oxo-unsaturated or di-unsaturated C.sub.9, C.sub.11 or C.sub.13 moiety according to the reaction: ##STR3## (ii) lactonization of the resulting gamma hydroxydecanoic acid by means of simultaneous acidification and heating according to the reaction: ##STR4## and (iii) lactonization (via distillation) of one or more of the resulting acids defined according to the structure: ##STR5## to form one or more lactones defined according to the generic structure: ##STR6## according to the reaction: ##STR7## wherein the sum of the number of carbon atoms in the X moiety and in the R moiety is equal to the number of carbon atoms in the Y moiety minus 1.Also described are the products produced according to such process as well as their organoleptic utilities for augmenting or enhancing the aroma or taste of consumable materials selected from the group consisting of perfume compositions, colognes, perfumed articles, foodstuffs, chewing gums, medicinal products, toothpastes, chewing tobaccos and smoking tobaccos.
摘要翻译： 描述了根据通用结构定义的含有不饱和内酯的物质组合物的方法：其中R表示C6烷基或烯基; X表示C2，C4或C6亚烷基或亚烯基; 条件是当X是亚烯基时R是C6烷基，当X是亚烷基时，R是C6链烯基，通过以下顺序的步骤：（i）使用选自以下的微生物来蓖麻油或蓖麻油酸发酵：念珠菌 ，ATCC 20226; 嗜油假丝酵母，ATCC 20177; 念珠菌属，ATCC 20504; 和念珠菌，ATCC 28137，由此形成根据通用结构定义的γ-羟基癸酸和其它酸的混合物：其中Y表示氧代饱和的，不饱和的或不饱和的C 9，C 11或C 13部分，根据 （ii）通过根据以下反应的同时酸化和加热来对所得的γ-羟基癸酸进行内酯化：（ⅲ）内酯化（经蒸馏） 根据以下结构定义的一种或多种所得酸：
以形成根据通用结构定义的一种或多种内酯：根据该反应： 其中，碳原子数 X部分和R部分等于Y部分中的碳原子数减1。还描述了根据这种方法产生的产物以及它们的感官效用，用于增强或增强co的香气或味道 选自香水组合物，古龙水，香料制品，食品，口香糖，药用产品，牙膏，咀嚼烟草和吸烟烟草的可选材料。
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