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公开(公告)号:US10894917B2
公开(公告)日:2021-01-19
申请号:US15606153
申请日:2017-05-26
Applicant: NICHIA CORPORATION
Inventor: Kenichi Aoyagi , Takashi Kaide , Motoharu Morikawa , Shoji Hosokawa
Abstract: Provided is a method of producing a β-sialon fluorescent material having a high light emission intensity and an excellent light emission luminance. The method includes preparing a calcined product having a composition of β-sialon containing an activating element; grinding the calcined product to obtain a ground product; and heat-treating the ground product to obtain a heat-treated product. A specific surface area of the ground product is 0.2 m2/g or more.
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公开(公告)号:US11512248B2
公开(公告)日:2022-11-29
申请号:US17033576
申请日:2020-09-25
Applicant: NICHIA CORPORATION
Inventor: Kenichi Aoyagi , Takashi Kaide , Yuya Takahashi , Shoji Hosokawa
IPC: C09K11/77 , C01F17/30 , C09K11/08 , C01B21/082
Abstract: Provided a method of producing a β-sialon fluorescent material having excellent emission intensity. The method includes providing a first composition containing aluminum, an oxygen atom, and a europium-containing silicon nitride, heat treating the first composition, contacting the heat-treated composition and a basic substance to obtain a second composition, and contacting the second composition resulting from contacting the heat-treated composition with the basic substance and an acidic liquid medium containing an acidic substance.
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公开(公告)号:US10833230B2
公开(公告)日:2020-11-10
申请号:US16793018
申请日:2020-02-18
Applicant: NICHIA CORPORATION
Inventor: Kenichi Aoyagi , Takashi Kaide , Takuya Nakabayashi , Tetsuya Ishikawa , Shoji Hosokawa
Abstract: A wavelength converting member comprising a first wavelength converting layer containing: a first fluorescent material having a light emission peak wavelength in a range of 620 nm or more and 660 nm or less; a second fluorescent material having a light emission peak wavelength in a range of 510 nm or more and 560 nm or less; and a resin, wherein the average particle diameter, as measured according to a Fisher Sub-Sieve Sizer method, of the first fluorescent material is in a range of 2 μm or more and 30 μm or less, wherein the second fluorescent material comprises a β-SiAlON fluorescent material, the circularity of the β-SiAlON fluorescent material is 0.7 or more, and the volume average particle diameter, as measured according to a laser diffraction scattering particle size distribution measuring method, of the β-SiAlON fluorescent material is in a range of 2 μm or more and 30 μm or less, and wherein the thickness of the first wavelength converting layer is in a range of 50 μm or more and 200 μm or less.
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公开(公告)号:US10608149B2
公开(公告)日:2020-03-31
申请号:US16369046
申请日:2019-03-29
Applicant: NICHIA CORPORATION
Inventor: Kenichi Aoyagi , Takashi Kaide , Takuya Nakabayashi , Tetsuya Ishikawa , Shoji Hosokawa
Abstract: A wavelength converting member comprising a first wavelength converting layer containing: a first fluorescent material having a light emission peak wavelength in a range of 620 nm or more and 660 nm or less; a second fluorescent material having a light emission peak wavelength in a range of 510 nm or more and 560 nm or less; and a resin, wherein the average particle diameter, as measured according to a Fisher Sub-Sieve Sizer method, of the first fluorescent material is in a range of 2 μm or more and 30 μm or less, wherein the second fluorescent material comprises a β-SiAlON fluorescent material, the circularity of the β-SiAlON fluorescent material is 0.7 or more, and the volume average particle diameter, as measured according to a laser diffraction scattering particle size distribution measuring method, of the β-SiAlON fluorescent material is in a range of 2 μm or more and 30 μm or less, and wherein the thickness of the first wavelength converting layer is in a range of 50 μm or more and 200 μm or less.
