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公开(公告)号：US20050176977A1
公开(公告)日：2005-08-11
申请号：US10513314
申请日：2003-04-25
IPC分类号： C07C67/03 , C07C67/333 , C11C3/06 , C11C3/14 , C07C51/347
CPC分类号： C11C3/14 , C07B2200/09 , C07C67/03 , C07C67/333 , C11C3/06 , C07C69/587
摘要： Processes for preparing conjugated fatty acid glycerides comprising: (a) isomerizing a fatty acid lower alkyl ester corresponding to the general formula (I) in the presence of a basic catalyst at a temperature of from 100 to 160° C., to form a conjugated fatty acid lower alkyl ester: R1CO—OR2 (I) wherein R1CO represents an acyl radical having from 16 to 22 carbon atoms and at least two carbon-carbon unsaturations and R2 represents an alkyl radical having from 1 to 4 carbon atoms; and (b) transesterifying the conjugated fatty acid lower alkyl ester with glycerol to form a conjugated fatty acid glyceride, wherein a lower alkanol corresponding to the general formula R2OH is formed, wherein R2 is as defined above, and the lower alkanol is continuously removed from the transesterification reaction; are described.
摘要翻译： 制备共轭脂肪酸甘油酯的方法，包括：（a）在碱性催化剂存在下，在100至160℃的温度下，使通式（I）的脂肪酸低级烷基酯异构化，形成共轭 脂肪酸低级烷基酯：<？in-line-formula description =“In-line formula”end =“lead”？> R 1 CO 2或I 2 ）<？in-line-formula description =“In-line formula”end =“tail”？>其中R 1 CO表示具有16至22个碳原子和至少两个碳原子的酰基 碳不饱和度和R 2表示具有1至4个碳原子的烷基; 和（b）用甘油酯交换共轭脂肪酸低级烷基酯以形成共轭脂肪酸甘油酯，其中形成对应于通式R 2 OH的低级链烷醇，其中R 2 如上所定义，低级烷醇从酯交换反应中连续除去; 被描述。
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公开(公告)号：US07179929B2
公开(公告)日：2007-02-20
申请号：US10513314
申请日：2003-04-25
IPC分类号： C07C51/00
CPC分类号： C11C3/14 , C07B2200/09 , C07C67/03 , C07C67/333 , C11C3/06 , C07C69/587
摘要： Processes for preparing conjugated fatty acid glycerides comprising: (a) isomerizing a fatty acid lower alkyl ester corresponding to the general formula (I) in the presence of a basic catalyst at a temperature of from 100 to 160° C., to form a conjugated fatty acid lower alkyl ester: R1CO—OR2 (I) wherein R1CO represents an acyl radical having from 16 to 22 carbon atoms and at least two carbon-carbon unsaturations and R2 represents an alkyl radical having from 1 to 4 carbon atoms; and (b) transesterifying the conjugated fatty acid lower alkyl ester with glycerol to form a conjugated fatty acid glyceride, wherein a lower alkanol corresponding to the general formula R2OH is formed, wherein R2 is as defined above, and the lower alkanol is continuously removed from the transesterification reaction; are described.
摘要翻译： 制备共轭脂肪酸甘油酯的方法，包括：（a）在碱性催化剂存在下，在100至160℃的温度下，使通式（I）的脂肪酸低级烷基酯异构化，形成共轭 脂肪酸低级烷基酯：<？in-line-formula description =“In-line formula”end =“lead”？> R 1 CO 2或I 2 ）<？in-line-formula description =“In-line formula”end =“tail”？>其中R 1 CO表示具有16至22个碳原子和至少两个碳原子的酰基 碳不饱和度和R 2表示具有1至4个碳原子的烷基; 和（b）用甘油酯交换共轭脂肪酸低级烷基酯以形成共轭脂肪酸甘油酯，其中形成对应于通式R 2 OH的低级链烷醇，其中R 2 如上所定义，低级烷醇从酯交换反应中连续除去; 被描述。
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公开(公告)号：US20060189817A1
公开(公告)日：2006-08-24
申请号：US10538383
申请日：2003-12-09
IPC分类号： C07C51/347
CPC分类号： C11C3/14 , C07C51/09 , C07C51/353 , C07C51/43 , C07C57/12
摘要： The present invention relates to a process for the production of conjugated linoleic acid, in which (a) linoleic acid lower alkyl esters containing 1 to 5 carbon atoms in a linear or branched alkyl chain are isomerized in the presence of alkali metal alcoholates, (b) the then conjugated linoleic acids are released from the ester after saponification, and (c) the free linoleic acids are subjected to crystallization. The crystallization step of said method provides a cost-effective option for producing conjugated linoleic acids with a high purity and excellent storage stability, in particular in low temperatures.
