公开(公告)号：US20170315025A1

公开(公告)日：2017-11-02

申请号：US15143702

申请日：2016-05-02

申请人： SHIMADZU CORPORATION

发明人： Akira AONO

IPC分类号： G01N1/22 ,  G01N30/32 ,  G01N30/02

摘要： A carrier gas flow path of at least from a trap to an analyzing portion is shared between a state wherein a sample component is trapped within the trap and a state wherein the sample component is not trapped within the trap. In this case, even after the sample has been introduced into the analyzing portion through the carrier gas flow path, there is a time interval over which the carrier gas flows within the carrier gas flow path. This makes it possible, through the carrier gas that flows within the carrier gas flow path afterward, to remove the sample component from within the flow path, despite there being a sample component within the carrier gas flow path at the time of sample introduction, thus making it possible to prevent the sample component from remaining within the flow path after sample introduction.

公开(公告)号：US20160252472A1

公开(公告)日：2016-09-01

申请号：US15032348

申请日：2013-12-02

申请人： SHIMADZU CORPORATION

发明人： Akira AONO

IPC分类号： G01N25/20

CPC分类号： G01N25/20 ,  G01N1/44 ,  G01N30/24 ,  G01N30/30 ,  G01N2030/3076

摘要： A heat retention start timing of each sample container is determined based on a room temperature detected by a room temperature sensor, and a starting temperature and an ending temperature of each sample at a time of programmed temperature analysis that are stored in an analysis condition storage section. Since cooling speed of each sample container varies depending on the room temperature, the cooling time (A12, B12, C12, . . . ) of each sample container may be predicted based on the ending temperature of each sample at the time of programmed temperature analysis, the starting temperature of a next sample at the time of the programmed temperature analysis, and the room temperature. By determining the heat retention start timing of each sample container according to the cooling time (A12, B12, C12, . . . ) of each sample container predicted in the above manner, a margin time (A13, B13, C13, . . . ) after the cooling time may be prevented from becoming unnecessarily long. Accordingly, the processing performance may be improved compared to a conventional configuration where the heat retention start timings of sample containers are shifted by fixed time intervals.

摘要翻译： 根据存储在分析条件存储部中的室温传感器检测到的室温，以及程序化温度分析时的各样品的起始温度和结束温度，确定各检体容器的保温开始时刻 。 由于每个样品容器的冷却速度根据室温而变化，因此可以根据程序温度分析时的每个样品的结束温度来预测每个样品容器的冷却时间（A12，B12，C12 ...） ，程序温度分析时的下一个样品的起始温度和室温。 通过根据以上述方式预测的每个样品容器的冷却时间（A12，B12，C12 ...）确定每个样品容器的保温开始时刻，余量时间（A13，B13，C13，...， ）可以防止冷却时间变得不必要地长。 因此，与采样容器的保温开始定时以固定时间间隔偏移的常规配置相比，可以提高处理性能。

公开(公告)号：US20150219532A1

公开(公告)日：2015-08-06

申请号：US14169733

申请日：2014-01-31

申请人： SHIMADZU CORPORATION

发明人： Akira AONO

IPC分类号： G01N1/22

CPC分类号： G01N1/2202 ,  G01N30/12 ,  G01N2001/2282 ,  G01N2030/025 ,  G01N2030/128

摘要： A sample introduction device having a channel configuration which allows recapture of samples and in which thorough purging is performed so that no sample components remain inside the channel. In the trap capture process, a first six-way switching valve is placed in state where ports a-f, b-c and d-e are connected, a second six-way switching valve is placed in state where ports a-b, c-d and e-f are connected, and an electromagnetic valve is opened. Carrier gas is introduced through a carrier gas channel, and is discharged via the first six-way valve-sample channel-second six-way switching valve-trap channel-second six-way switching valve-channel-first six-way valve-discharge channel. Carrier gas is also introduced through the path going through the electronic control flow controller, so the operation of stabilization of the analysis channel continues to be performed.

摘要翻译： 具有通道结构的样品引入装置，其允许重新捕获样品，并且进行彻底清洗，使得通道内不残留样品成分。 在陷阱捕获过程中，将第一六通切换阀置于端口af，bc和de连接的状态，在端口ab，cd和ef连接的状态下放置第二六通切换阀， 电磁阀打开。 载气通过载气通道引入，并通过第一六通阀样通道 - 第二六通切换阀 - 捕集通道 - 第二六通切换阀 - 通道 - 第一六通阀 - 排出 渠道。 载气也通过电子控制流量控制器的路径引入，因此继续执行分析通道的稳定运行。

公开(公告)号：US20230408460A1

公开(公告)日：2023-12-21

申请号：US18139109

申请日：2023-04-25

申请人： Shimadzu Corporation

发明人： Yoshitake YAMAMOTO ,  Akira AONO

IPC分类号： G01N30/32 ,  B01D53/02

CPC分类号： G01N30/32 ,  B01D53/025 ,  G01N2030/025

摘要： Provided is a sample container and a gas chromatograph capable of detecting the pressure in the flow path for supplying a pressurized gas into a flow path. The ample supply device includes and insertion tube, a pressurized gas supply unit, a valve, and a pressure sensor. The pressurized gas supply unit is connected to the insertion tube via the flow path. The valve opens and closes the flow path. The pressure sensor senses the pressure between the valve and the insertion tube in the flow path. In the sample supply device, the pressure in the flow path connecting the pressurized gas supply unit and the insertion tube is detected, based on the detection signal from the pressure sensor in a state in which the valve is closed, and the insertion tube is inserted into the space in the sample container, before supplying a pressurized gas by a pressurized gas supply unit.

