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公开(公告)号：US09102804B2
公开(公告)日：2015-08-11
申请号：US13395912
申请日：2010-09-16
IPC分类号： C08J3/12 , C08J3/28 , C08J3/24 , C08F220/06 , C08F222/10
CPC分类号： C08J3/28 , C08F220/06 , C08F222/1006 , C08J3/122 , C08J3/245 , C08J2300/00
摘要： A method for producing a water-absorbing resin comprises circulation of the water-absorbing resin in a predetermined amount in a pulverization step before a surface cross-linking step. At least a part of a classified polymer is supplied again to the same or a different pulverization step before the surface cross-linking step, wherein the circulation pulverization ratio in the pulverization step, represented by the following equation, is 1.10 to 1.50: (Circulation pulverization ratio)=(total supply amount of the water-absorbing resin to the pulverization step)/(total discharge amount of the water-absorbing resin at the drying step) wherein (total supply amount of the water-absorbing resin to the pulverization step)=(total discharge amount of the water-absorbing resin at the drying step)+(amount of the classified polymer supplied again to the same or a different pulverization step).
摘要翻译： 吸水性树脂的制造方法包括在表面交联工序之前的粉碎工序中使规定量的吸水性树脂循环。 将分级聚合物的至少一部分再次供给到在表面交联步骤之前的相同或不同的粉碎步骤中，其中由下式表示的粉碎步骤中的循环粉碎比为1.10至1.50：（循环 粉碎比）=（粉碎步骤中的吸水性树脂的总供给量）/（干燥工序中的吸水性树脂的总排出量）（其中，对粉碎工序的吸水性树脂的总供给量 ）=（干燥步骤中的吸水性树脂的总排出量）+（再次供给到相同或不同的粉碎工序的分类聚合物的量）。
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公开(公告)号：US20120220745A1
公开(公告)日：2012-08-30
申请号：US13496440
申请日：2010-09-16
IPC分类号： C08F20/06
CPC分类号： C08J3/28 , C08F220/06 , C08F222/1006 , C08J3/122 , C08J3/245 , C08J2300/00
摘要： [PROBLEM]It is an object of the present invention to enhance and stabilize properties of a water-absorbing resin, for example, damage resistance or water-absorbing speed, by a simple and convenient method without requiring change of raw materials or expensive facility investment, in a large scale production method for the water-absorbing resin.[MEANS FOR SOLVING THE PROBLEM]It is solved by circulation of the water-absorbing resin in a predetermined amount or more in the pulverization step before the surface cross-linking step. That is, at least a part of the classified polymer is supplied again to the same or different pulverization step, before the surface cross-linking step, wherein circulation pulverization ratio in the pulverization step, represented by the following equation is larger than 1.50: (Circulation pulverization ratio)=(total supply amount of the water-absorbing resin to the pulverization step)/(total discharge amount of the water-absorbing resin at the drying step) (wherein total supply amount of the water-absorbing resin to the pulverization step)=(total discharge amount of the water-absorbing resin at the drying step)+(amount of the classified polymer supplied again to the same or different pulverization step)).