摘要翻译： 本发明涉及生产共轭亚油酸的方法，其中（a）在直链或支链烷基链中含有1至5个碳原子的亚油酸低级烷基酯在碱金属醇化物存在下异构化，（b ）然后皂化后从酯中释放出共轭亚油酸，（c）游离亚油酸进行结晶。 所述方法的结晶步骤提供了用于生产具有高纯度和优异的储存稳定性的共轭亚油酸的成本有效的选择，特别是在低温下。
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4.发明申请公开(公告)号：US20080254184A1
公开(公告)日：2008-10-16
申请号：US11857496
申请日：2007-09-19
申请人： Peter Horlacher , Robert Salacz , Alois Hofmann , Juergen Gierke
发明人： Peter Horlacher , Robert Salacz , Alois Hofmann , Juergen Gierke
CPC分类号： A23D9/00 , A23D7/0053 , A23D9/007 , A23D9/013 , A23D9/05 , A23L2/52 , A23L33/105 , A23L33/115 , A23L33/12 , A23V2002/00 , A23V2250/1882 , A23V2250/5028
摘要： A powder containing particles, which particles include gum arabic and at least one polyunsaturated fatty acid (PUFA) ester, where the ratio by weight of the quantity of gum arabic present in the particles to the quantity of the polyunsaturated fatty acid ester present in the particles is from about 1:1.4 to about 1:0.25, is provided. A process for the production of the particles is also provided.
摘要翻译： 含有颗粒的粉末，该颗粒包括阿拉伯树胶和至少一种多不饱和脂肪酸（PUFA）酯，其中颗粒中存在的阿拉伯树胶量与颗粒中存在的多不饱和脂肪酸酯的量的重量比 为约1：1.4至约1：0.25。 还提供了生产颗粒的方法。
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公开(公告)号：US20060057187A1
公开(公告)日：2006-03-16
申请号：US11215709
申请日：2005-08-30
申请人： Rainer Eskuchen , Juergen Gierke , Peter Horlacher
发明人： Rainer Eskuchen , Juergen Gierke , Peter Horlacher
CPC分类号： A23C9/1528 , A23D7/0053 , A23D7/011 , A23D7/04 , A23L33/12 , A23V2002/00 , A23V2250/1866 , A23V2200/222 , A23V2250/64 , A23V2250/1842
摘要： The disclosed invention relates to emulsions containing, based on the total weight of the emulsion, a) 0.1 to 50% by weight of a conjugated linoleic acid or derivative thereof, b) 0.1 to 30% by weight of a vegetable lecithin mixture, c) 0 to 20% by weight of a co-emulsifier, d) 0 to 70% by weight of a polyol, e) 0 to 70% by weight of a carbohydrate, f) 0 to 1% by weight of an antioxidant, and g) 20 to 99% by weight of an aqueous phase, with the proviso that the emulsion contains no other oils and fats except for the triglycerides of components a), b) and/or c) optionally present. The emulsions may be directly processed in foods, more particularly beverages, and show high stability in storage.
摘要翻译： 所公开的发明涉及基于乳液总重量的乳液，a）0.1至50重量％的共轭亚油酸或其衍生物，b）0.1至30重量％的植物卵磷脂混合物，c） 0〜20重量％的助乳化剂，d）0〜70重量％的多元醇，e）0〜70重量％的碳水化合物，f）0〜1重量％的抗氧化剂，g ）20至99重量％的水相，条件是除了任选存在的组分a），b）和/或c）的甘油三酸酯之外，乳液不含其它油和脂肪。 乳剂可以直接在食品，特别是饮料中加工，并且在储存中表现出高的稳定性。
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公开(公告)号：US09144545B2
公开(公告)日：2015-09-29
申请号：US12064651
申请日：2006-08-12
CPC分类号： A61K9/1658 , A23L33/11 , A23L33/17 , A23L33/19 , A61K9/1623
摘要： Compositions in powder form of sterols or stanol esters, and milk powder and/or proteins are disclosed. A process of making the compositions is also disclosed. The suitability of incorporation of the compositions in powder form in food products, for example beverages and milk products, is also disclosed.
摘要翻译： 公开了甾醇或甾烷醇酯的粉末形式的组合物，以及奶粉和/或蛋白质。 还公开了制备组合物的方法。 还公开了将组合物以粉末形式并入食品，例如饮料和奶制品的适用性。
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公开(公告)号：US20100055190A1
公开(公告)日：2010-03-04
申请号：US12282171
申请日：2007-02-27
CPC分类号： A23D7/0056 , A23D7/013 , A23L33/11 , C07J9/005
摘要： The invention relates to a powder formulation containing sterol in the form of a super-cooled melt from sterols and sterol esters, provided that the sterol ester content is at least 30 wt % in relation to the content of the powder. The introduced sterol ester is a fatty acid ester having a chain length of 2 to 24, preferably 8 to 12 carbon atoms. As the sterol preparations are wettable and melt easily without the use of complex equipment, they can easily be incorporated into food, and produce, in particular, good organoleptic and sensory properties, in particular, in drinks.
