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公开(公告)号：US4009214A
公开(公告)日：1977-02-22
申请号：US571805
申请日：1975-04-25
申请人： Morgan C. Sze , John E. Paustian
发明人： Morgan C. Sze , John E. Paustian
IPC分类号： B01D53/68 , B01D53/02 , B01J20/04 , C01B7/00 , C01B7/01 , C01B7/07 , C07C17/154 , C07C17/38 , C07C19/10 , C07C17/15 , C07C7/08
摘要： Hydrogen chloride gas, containing hydrogen fluoride and/or silicon tetrafluoride, is contacted with calcium chloride supported on activated alumina, to separate the hydrogen fluoride and/or silicon tetrafluoride therefrom.
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公开(公告)号：US4008241A
公开(公告)日：1977-02-15
申请号：US609626
申请日：1975-09-02
IPC分类号： C07D213/803 , C07D213/81 , C07D213/82 , C07D213/56
CPC分类号： C07D213/81
摘要： Nicotinamide is produced by aqueous ammonia hydrolysis of nicotinonitrile wherein the conversion is limited to at least 30% and no greater than 70%, with the nicotinonitrile concentration, expressed as weight product amide per 100 pounds of water, being at least 100 parts and no greater than 300 parts, with the hydrolysis being effected in the presence of ammonium nicotinate in an amount sufficient to essentially eliminate net production thereof. Ammonia and nicotinonitrile are stripped from the hydrolysis effluent, and nicotinamide recovered, by crystallization, from the stripped hydrolysis effluent.
摘要翻译： 烟酰胺是通过烟腈氨水解产生的，其中转化率限制在至少30％且不大于70％，烟腈浓度以每100磅水重量产物酰胺表示，至少为100份且不大于 超过300份，水解在烟酸铵存在下进行，其量足以基本上消除其净产生。 从水解流出物中除去氨和烟腈，并通过结晶从汽提的水解流出物中回收烟酰胺。
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公开(公告)号：US4174452A
公开(公告)日：1979-11-13
申请号：US877339
申请日：1978-02-13
IPC分类号： C07C51/08 , C07C63/26 , C07D213/55
CPC分类号： C07C51/08
摘要： A nitrile, such as terephthalonitrile or nicotinonitrile is reacted with water, in the vapor phase, in the presence of a catalyst, such as supported phosphoric acid, to produce the corresponding carboxylic acid.
摘要翻译： 在催化剂如负载磷酸的存在下，将腈，如对苯二腈或烟腈与水在气相中反应，生成相应的羧酸。
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公开(公告)号：US3931243A
公开(公告)日：1976-01-06
申请号：US436861
申请日：1974-01-28
IPC分类号： C07D307/89 , C07C51/00 , C07C51/06 , C07C51/08 , C07C51/41 , C07C51/54 , C07C67/00 , C07C209/00 , C07C211/63
摘要： Anhydrides of carboxylic acids, more particularly, of aromatic, naphthenic and saturated aliphatic acids having at least one pair of carboxyl groups attached to adjacent carbon atoms, can be prepared by thermal decomposition of amine salts of the acids, with removal of the amine. The amine salts may be produced by aqueous hydrolysis of the corresponding nitriles, imides, or amides in the presence of an amine, or by hydrolysis to the ammonium salts followed by conversion to the amine salt by stripping off ammonia in the presence of an amine.
摘要翻译： 具有至少一对连接到相邻碳原子上的羧基的羧酸的酸酐，更特别是具有至少一对羧基的芳族，环烷基和饱和脂肪酸的酸酐可通过胺的胺盐的热分解来制备。 胺盐可以通过在胺存在下水解相应的腈，酰亚胺或酰胺，或通过水解成铵盐，然后通过在胺的存在下通过汽提来转化成胺盐来制备。
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公开(公告)号：US4691031A
公开(公告)日：1987-09-01
申请号：US622767
申请日：1984-06-20
申请人： George D. Suciu , John E. Paustian
发明人： George D. Suciu , John E. Paustian
CPC分类号： C07C17/15 , B01J8/0055 , B01J8/28 , B01J8/34 , B01J8/386 , B01J8/388 , C07C51/215 , B01J2208/00141
摘要： A process for preventing backmixing in a fluidized bed vessel wherein a gaseous fluid phase and fluidized solids are moved co-currently through a plurality of fluid bed compartments in substantially plug flow. The vessel may be used for production of maleic anhydride.