摘要翻译： 本发明的目的是通过简单方便的方法来增强和稳定吸水树脂的性能，例如耐损伤性或吸水速度，而不需要改变原料或昂贵的设备投资 在大量的吸水树脂的制造方法中。 解决问题的手段通过在表面交联工序之前的粉碎工序中使吸水性树脂循环一定量以上来解决。 也就是说，在表面交联步骤之前，将分类的聚合物的至少一部分再次供给到相同或不同的粉碎步骤，其中由下式表示的粉碎步骤中的循环粉碎比大于1.50：（ 循环粉碎比）=（粉碎步骤中的吸水性树脂的总供给量）/（干燥工序中的吸水性树脂的总排出量）（其中，吸水性树脂与粉碎的总供给量 步骤）=（干燥步骤中的吸水性树脂的总排出量）+（再次供给相同或不同的粉碎步骤的分类聚合物的量））。
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3.发明授权Method for producing water absorbent polyacrylic acid (salt) resin powder, and water absorbent polyacrylic acid (salt) resin powder 有权吸水性聚丙烯酸（盐）树脂粉末和吸水性聚丙烯酸（盐）树脂粉末的制造方法公开(公告)号：US09447203B2
公开(公告)日：2016-09-20
申请号：US13639082
申请日：2011-04-07
申请人： Sayaka Machida , Kazushi Torii , Yoko Shirai , Hiroyuki Ikeuchi , Shigeru Sakamoto , Koji Tachi , Reiko Nakatsuru
发明人： Sayaka Machida , Kazushi Torii , Yoko Shirai , Hiroyuki Ikeuchi , Shigeru Sakamoto , Koji Tachi , Reiko Nakatsuru
IPC分类号： B01J20/26 , C08F6/00 , C08F220/06 , C08J3/24 , B29B9/06 , B29C47/00 , B29C47/38 , C08F222/10 , B29C47/30 , B29C47/66 , B29C47/92 , B29B9/16
CPC分类号： B01J20/267 , B01J20/28004 , B01J20/28016 , B01J20/3007 , B01J20/3021 , B01J20/3078 , B01J20/3085 , B29B9/06 , B29B2009/161 , B29C47/0011 , B29C47/30 , B29C47/385 , B29C47/667 , B29C47/92 , B29C2947/9259 , B29C2947/92704 , C08F6/008 , C08F220/06 , C08F220/20 , C08F222/1006 , C08J3/245 , C08J2333/02 , Y10T428/2982 , C08L33/02
摘要： An object of the present invention is to provide a method for producing water absorbent resin powder in which permeability potential (SFC) is improved while a water absorbing rate (FSR) is being kept. The method is a method for producing water absorbent polyacrylic acid (salt) resin powder including the steps of: (i) polymerizing an acrylic acid (salt) monomer aqueous solution; (ii) during or after the step of (i), performing gel grinding of a hydrogel crosslinked polymer obtained by the polymerization, wherein the hydrogel crosslinked polymer has resin solid content of 10 wt % to 80 wt %, and the gel grinding is carried out with gel grinding energy (GGE) of 18 [J/g] to 60 [J/g]; (iii) drying a particulate hydrogel crosslinked polymer obtained by the gel grinding, wherein the drying is performed at 150° C. to 250° C.; and (iv) carrying out a surface treatment to the particulate hydrogel crosslinked polymer thus dried.
摘要翻译： 本发明的目的是提供一种吸水性树脂粉末的制造方法，其中在保持吸水率（FSR）的同时提高渗透率（SFC）。 该方法是生产吸水性聚丙烯酸（盐）树脂粉末的方法，包括以下步骤：（i）使丙烯酸（盐）单体水溶液聚合; （ii）在（i）的步骤期间或之后，进行通过聚合获得的水凝胶交联聚合物的凝胶研磨，其中所述水凝胶交联聚合物的树脂固含量为10重量％至80重量％，并且进行凝胶研磨 （GGE）为18 [J / g]至60 [J / g]; （iii）干燥通过凝胶研磨获得的颗粒状水凝胶交联聚合物，其中干燥在150℃至250℃下进行; 和（iv）对由此干燥的颗粒状水凝胶交联聚合物进行表面处理。
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公开(公告)号：US08513378B2
公开(公告)日：2013-08-20
申请号：US13496440
申请日：2010-09-16
CPC分类号： C08J3/28 , C08F220/06 , C08F222/1006 , C08J3/122 , C08J3/245 , C08J2300/00
摘要： The present invention provides a method for producing a water-absorbing resin powder. The method includes a polymerization step, a drying step, a pulverization step, a classification step, and a surface cross-linking step. It further includes an additional step, performed before the surface cross-linking step, in which at least part of the classified polymer is supplied again to the same or a different pulverization step. The circulation pulverization ratio in the pulverization step is higher than 1.50.
