Method of producing β-sialon fluorescent material

    公开(公告)号:US11512250B2

    公开(公告)日:2022-11-29

    申请号:US17120662

    申请日:2020-12-14

    Abstract: Provided is a method of producing a β-sialon fluorescent material having a high light emission intensity and an excellent light emission luminance. The method includes preparing a calcined product having a composition of β-sialon containing an activating element; grinding the calcined product to obtain a ground product; and heat-treating the ground product to obtain a heat-treated product. A specific surface area of the ground product is 0.2 m2/g or more.

    Method for producing β-sialon fluorescent material

    公开(公告)号:US11427758B2

    公开(公告)日:2022-08-30

    申请号:US16504937

    申请日:2019-07-08

    Abstract: A method for producing β-sialon fluorescent material having excellent emission intensity is provided. The method for producing β-sialon fluorescent material includes providing a composition comprising silicon nitride that contains aluminium, an oxygen atom, and europium, heat treating the composition, contacting the heat-treated composition with a basic substance, and washing the composition, which has been contacted with the basic substance, with an acidic liquid medium.

    Method for producing beta-sialon fluorescent material

    公开(公告)号:US10316249B2

    公开(公告)日:2019-06-11

    申请号:US15165580

    申请日:2016-05-26

    Abstract: A method for producing a β-sialon fluorescent material superior in light emitting luminance is provided. The method includes heat-treating a first mixture containing an aluminum compound, a europium compound, and a first silicon oxynitride compound to obtain a first heat-treated product, and heat-treating a second mixture containing the first heat-treated product, an aluminum compound, a europium compound, and a second silicon oxynitride compound, which has a larger oxygen content than the first silicon oxynitride compound, to obtain a second heat-treated product.

    Method for producing β-sialon fluorescent material

    公开(公告)号:US11560514B2

    公开(公告)日:2023-01-24

    申请号:US16454917

    申请日:2019-06-27

    Abstract: Provided is a method for producing a β-sialon fluorescent material, comprising preparing a composition containing a silicon nitride that contains aluminium, oxygen, and europium; heat-treating the composition at a temperature in a range of 1300° C. or more and 1600° C. or less to obtain a heat-treated product; subjecting the heat-treated product to a temperature-decrease of from the heat treatment temperature to 1000° C. as a first temperature-decrease step; and subjecting the heat-treated product to a temperature-decrease of from 1000° C. to 400° C. as a second temperature-decrease step. The first temperature-decrease step has a temperature-decrease rate in a range of 1.5° C./min or more and 200° C./min or less, and the second temperature-decrease step has a temperature-decrease rate in a range of 1° C./min or more and 200° C./min or less.

    Method for producing β-sialon fluorescent material

    公开(公告)号:US10385267B2

    公开(公告)日:2019-08-20

    申请号:US15378690

    申请日:2016-12-14

    Abstract: A method for producing β-sialon fluorescent material having excellent emission intensity is provided. The method for producing β-sialon fluorescent material includes providing a composition comprising silicon nitride that contains aluminum, an oxygen atom, and europium, heat treating the composition, and contacting the heat-treated composition with a basic substance.

Patent Agency Ranking