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    PROCESS FOR THE ALKOXYLATION OF (PER) FLUOROPOLYETHER ALCOHOLS
    3.
    发明申请
    PROCESS FOR THE ALKOXYLATION OF (PER) FLUOROPOLYETHER ALCOHOLS 有权
    （PER）氟聚乙醇醇的烷基化方法

    公开(公告)号：US20150329453A1

    公开(公告)日：2015-11-19

    申请号：US14651542

    申请日：2013-12-04

    Applicant: SOLVAY SPECIALTY POLYMERS ITALY S.P.A.

    Inventor： Pier Antonio GUARDA ,  Gianfranco SPATARO

    IPC: C07C41/18

    CPC classification number: C07C41/18 ,  C08G65/007 ,  C08G65/2609 ,  C08G65/2654 ,  C08G65/2687 ,  C08G65/2696 ,  C08G65/328 ,  C08G65/331 ,  C08G2650/48

    Abstract: A convenient process for the manufacture of alkoxylated derivatives of PFPE alcohols is herein provided. The process envisages the use of a boron-based catalyst and an iodine source and is characterised in that a PFPE alkoxide is prepared separately, contacted with a boric acid triester of the same PFPE alcohol and finally submitted to alkoxylation in the presence of an iodine source. The process allows achieving an alkoxylation degree of at least 2 with high yields and under conditions that are convenient on an industrial scale.

    Abstract translation: 本文提供了制备PFPE醇的烷氧基化衍生物的方便方法。 该方法设想使用硼基催化剂和碘源，其特征在于分别制备PFPE醇盐，与相同PFPE醇的硼酸三酯接触，最后在碘源存在下进行烷氧基化 。 该方法允许以高产率和在工业规模上方便的条件下实现至少2的烷氧基化度。

    AROMATIC COMPOUNDS BEARING HYDROXYL-SUBSTITUTED (PER)FLUOROPOLYETHER CHAINS
    4.
    发明申请
    AROMATIC COMPOUNDS BEARING HYDROXYL-SUBSTITUTED (PER)FLUOROPOLYETHER CHAINS 审中-公开

    公开(公告)号：US20170081266A1

    公开(公告)日：2017-03-23

    申请号：US15311518

    申请日：2015-05-14

    Applicant: SOLVAY SPECIALTY POLYMERS ITALY S.P.A.

    Inventor： Roberto VALSECCHI ,  Pier Antonio GUARDA ,  Rosaldo PICOZZI

    IPC: C07C43/23 ,  C10M131/10 ,  G11B5/725 ,  C10M105/54

    Abstract: Compounds [compounds (L)] comprising at least one monocyclic, polycyclic or polycondensed aromatic moiety [moiety (A*)], wherein: at least one carbon atom of moiety (A*) is substituted with a fluoropolyoxyalkene chain [chain (Rf)], said chain (Rf) comprising: a) a fluorocarbon segment having ether linkages in the main chain and b) at least one hydroxyl group and wherein: at least one other carbon atom of moiety (A*) is substituted with an electron-withdrawing group and mixtures thereof are herein disclosed. Disclosed are also a process for manufacturing compounds (L), a method for lubricating MRM comprising using compounds (L), a lubricant composition comprising one or more compounds (L) and a method for manufacturing a composition (C).

    METHOD OF MANUFACTURING CYCLOPHOSPHAZENE DERIVATIVES
    7.
    发明申请
    METHOD OF MANUFACTURING CYCLOPHOSPHAZENE DERIVATIVES 有权
    制备环磷酰胺衍生物的方法

    公开(公告)号：US20160130289A1

    公开(公告)日：2016-05-12

    申请号：US14896048

    申请日：2014-06-03

    Applicant: SOLVAY SPECIALTY POLYMERS ITALY S.P.A.

    Inventor： Roberto VALSECCHI ,  Rosaldo PICOZZI ,  Pier Antonio GUARDA

    IPC: C07F9/6593 ,  C10M105/74

    CPC classification number: C07F9/65815 ,  C07F9/65812 ,  C07F9/65817 ,  C08G65/007 ,  C08G65/3356 ,  C08G65/337 ,  C10M105/74 ,  G11B5/725

    Abstract: A method of manufacturing cyclophosphazenes PFPE derivatives to be used in the lubrication of magnetic recording media is herein provided. The method comprises: a) a (per)fluoropolyether (PFPE) polyol [PFPE (Ppol)] comprising a fluoropolyoxyalkylene chain (Rf) having two chain ends, each chain end comprising at least one hydroxy group, and b) the corresponding alkoxide of perfluoropolyether (Ppol) [PFPE (Palk)] wherein the equivalent concentration of PFPE (Palk) in PFPE (Ppol) is lower than 30%, preferably ranging from 5% to 15%; 2) contacting mixture (M) with a perhalocyclophosphazene (CPhalo) to provide a mixture (M1) containing an equivalent ratio of PFPE (Palk)/(CPhalo) of at least 1; 3) allowing mixture (M1) to react until complete disappearance of P—Cl groups to provide a mixture (M2); 4) submitting mixture (M2) to hydrolysis to provide a mixture (M3); 5) optionally removing (Ppol) from mixture (M3) to provide a mixture (M4). A method of purifying mixture (M4) is also herein provided.

    Abstract translation: 本文提供了制造用于润滑磁记录介质的环磷腈PFPE衍生物的方法。 该方法包括：a）包含具有两个链端的氟聚氧化烯链（Rf）的（全）氟聚醚（PFPE）多元醇[PFPE（Ppol）]，每个链端包含至少一个羟基，和b）相应的醇盐 全氟聚醚（Ppol）[PFPE（Palk）]，其中PFPE（Ppol）中PFPE（Palk）的当量浓度低于30％，优选5％至15％; 2）使混合物（M）与全卤代环丙腈（CPhalo）接触，以提供含有至少1的PFPE（Palk）/（CPalO）的当量比的混合物（M1） 3）允许混合物（M1）反应直到P-Cl基团完全消失以提供混合物（M2）; 4）将混合物（M2）进行水解以提供混合物（M3）; 5）任选地从混合物（M3）中除去（Ppol）以提供混合物（M4）。 还提供了一种纯化混合物（M4）的方法。

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