摘要翻译： 本发明涉及一种粉末制剂，其含有来自甾醇和甾醇酯的过冷却熔体形式的固醇，条件是相对于粉末含量，甾醇酯含量至少为30重量％。 引入的甾醇酯是链长为2至24，优选8至12个碳原子的脂肪酸酯。 由于甾醇制剂在不使用复杂设备的情况下易于润湿和熔化，因此它们可以容易地并入食物中，特别是特别是在饮料中产生良好的感官和感官特性。
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公开(公告)号：US20090099146A1
公开(公告)日：2009-04-16
申请号：US12282172
申请日：2007-02-27
CPC分类号： A23C9/1315 , A23C9/1528 , A23D7/011 , A23D7/013 , A23D9/013 , A23L33/11 , A23L33/12 , C07J9/005 , C11C3/003
摘要： The invention relates to sterol fatty acid esters of average chained fatty acids, having a chain length of 8 and 10 carbon atoms in a fatty acid distribution C8 to C10 (weight ratio) from 95:5 to 5:95, preferably, fatty acid distributions of C8 to C10 (weight ratio) from 90:10 to 20:80 and in particular, distributions of the fatty acids C8 to C10 (weight ratio) from 64:36 to 50:50 or from 78:22 to 65:35, are used. Preferably, capric and/or caprylic acids are used as fatty acids. Said sterol compounds can be easily incorporated into food, in particular, into drinks and milk products based on their wettability and easy to melt properties at low temperatures without using complex equipment, and have good organolepetic and sensory properties, and improved stability in relation to commercial sterol esters having long-chained and unsaturated fatty acids.
摘要翻译： 本发明涉及脂肪酸分布C8〜C10（重量比）为95:5〜5:95的链长为8〜10个碳原子的平均链状脂肪酸的甾醇脂肪酸酯，优选为脂肪酸分布 C8〜C10（重量比）为90:10〜20:80，特别是脂肪酸C8〜C10（重量比）为64:36〜50:50或78:22〜65:35的分布， 被使用。 优选地，癸酸和/或辛酸用作脂肪酸。 所述甾醇化合物可以容易地结合到食品中，特别是基于它们的润湿性和在低温下容易熔融的性质而不使用复杂的设备，并且具有良好的有机物和感官特性以及改进的与商业相关的稳定性 具有长链和不饱和脂肪酸的甾醇酯。
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公开(公告)号：US20080187643A1
公开(公告)日：2008-08-07
申请号：US12064651
申请日：2006-08-12
CPC分类号： A61K9/1658 , A23L33/11 , A23L33/17 , A23L33/19 , A61K9/1623
摘要： Compositions in powder form of sterols or stanol esters, and milk powder and/or proteins are disclosed. A process of making the compositions is also disclosed. The suitability of incorporation of the compositions in powder form in food products, for example beverages and milk products, is also disclosed.
摘要翻译： 公开了甾醇或甾烷醇酯的粉末形式的组合物，以及奶粉和/或蛋白质。 还公开了制备组合物的方法。 还公开了将组合物以粉末形式并入食品，例如饮料和奶制品的适用性。
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公开(公告)号：US20130331588A1
公开(公告)日：2013-12-12
申请号：US14000443
申请日：2012-03-03
申请人： Dieter Hietsch , Peter Horlacher
发明人： Dieter Hietsch , Peter Horlacher
IPC分类号： C07C67/54 , C07C69/587
CPC分类号： C07C67/54 , C07C67/60 , C07C69/587 , C11C1/10 , C11C3/003
摘要： The present invention relates to a method for working up a mixture which contains esters of EPA and/or DHA with monohydric alcohols having 1 to 6 carbon atoms, esters of other fatty acids with monohydric alcohols having 1 to 6 carbon atoms, and free cholesterol, wherein the method comprises adding a transesterification catalyst to the mixture, converting at least some of the free cholesterol into esterified cholesterol and thereafter distilling the mixture, wherein the distillation is carried out in such a manner that a product is obtained which contains EPA and/or DHA, both in the form of esters thereof with monohydric alcohols having 1 to 6 carbon atoms, in a higher relative amount, based on all fatty acids in free or bound form present in the product, than said mixture. In addition, the present invention relates to a product which is obtainable by the method according to the invention, wherein the product contains 10 to 99.99% by weight of esters of EPA and/or of DHA with monohydric alcohols having 1 to 6 carbon atoms and 0.0001 to a maximum of 0.3% by weight of cholesterol in free or bound form.
摘要翻译： 本发明涉及一种用于处理含有EPA和/或DHA的酯与具有1至6个碳原子的一元醇的混合物的混合物的方法，其它脂肪酸与具有1至6个碳原子的一元醇的酯和游离胆固醇， 其中所述方法包括向所述混合物中加入酯交换催化剂，将至少一些游离胆固醇转化为酯化胆固醇，然后蒸馏混合物，其中蒸馏是以获得含有EPA和/或 DHA，以其与具有1至6个碳原子的一元醇的酯的形式，以相对于所述混合物中存在的游离或结合形式的所有脂肪酸的相对量较高。 另外本发明涉及通过本发明的方法获得的产品，其中该产品含有10至99.99重量％的EPA和/或DHA的酯与具有1至6个碳原子的一元醇的酯和 0.0001至最大0.3重量％的游离或结合形式的胆固醇。
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