PROCESS FOR PRODUCING CELLULOSE DERIVATIVES OF HIGH BULK DENSITY AND GOOD FLOWABILITY
    2.
    发明申请
    PROCESS FOR PRODUCING CELLULOSE DERIVATIVES OF HIGH BULK DENSITY AND GOOD FLOWABILITY 有权
    用于生产高密度密度和良好流动性的纤维素衍生物的方法

    公开(公告)号:US20140017319A1

    公开(公告)日:2014-01-16

    申请号:US14009432

    申请日:2012-03-29

    IPC分类号: A61K9/14

    摘要: A particulate cellulose derivative is obtained in a process of grinding and drying a moist cellulose derivative which comprises the steps of A) providing a cellulose derivative having a moisture content of from 60 to 95 percent, based on the total weight of the moist cellulose derivative, B) grinding and partially drying the moist cellulose derivative in a gas-swept impact mill; and C) contacting the ground and partially dried cellulose derivative with an additional amount of a drying gas outside the gas-swept impact mill. The obtained particulate cellulose derivative has a high untapped bulk density and a good flowability.

    摘要翻译: 在研磨和干燥湿纤维素衍生物的方法中获得颗粒状纤维素衍生物,其包括以下步骤:A)提供基于湿纤维素衍生物的总重量的水分含量为60至95%的纤维素衍生物, B)在气体扫掠冲击式研磨机中研磨和部分干燥湿纤维素衍生物; 和C)将接地和部分干燥的纤维素衍生物与气体扫掠冲击式磨机外部的附加量的干燥气体接触。 得到的颗粒状纤维素衍生物的未开发堆积密度高,流动性良好。

    PROCESS FOR DRY-GRINDING A POLYSACCHARIDE DERIVATIVE
    3.
    发明申请
    PROCESS FOR DRY-GRINDING A POLYSACCHARIDE DERIVATIVE 有权
    用于干燥多糖衍生物的方法

    公开(公告)号:US20120187225A1

    公开(公告)日:2012-07-26

    申请号:US13391337

    申请日:2010-08-31

    IPC分类号: C08J3/12 B02C23/18 B02C23/06

    CPC分类号: C08J3/12 C08J2301/00

    摘要: In a process for producing a particulate polysaccharide derivative by dry-grinding a moist polysaccharide derivative the median length of the particles after dry-grinding is controlled by controlling the moisture content of the polysaccharide derivative prior to dry-grinding. Advantageously the median length of the particles after dry-grinding is adjusted to a first value by a first moisture content of the polysaccharide derivative prior to dry-grinding and is adjusted to a second value by a second moisture content.

    摘要翻译: 在通过干磨多湿衍生物制造颗粒状多糖衍生物的方法中,通过在干式研磨之前控制多糖衍生物的含水量来控制干磨后的颗粒的中值长度。 有利的是,干磨后的颗粒的中值长度在干磨之前通过多糖衍生物的第一含水量调节至第一值,并通过第二含水量调节至第二值。

    Process for reducing the amount of water-insoluble fibers in a water-soluble cellulose derivative
    5.
    发明授权
    Process for reducing the amount of water-insoluble fibers in a water-soluble cellulose derivative 有权
    用于减少水溶性纤维素衍生物中的水不溶性纤维的量的方法

    公开(公告)号:US09359450B2

    公开(公告)日:2016-06-07

    申请号:US14009430

    申请日:2012-03-29

    IPC分类号: C08B11/20

    CPC分类号: C08B11/20

    摘要: The amount of water-insoluble fibers in a water-soluble cellulose derivative is reduced in a process comprising the steps of a) providing a water-soluble cellulose derivative having a residual amount of at least 20 ppm by weight of water-insoluble fibers in a 2 weight percent aqueous solution of the water-soluble cellulose derivative; b) mixing the water-soluble cellulose derivative of step a) with a liquid in a compounder to provide a moist water-soluble cellulose derivative having a temperature of at least 50 C and a moisture content of from 35 to 90 percent, based on the total weight of the moist cellulose derivative; and c) drying-grinding the mixture of step b) in a gas-swept impact mill to obtain a dried and ground cellulose derivative.

    摘要翻译: 在水溶性纤维素衍生物中的水不溶性纤维的量减少,包括以下步骤:a)提供在水溶性纤维素衍生物中提供残留量为至少20重量ppm的水不溶性纤维的水溶性纤维素衍生物 2重量%的水溶性纤维素衍生物的水溶液; b)将步骤a)的水溶性纤维素衍生物与混合器中的液体混合,以提供温度至少为50℃,水分含量为35至90%的湿水溶性纤维素衍生物,基于 湿纤维素衍生物的总重量; 和c)在气体扫掠冲击式研磨机中将步骤b)的混合物干燥研磨,得到干燥和研磨的纤维素衍生物。

    Process for dry-grinding a polysaccharide derivative
    6.
    发明授权
    Process for dry-grinding a polysaccharide derivative 有权
    干磨多糖衍生物的方法

    公开(公告)号:US08973853B2

    公开(公告)日:2015-03-10

    申请号:US13498621

    申请日:2010-07-28

    摘要: In a process for producing a particulate polysaccharide derivative by dry-grinding a moist polysaccharide derivative, one or more of the properties selected from median diameter, median length, bulk density and dissolution rate is controlled by controlling the temperature of the polysaccharide derivative prior to dry-grinding. Advantageously one or more of the properties selected from median diameter, median length, bulk density and dissolution rate of the particles after dry-grinding is adjusted to a first value by a first temperature of the polysaccharide derivative prior to dry-grinding and is adjusted to a second value by a second temperature.