公开(公告)号：US20210333246A1

公开(公告)日：2021-10-28

申请号：US16470392

申请日：2018-02-22

申请人： SHIMADZU CORPORATION

发明人： Isao SAWAMURA ,  Akira AONO

IPC分类号： G01N30/12

摘要： A sample introduction device 10 includes a tube holding section 21 and a sample removing mechanism 40. The sample removing mechanism 40 removes a sample 6 in a sample tube 2 held by the tube holding section 21. Thus, in the sample introduction device 10, the sample 6 in the sample tube 2 held by the tube holding section 21 can be automatically removed. As a result, the operator no longer needs to perform an operation of taking out the sample 6 from the sample tube 2. Thus, a work load on the operator can be reduced.

公开(公告)号：US20180356316A1

公开(公告)日：2018-12-13

申请号：US15778355

申请日：2015-12-15

申请人： SHIMADZU CORPORATION

发明人： Akira AONO ,  Isao SAWAMURA

IPC分类号： G01N1/22 ,  G01N30/16 ,  G01N30/54 ,  G01N30/46

CPC分类号： G01N1/2247 ,  G01N1/00 ,  G01N1/22 ,  G01N30/16 ,  G01N30/465 ,  G01N30/54 ,  G01N2030/128

摘要： A sample introduction device includes a tube holding unit 10, a tube heating unit 20, and a movement mechanism 30. The tube holding unit 10 holds a sample tube 1. The tube heating unit 20 comes into contact with the sample tube 1 held in the tube holding unit 10 and heats the sample tube 1 to desorb sample components in the sample tube 1. The tube holding unit 10 and the tube heating unit 20 are attached to the movement mechanism 30 so as to be able to move separately. The movement mechanism 30 includes a nut 32 which can be attached to and detached from the tube holding unit 10 and the tube heating unit 20, and a support shaft 31 which supports the nut 32 such that the nut 32 can move.

公开(公告)号：US20220326195A1

公开(公告)日：2022-10-13

申请号：US17641679

申请日：2020-11-18

申请人： SHIMADZU CORPORATION

发明人： Akira AONO ,  Shota HATA ,  Naru MARUOKA ,  Hideki SATO

IPC分类号： G01N30/20 ,  G01N30/88 ,  G01N30/26

摘要： A switching mechanism 110 can perform switching to a pressurized state in which gas is supplied from a pipe 203 to an insertion tube 101, or a derivation state in which gas in a head space 23 that is pressurized is derived from the insertion tube 101 to the pipe 207 via a collection unit 104. The switching mechanism 110 includes a discharge valve 103 that puts the insertion tube 101 and the pipe 207 into a non-communication state in the pressurized state and puts the insertion tube 101 and the pipe 207 into a communication state in the derivation state. A resistance pipe 206 supplies gas to a channel between the collection unit 104 and the discharge valve 103 in the derivation state.

公开(公告)号：US20190041367A1

公开(公告)日：2019-02-07

申请号：US16077068

申请日：2016-03-07

申请人： SHIMADZU CORPORATION

发明人： Akira AONO ,  Isao SAWAMURA

IPC分类号： G01N30/20 ,  G01N30/12 ,  G01N30/18

摘要： A sample introduction device 100 includes a heating unit 102, an ultraviolet irradiation unit 103, and a sample supply part 106. The heating unit 102 vaporizes a sample 22 by heating externally a container 2 in which the sample 22 is enclosed. The ultraviolet irradiation unit 103 causes ultraviolet rays to pass through the container 2 and irradiates the sample 22 with the ultraviolet rays. The sample supply part 106 supplies the sample vaporized in the container 2 to a gas chromatograph 1 side.

公开(公告)号：US20150047442A1

公开(公告)日：2015-02-19

申请号：US13966765

申请日：2013-08-14

申请人： SHIMADZU CORPORATION

发明人： Akira AONO

IPC分类号： G01N30/16

CPC分类号： G01N30/20 ,  G01N1/2214 ,  G01N2030/025 ,  G01N2030/085 ,  G01N2030/207

摘要： In a gas sample analysis device including a metering tube, sample gas supply channel, carrier gas supply channel, evacuation channel and collection tube, there is provided a first channel switching valve which switches between a load state in which the metering tube is interposed between said sample gas supply channel and the evacuation channel and an injection state in which the metering tube is interposed between the sample gas supply channel and gas analysis device; and a second channel switching valve which, in the load state or injection state, switches between a collection tube interposition state in which the collection tube is interposed between the sample gas supply channel and the metering tube or between the metering tube and the gas analysis device, and a collection tube shunt state in which the collection tube is not interposed.

摘要翻译： 在包括计量管，样品气体供给通道，载气供给通道，排气通道和收集管的气体样品分析装置中，设置有第一通道切换阀，其在计量管介于所述 样品气体供给通道和排气通道以及计量管插入在样品气体供给通道和气体分析装置之间的注入状态; 以及第二通道切换阀，所述第二流路切换阀在所述负荷状态或注入状态下，在收集管插入状态之间切换，在所述收集管插入状态中，所述收集管插入在所述样品气体供给流路和所述计量管之间，或者在所述计量管与所述气体分析装置 ，收集管未插入收集管分流状态。