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    System and process for cumene hydroperoxide cleavage with improved online instrumentation configuration
    4.
    发明授权
    System and process for cumene hydroperoxide cleavage with improved online instrumentation configuration 有权

    公开(公告)号：US10065171B2

    公开(公告)日：2018-09-04

    申请号：US15520559

    申请日：2015-10-22

    申请人： SABIC Global Technologies B.V.

    发明人： Mark Erik Nelson ,  James Patrick Williams

    IPC分类号： C07C45/53 ,  C07C37/08 ,  C07C407/00 ,  B01J19/00 ,  B01J19/24

    摘要： Disclosed herein are a method and systems for cumene hydroperoxide cleavage with an improved configuration for online instrumentation. The systems comprise a first fluid loop comprising one or more reactors and a fluid pump and a second fluid loop in fluid communication with the first fluid loop. This second fluid loop comprises an instrument configured to measure a characteristic of a fluid flowing through the second loop, wherein an input of the second fluid loop is disposed downstream of said fluid pump and an output of the second fluid loop is disposed upstream of said fluid pump. The method comprises causing fluid to flow within a first stage comprising one or more reactors and a fluid pump, wherein the first stage is configured to decompose a cumene hydroperoxide in the presence of a catalyst mixture to form a dicumyl peroxide mixture. The method also comprises causing at least a portion of the fluid to flow through a instrumentation line in open fluid communication with the first stage. This instrumentation line comprises an instrument configured to measure a characteristic of the fluid flowing through the instrumentation line and an input of the instrument line is disposed downstream of said fluid pump.

    OPTICAL ANALYSIS AND SAMPLING SYSTEMS
    7.
    发明申请
    OPTICAL ANALYSIS AND SAMPLING SYSTEMS 审中-公开

    公开(公告)号：US20200232912A1

    公开(公告)日：2020-07-23

    申请号：US16838220

    申请日：2020-04-02

    申请人： SABIC GLOBAL TECHNOLOGIES B.V.

    发明人： Mark Erik Nelson ,  Arkady Samuilovich Dykman ,  Andrey Vladimirovich Zinenkov

    IPC分类号： G01N21/27 ,  G01N1/10 ,  G01N21/05 ,  G01N21/359 ,  G01N21/17 ,  G01N1/14 ,  G01N21/75 ,  G01N1/38

    摘要： A sampling system for an optical cell containing a process fluid comprises a first bi-directional pump in fluid communication with a sampling path and a second bi-directional pump in fluid communication with the first bi-directional pump and a storage vessel. The first bi-directional pump is configured to withdraw a first sample of the process fluid and to cause the first sample to flow towards the first bi-directional pump. The second bi-directional pump is configured to withdraw a second sample from the storage vessel and to cause the second sample to move toward and mix with the first sample. A first rate of withdraw of the first sample is greater than a second rate of movement of the second sample toward the first sample, and the difference between the first rate and the second rate correspond to a pre-determined ratio of the first sample mixed with the second sample.

    Optical analysis and sampling systems
    8.
    发明授权
    Optical analysis and sampling systems 有权

    公开(公告)号：US10648906B2

    公开(公告)日：2020-05-12

    申请号：US15524305

    申请日：2015-11-23

    申请人： SABIC GLOBAL TECHNOLOGIES B.V.

    发明人： Mark Erik Nelson ,  Arkady Samuilovich Dykman ,  Andrey Vladimirovich Zinenkov

    IPC分类号： G01N1/10 ,  G01N1/14 ,  G01N1/38 ,  G01N21/05 ,  G01N21/27 ,  G01N21/75 ,  G01N21/17 ,  G01N21/359

    摘要： In an embodiment, an optical system comprises an optical cell having an interior fluid chamber defined by an interior surface of a housing, a process inlet disposed in the housing and in fluid communication with the interior fluid chamber, and a process outlet disposed in the housing and in fluid communication with the interior fluid chamber, wherein the process inlet and process outlet facilitate the flow of a fluid through the interior fluid chamber. A sampling outlet can be disposed in the housing and in fluid communication with the interior fluid chamber. A first bi-directional pump can be in fluid communication with the sampling outlet and a first storage vessel and can be configured to withdraw a first sample of the fluid via the sampling outlet and to cause the first sample to flow into the first storage vessel.