摘要翻译： 一种用于防止流化床容器中的回混的方法，其中气态流体相和流化固体通过基本上塞子流中的多个流化床隔室同时移动。 该容器可用于生产马来酸酐。
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公开(公告)号：US4415460A
公开(公告)日：1983-11-15
申请号：US369352
申请日：1982-04-19
申请人： George D. Suciu , John E. Paustian
发明人： George D. Suciu , John E. Paustian
CPC分类号： C01D3/14 , C02F1/76 , C25B15/08 , Y10S210/908
摘要： Organic impurities in aqueous salt solutions; e.g., alkali or alkaline earth chloride solutions in particular, brines, are oxidized with chlorate ions at a pH of no greater than 5.0 and a temperature of at least 130.degree. C. to convert the organics to carbon dioxide. The process has particular applicability to oxidation of organic impurities in an aqueous brine solution derived from the saponification of a chlorohydrin to olefin oxide, prior to introduction of the brine into an electrolytic cell.
摘要翻译： 盐水溶液中的有机杂质; 例如碱金属或碱土金属氯化物溶液，特别是盐水，在不大于5.0的pH和至少130℃的温度下用氯酸根离子氧化，以将有机物转化为二氧化碳。 在将盐水引入电解池之前，该方法特别适用于在衍生自氯代醇至烯烃氧化物的皂化中衍生的盐水水溶液中的有机杂质的氧化。
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公开(公告)号：US5003119A
公开(公告)日：1991-03-26
申请号：US478749
申请日：1990-02-12
IPC分类号： C07C2/66 , C07C4/00 , C07C15/02 , C07C15/085
CPC分类号： C07C15/085 , C07C15/02 , C07C2/66 , C07C4/00 , C07C2529/04
摘要： A process for the manufacture of alkylbenzenes wherein a feed of fresh and recycle benzene and fresh olefin are reacted in the presence of an alkylation catalyst in an alkylator having at least two reaction stages wherein each stage is adiabatic. Essentially all of the olefin is completely reacted in each stage of the alkylator. Fresh olefin is fed into each stage of the alkylator. Preferred alkylbenzenes which are produced by this process are ethylbenzene and cumene.
摘要翻译： 制备烷基苯的方法，其中新鲜和再循环的苯和新鲜烯烃的进料在具有至少两个反应阶段的烷基化催化剂存在下反应，其中每个阶段是绝热的。 基本上所有的烯烃在烷基化剂的每个阶段都完全反应。 将新鲜的烯烃加入到烷基化器的每个阶段。 通过该方法制备的优选的烷基苯是乙苯和枯烯。
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公开(公告)号：US4240885A
公开(公告)日：1980-12-23
申请号：US61743
申请日：1979-07-30
申请人： George D. Suciu , John E. Paustian
发明人： George D. Suciu , John E. Paustian
摘要： Organic impurities in aqueous salt solutions; e.g., alkali or alkaline earth chloride solutions in particular, brines, are oxidized with chlorate ions at a pH of no greater than 5.0 and a temperature of at least 130.degree. C. to convert the organics to carbon dioxide. The process has particular applicability to oxidation of organic impurities in an aqueous brine solution derived from the saponification of a chlorohydrin to olefin oxide, prior to introduction of the brine into an electrolytic cell.
摘要翻译： 盐水溶液中的有机杂质; 例如碱金属或碱土金属氯化物溶液，特别是盐水，在不大于5.0的pH和至少130℃的温度下用氯酸根离子氧化，以将有机物转化为二氧化碳。 在将盐水引入电解池之前，该方法特别适用于在衍生自氯代醇至烯烃氧化物的皂化中衍生的盐水水溶液中的有机杂质的氧化。
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公开(公告)号：US3944598A
公开(公告)日：1976-03-16
申请号：US372047
申请日：1973-06-21
IPC分类号： C07C51/54 , C07C87/00 , C07D213/00 , C07D295/00 , C07D307/00
CPC分类号： C07C51/54
摘要： Amine salts of aromatic and aliphatic carboxylic acids are produced by hydrolysis of a corresponding nitrile, imide, amide or mixtures thereof in the presence of an amine, and stripping of evolved ammonia. The amine salts may be used in separation of certain isomeric acids, and are useful as intermediates in the production of the corresponding carboxylic acids and derivatives thereof, such as esters and anhydrides.
摘要翻译： 芳族和脂族羧酸的胺盐通过在胺的存在下水解相应的腈，酰亚胺，酰胺或其混合物，以及汽提放出的氨来制备。 胺盐可用于分离某些异构酸，并且可用作制备相应的羧酸及其衍生物如酯和酸酐的中间体。
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