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公开(公告)号:US20220278355A1
公开(公告)日:2022-09-01
申请号:US17625996
申请日:2020-07-29
Applicant: RHODIA OPERATIONS
Inventor: Réka TOTH , Laure BERTRY , Valérie BUISSETTE , Thierry LE MERCIER , Marc-David BRAIDA , Robin AMISSE
IPC: H01M10/056 , C01G25/00 , C01G33/00 , C01G49/00 , H01M10/0525
Abstract: The present invention relates to a method of preparation of a garnet-type inorganic material. It also relates to the garnet-type inorganic material itself. The process comprises the following steps: (1) bringing an aqueous solution S comprising (i) a salt of zirconium, (ii) a salt of lanthanum and (iii) a salt of the element A or a precursor of an oxide of element A into contact with an aqueous solution of a basic compound, as a result of which a precipitate suspended in the reaction medium is obtained; (2) stirring the reaction medium obtained at the end of step (1) for at least 30 min; (3) bringing the precipitate obtained at the end of step (2) into contact with an additive selected in the group consisting of: anionic surfactants; nonionic surfactants; polyethylene glycols; carboxylic acids and their salts; and surfactants of the carboxymethylated fatty alcohol ethoxylate type; (4) calcining in air the precipitate recovered at the end of the previous step at a temperature which is at least 400° C.; (5) bringing into contact the product obtained at the end of step (4) with a salt of lithium; (6) calcining in air the product obtained at the end of step (5) at a temperature between 700° C. and 1100° C.; 20 the inorganic compound M comprising or consisting essentially of a garnet oxide or garnet-type oxide containing, as constituent elements, the elements Li, La, Zr and at least one element A selected in the group consisting of Al, Ga, Nb, Fe, W, Ta, or a mixture thereof.
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公开(公告)号:US20210070630A1
公开(公告)日:2021-03-11
申请号:US17049658
申请日:2019-04-25
Inventor: Jean-Marie TARASCON , Jiwei MA , Laure BERTRY , Robin AMISSE , Marc-David BRAIDA , Thierry LE MERCIER , Valérie BUISSETTE
Abstract: The present invention relates to the new process of preparation of a Li-rich layered oxide based on Mn and optionally on Ni and/or Co in which F is incorporated within the crystal of the oxide (or “fluorinated oxide”). It also relates to the new fluorinated oxide its use as a component in a cathode of a battery.
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公开(公告)号:US20210024755A1
公开(公告)日:2021-01-28
申请号:US17043741
申请日:2019-04-11
Applicant: RHODIA OPERATIONS
Inventor: Cédric FERAL-MARTIN , Laure BERTRY , Emmanuelle ALLAIN NAJMAN
Abstract: A precipitated silica suitable for thermal insulation applications and a process for its manufacture.
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公开(公告)号:US20220306480A1
公开(公告)日:2022-09-29
申请号:US17618904
申请日:2020-06-23
Applicant: RHODIA OPERATIONS
Inventor: Pascaline GARBEY , Frédéric COLBEAU-JUSTIN , Laure BERTRY
IPC: C01B33/193
Abstract: A chemically modified precipitated silica characterised by the presence of methyl moieties chemically bound to the silica and a process for its manufacture.
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公开(公告)号:US20210305549A1
公开(公告)日:2021-09-30
申请号:US17263819
申请日:2019-07-30
Applicant: RHODIA OPERATIONS
Inventor: Laure BERTRY , Robin AMISSE , Valérie BUISSETTE , Marc-David BRAIDA , Stéphanie LESTURGEZ , Thierry LE MERCIER
IPC: H01M4/36 , C01B25/455 , H01M4/58 , H01M4/587 , H01M4/62 , H01M10/054
Abstract: The invention relates to an NVPF-based composition and the use thereof in the field of batteries as an electrochemically active material. The invention also relates to a conductive composition comprising said composition as well as to a method for obtaining said composition.
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