    摘要翻译: 在通过干磨多湿衍生物制造颗粒状多糖衍生物的方法中,通过在干燥前控制多糖衍生物的温度来控制选自中值粒径,中值长度,体积密度和溶出速度的一种或多种性质 研磨。 有利的是,干磨后颗粒的中值粒径,中值长度,体积密度和溶解速度中的一种或多种性质在干磨前被多糖衍生物的第一温度调节至第一值,并调节至 第二值为第二温度。

    Process for dry-grinding a polysaccharide derivative
    7.
    发明授权
    Process for dry-grinding a polysaccharide derivative 有权
    干磨多糖衍生物的方法

    公开(公告)号:US08727246B2

    公开(公告)日:2014-05-20

    申请号:US13391337

    申请日:2010-08-31

    IPC分类号: B02C11/08

    CPC分类号: C08J3/12 C08J2301/00

    摘要: In a process for producing a particulate polysaccharide derivative by dry-grinding a moist polysaccharide derivative the median length of the particles after dry-grinding is controlled by controlling the moisture content of the polysaccharide derivative prior to dry-grinding. Advantageously the median length of the particles after dry-grinding is adjusted to a first value by a first moisture content of the polysaccharide derivative prior to dry-grinding and is adjusted to a second value by a second moisture content.

    摘要翻译: 在通过干磨多湿衍生物制造颗粒状多糖衍生物的方法中,通过在干式研磨之前控制多糖衍生物的含水量来控制干磨后的颗粒的中值长度。 有利的是,干磨后的颗粒的中值长度在干磨之前通过多糖衍生物的第一含水量调节至第一值,并通过第二含水量调节至第二值。

    Purification of aqueous reaction or washing medium containing cellulose
ethers
    8.
    发明授权
    Purification of aqueous reaction or washing medium containing cellulose ethers 失效
    含有纤维素醚的水性反应或洗涤介质的纯化

    公开(公告)号:US5482634A

    公开(公告)日:1996-01-09

    申请号:US259319

    申请日:1994-06-13

    CPC分类号: C08B11/22 C08B11/20

    摘要: In a process for purifying an aqueous liquid reaction and/or washing medium containing i) hot water-insoluble cellulose ethers and ii) hot water-soluble cellulose ethers and/or macromolecular cellulose ether by-products, in a purification step a) the aqueous medium has a temperature above the gel point of the hot water-insoluble cellulose ether and gelled cellulose ether is separated from the aqueous medium by means of a solid-bowl centrifuge or a plate separator and in a purification step b) the remaining aqueous liquor is treated by ultrafiltration at a concentration ratio of at least 40.

    摘要翻译: 在纯化含水液体反应和/或洗涤介质的方法中,其包含i)热水不溶性纤维素醚和ii)热水溶性纤维素醚和/或大分子纤维素醚副产物,在纯化步骤a)水性 介质的温度高于热水不溶性纤维素醚的凝胶点,并且凝胶状纤维素醚通过固体碗式离心机或平板分离器从水性介质中分离出来,并且在纯化步骤中b)剩余的含水液体为 以浓度比至少为40的超滤处理。

    PROCESS FOR DRY-GRINDING A POLYSACCHARIDE DERIVATIVE
    10.
    发明申请
    PROCESS FOR DRY-GRINDING A POLYSACCHARIDE DERIVATIVE 有权
    用于干燥多糖衍生物的方法

    公开(公告)号:US20130112787A1

    公开(公告)日:2013-05-09

    申请号:US13498621

    申请日:2010-07-28

    IPC分类号: B02C19/18 B02C23/24

    摘要: In a process for producing a particulate polysaccharide derivative by dry-grinding a moist polysaccharide derivative, one or more of the properties selected from median diameter, median length, bulk density and dissolution rate is controlled by controlling the temperature of the polysaccharide derivative prior to thy-grinding. Advantageously one or more of the properties selected from median diameter, median length, bulk density and dissolution rate of the particles after thy-grinding is adjusted to a first value by a first temperature of the polysaccharide derivative prior to thy-grinding and is adjusted to a second value by a second temperature.

    摘要翻译: 在通过干式研磨湿多糖衍生物制备颗粒状多糖衍生物的方法中,通过控制多糖衍生物在您之前的温度来控制从中值粒径,中值长度,体积密度和溶解速率中选择的一种或多种性质 研磨。 有利的是,一个或多个选自中值粒径,中值长度,体积密度和磨细后的颗粒的溶解速度的性质在碾磨之前通过多糖衍生物的第一温度调节至第一值,并调节至 第二值为第二温度。