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    DETECTION OF DEFECTS IN SOLID-POLYMER COATINGS USING REDUCTION-OXIDATION PROBES
    1.
    发明申请
    DETECTION OF DEFECTS IN SOLID-POLYMER COATINGS USING REDUCTION-OXIDATION PROBES 有权
    使用减少氧化探针检测固体聚合物涂层中的缺陷

    公开(公告)号：US20140174954A1

    公开(公告)日：2014-06-26

    申请号：US14058512

    申请日：2013-10-21

    申请人： PRIETO BATTERY, INC. ,  COLORADO STATE UNIVERSITY RESEARCH FOUNDATION

    发明人： Derek C. Johnson ,  Amy L. Prieto ,  Matthew Rawls ,  Wesley A. Hoffert

    IPC分类号： G01N27/26

    CPC分类号： H01M10/0585 ,  C09D5/24 ,  C09D5/4407 ,  G01N17/02 ,  G01N27/26 ,  G01N27/48 ,  H01M2/145 ,  H01M2/1653 ,  H01M10/0525 ,  Y10T29/49115

    摘要： Electrochemical methods for probing solid polymer electrolyte surface coatings on electrically conducting, active, three-dimensional electrode materials for use in lithium-ion batteries, to quantitatively determine the conformity, uniformity, and the presence of pinholes, and/or other defects in coatings, without requiring the detachment of the coating from the electrode or otherwise inducing damage to the coating, are described. Coated electrodes are submersed in an electrolyte solution containing a redox-active probe species which does not induce electrochemical damage to either the working electrode or the solid polymer electrolyte surface coating. For coated Cu2Sb working electrodes, molecules including a water-soluble redox active viologen moiety have been found to be effective. The current as a function of the applied potential for an uncoated working electrode is used as a baseline for testing solid polymer surface coatings on working electrodes, and the difference in the observed current between the electrodes for a given potential is a quantitative indicator of the ability of the probe species to access the surface of the working electrode through the solid polymer electrolyte coating.

    摘要翻译： 在用于锂离子电池的导电，活性，三维电极材料上探测固体聚合物电解质表面涂层的电化学方法，以定量确定针孔的一致性，均匀性和/或其他缺陷， 描述了不需要从电极分离涂层或以其他方式引起对涂层的损伤。 涂覆电极浸没在含有不会对工作电极或固体聚合物电解质表面涂层引起电化学损伤的氧化还原活性探针物质的电解质溶液中。 对于包被的Cu2Sb工作电极，已经发现包括水溶性氧化还原活性成核剂部分的分子是有效的。 作为未涂覆的工作电极的施加电位的函数的电流被用作在工作电极上测试固体聚合物表面涂层的基线，并且给定电位的电极之间观察到的电流的差异是能量的定量指标 的探针物质通过固体聚合物电解质涂层进入工作电极的表面。

    Electropolymerization of a coating onto an electrode material
    5.
    发明授权
    Electropolymerization of a coating onto an electrode material 有权
    将涂层电聚合到电极材料上

    公开(公告)号：US09337514B2

    公开(公告)日：2016-05-10

    申请号：US14059148

    申请日：2013-10-21

    申请人： COLORADO STATE UNIVERSITY RESEARCH FOUNDATION ,  PRIETO BATTERY, INC.

    发明人： Derek C. Johnson ,  Amy L. Prieto ,  Matthew Rawls ,  Daniel J. Bates ,  C. Michael Elliott

    IPC分类号： H01M10/0585 ,  H01M10/0525 ,  H01M2/14 ,  H01M2/16 ,  C25D11/00 ,  G01N27/26

    CPC分类号： H01M10/0585 ,  C09D5/24 ,  C09D5/4407 ,  G01N17/02 ,  G01N27/26 ,  G01N27/48 ,  H01M2/145 ,  H01M2/1653 ,  H01M10/0525 ,  Y10T29/49115

    摘要： Methods for reductively polymerizing vinylic based monomers from a solution thereof onto the surface of an electrode material, resulting in thin, electrically insulating solid-polymer electrolyte coatings strongly bound to the surface of the electrode material, are described. The strong bond permits a second electrode to be coated directly onto the solid-polymer electrolyte, thereby incorporating the required components for a Li-ion battery cell. At least one initiator species, which is readily reduced by accepting an electron from the electrode material, is included in electropolymerization deposition solution for permitting the polymerization of vinylic species that would otherwise not electrochemically polymerize without damage to either the electrode material or to the solvents employed.

    摘要翻译： 描述了将乙烯基类单体从其溶液还原聚合到电极材料的表面上的方法，导致与电极材料的表面强烈结合的薄的电绝缘的固体聚合物电解质涂层。 强键可以将第二电极直接涂覆在固体聚合物电解质上，从而将所需的组分用于锂离子电池。 至少一种引发剂物质通过从电极材料中接收电子而容易地还原，包括在电聚合沉积溶液中，用于允许不会电化学聚合而不损坏电极材料或所用溶剂的乙烯基物质的聚合 。

    ELECTROPOLYMERIZATION OF A COATING ONTO AN ELECTRODE MATERIAL
    6.
    发明申请
    ELECTROPOLYMERIZATION OF A COATING ONTO AN ELECTRODE MATERIAL 有权
    电镀在电极材料上的电解

    公开(公告)号：US20140173889A1

    公开(公告)日：2014-06-26

    申请号：US14059148

    申请日：2013-10-21

    申请人： PRIETO BATTERY, INC. ,  COLORADO STATE UNIVERSITY RESEARCH FOUNDATION

    发明人： Derek C. Johnson ,  Amy L. Prieto ,  Matthew Rawls ,  Daniel J. Bates ,  C. Michael Elliott

    IPC分类号： H01M10/0585

    CPC分类号： H01M10/0585 ,  C09D5/24 ,  C09D5/4407 ,  G01N17/02 ,  G01N27/26 ,  G01N27/48 ,  H01M2/145 ,  H01M2/1653 ,  H01M10/0525 ,  Y10T29/49115

    摘要： Methods for reductively polymerizing vinylic based monomers from a solution thereof onto the surface of an electrode material, resulting in thin, electrically insulating solid-polymer electrolyte coatings strongly bound to the surface of the electrode material, are described. The strong bond permits a second electrode to be coated directly onto the solid-polymer electrolyte, thereby incorporating the required components for a Li-ion battery cell. At least one initiator species, which is readily reduced by accepting an electron from the electrode material, is included in electropolymerization deposition solution for permitting the polymerization of vinylic species that would otherwise not electrochemically polymerize without damage to either the electrode material or to the solvents employed.

    摘要翻译： 描述了将乙烯基类单体从其溶液还原聚合到电极材料的表面上的方法，导致与电极材料的表面强烈结合的薄的电绝缘的固体聚合物电解质涂层。 强键可以将第二电极直接涂覆在固体聚合物电解质上，从而将所需的组分用于锂离子电池。 至少一种引发剂物质通过从电极材料中接收电子而容易地还原，包括在电聚合沉积溶液中，用于允许不会电化学聚合而不损坏电极材料或所用溶剂的乙烯基物质的聚合 。