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公开(公告)号:US10316249B2
公开(公告)日:2019-06-11
申请号:US15165580
申请日:2016-05-26
Applicant: NICHIA CORPORATION
Inventor: Motoharu Morikawa , Kenichi Aoyagi , Takashi Kaide , Shoji Hosokawa
IPC: C09K11/77
Abstract: A method for producing a β-sialon fluorescent material superior in light emitting luminance is provided. The method includes heat-treating a first mixture containing an aluminum compound, a europium compound, and a first silicon oxynitride compound to obtain a first heat-treated product, and heat-treating a second mixture containing the first heat-treated product, an aluminum compound, a europium compound, and a second silicon oxynitride compound, which has a larger oxygen content than the first silicon oxynitride compound, to obtain a second heat-treated product.
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公开(公告)号:US10190044B2
公开(公告)日:2019-01-29
申请号:US15228109
申请日:2016-08-04
Applicant: NICHIA CORPORATION
Inventor: Shoji Hosokawa , Motoharu Morikawa , Tadayoshi Yanagihara , Kenichi Aoyagi , Takashi Kaide
Abstract: A method for producing a β-sialon fluorescent material can be provided. The method includes preparing a composition containing silicon nitride that contains aluminium, an oxygen atom, and europium, heat-treating the composition in a rare gas atmosphere or in a vacuum, and contacting the heat-treated composition with a gas containing elemental fluorine.
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公开(公告)号:US11427758B2
公开(公告)日:2022-08-30
申请号:US16504937
申请日:2019-07-08
Applicant: NICHIA CORPORATION
Inventor: Motoharu Morikawa , Shoji Hosokawa , Takashi Kaide , Kenichi Aoyagi
Abstract: A method for producing β-sialon fluorescent material having excellent emission intensity is provided. The method for producing β-sialon fluorescent material includes providing a composition comprising silicon nitride that contains aluminium, an oxygen atom, and europium, heat treating the composition, contacting the heat-treated composition with a basic substance, and washing the composition, which has been contacted with the basic substance, with an acidic liquid medium.
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公开(公告)号:US11512250B2
公开(公告)日:2022-11-29
申请号:US17120662
申请日:2020-12-14
Applicant: NICHIA CORPORATION
Inventor: Kenichi Aoyagi , Takashi Kaide , Motoharu Morikawa , Shoji Hosokawa
Abstract: Provided is a method of producing a β-sialon fluorescent material having a high light emission intensity and an excellent light emission luminance. The method includes preparing a calcined product having a composition of β-sialon containing an activating element; grinding the calcined product to obtain a ground product; and heat-treating the ground product to obtain a heat-treated product. A specific surface area of the ground product is 0.2 m2/g or more.
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公开(公告)号:US11753302B2
公开(公告)日:2023-09-12
申请号:US17937766
申请日:2022-10-03
Applicant: NICHIA CORPORATION
Inventor: Kenichi Aoyagi , Takashi Kaide , Yuya Takahashi , Shoji Hosokawa
IPC: C01B21/082 , C01F17/30 , C09K11/08 , C09K11/77
CPC classification number: C01B21/0826 , C01F17/30 , C09K11/0883 , C09K11/7734 , C09K11/77348
Abstract: Provided a method of producing a β-sialon fluorescent material having excellent emission intensity. The method includes providing a first composition containing aluminum, an oxygen atom, and a europium-containing silicon nitride, heat treating the first composition, contacting the heat-treated composition and a basic substance to obtain a second composition, and contacting the second composition resulting from contacting the heat-treated composition with the basic substance and an acidic liquid medium containing an acidic substance.
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公开(公告)号:US10093855B2
公开(公告)日:2018-10-09
申请号:US15172862
申请日:2016-06-03
Applicant: NICHIA CORPORATION
Inventor: Kenichi Aoyagi , Takashi Kaide , Motoharu Morikawa , Shoji Hosokawa
IPC: C09K11/77
Abstract: A method for producing a β-sialon fluorescent material is provided. The method includes heat-treating a mixture containing an aluminum compound, a first europium compound, and silicon nitride to obtain a first heat-treated product; and heat-treating the first heat-treated product with a second europium compound in a rare gas atmosphere to obtain a second heat-treated product.
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