摘要翻译： 本发明提供一种吸水性树脂粉末的制造方法。 该方法包括聚合步骤，干燥步骤，粉碎步骤，分级步骤和表面交联步骤。 其还包括在表面交联步骤之前进行的另外的步骤，其中将至少部分分类的聚合物再次供应到相同或不同的粉碎步骤。 粉碎步骤中的循环粉碎比高于1.50。
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5.发明申请METHOD FOR PRODUCING WATER ABSORBENT POLYACRYLIC ACID (SALT) RESIN POWDER, AND WATER ABSORBENT POLYACRYLIC ACID (SALT) RESIN POWDER 有权生产水吸收聚丙烯酸（盐）树脂粉的方法和水吸收聚丙烯酸（盐）树脂粉公开(公告)号：US20130026412A1
公开(公告)日：2013-01-31
申请号：US13639082
申请日：2011-04-07
申请人： Sayaka Machida , Kazushi Torii , Yoko Shirai , Hiroyuki Ikeuchi , Shigeru Sakamoto , Koji Tachi , Reiko Nakatsuru
发明人： Sayaka Machida , Kazushi Torii , Yoko Shirai , Hiroyuki Ikeuchi , Shigeru Sakamoto , Koji Tachi , Reiko Nakatsuru
IPC分类号： B01J20/26 , C08F222/20
CPC分类号： B01J20/267 , B01J20/28004 , B01J20/28016 , B01J20/3007 , B01J20/3021 , B01J20/3078 , B01J20/3085 , B29B9/06 , B29B2009/161 , B29C47/0011 , B29C47/30 , B29C47/385 , B29C47/667 , B29C47/92 , B29C2947/9259 , B29C2947/92704 , C08F6/008 , C08F220/06 , C08F220/20 , C08F222/1006 , C08J3/245 , C08J2333/02 , Y10T428/2982 , C08L33/02
摘要： An object of the present invention is to provide a method for producing water absorbent resin powder in which permeability potential (SFC) is improved while a water absorbing rate (FSR) is being kept. The method is a method for producing water absorbent polyacrylic acid (salt) resin powder including the steps of: (i) polymerizing an acrylic acid (salt) monomer aqueous solution; (ii) during or after the step of (i), performing gel grinding of a hydrogel crosslinked polymer obtained by the polymerization, wherein the hydrogel crosslinked polymer has resin solid content of 10 wt % to 80 wt %, and the gel grinding is carried out with gel grinding energy (GGE) of 18 [J/g] to 60 [J/g]; (iii) drying a particulate hydrogel crosslinked polymer obtained by the gel grinding, wherein the drying is performed at 150° C. to 250° C.; and (iv) carrying out a surface treatment to the particulate hydrogel crosslinked polymer thus dried.
摘要翻译： 本发明的目的是提供一种吸水性树脂粉末的制造方法，其中在保持吸水率（FSR）的同时提高渗透率（SFC）。 该方法是生产吸水性聚丙烯酸（盐）树脂粉末的方法，包括以下步骤：（i）使丙烯酸（盐）单体水溶液聚合; （ii）在（i）的步骤期间或之后，进行通过聚合获得的水凝胶交联聚合物的凝胶研磨，其中所述水凝胶交联聚合物的树脂固含量为10重量％至80重量％，并且进行凝胶研磨 （GGE）为18 [J / g]至60 [J / g]; （iii）干燥通过凝胶研磨获得的颗粒状水凝胶交联聚合物，其中干燥在150℃至250℃下进行; 和（iv）对由此干燥的颗粒状水凝胶交联聚合物进行表面处理。
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公开(公告)号：US20120220733A1
公开(公告)日：2012-08-30
申请号：US13395912
申请日：2010-09-16
IPC分类号： C08F120/06 , C08F2/10 , C08F6/12
CPC分类号： C08J3/28 , C08F220/06 , C08F222/1006 , C08J3/122 , C08J3/245 , C08J2300/00
摘要： [PROBLEM]It is an object of the present invention to enhance and stabilize properties of a water-absorbing resin, for example, damage resistance or water-absorbing speed, by a simple and convenient method without requiring change of raw materials or expensive facility investment, in a large scale production method for the water-absorbing resin.[MEANS FOR SOLVING THE PROBLEM]It is solved by circulation of the water-absorbing resin in a predetermined amount or more in the pulverization step before the surface cross-linking step. That is, at least a part of the classified polymer is supplied again to the same or different pulverization step, before the surface cross-linking step, wherein circulation pulverization ratio in the pulverization step, represented by the following equation is 1.10 to 1.50: (Circulation pulverization ratio)=(total supply amount of the water-absorbing resin to the pulverization step)/(total discharge amount of the water-absorbing resin at the drying step) (wherein total supply amount of the water-absorbing resin to the pulverization step)=(total discharge amount of the water-absorbing resin at the drying step)+(amount of the classified polymer supplied again to the same or different pulverization step)).
摘要翻译： 本发明的目的是通过简单方便的方法来增强和稳定吸水树脂的性能，例如耐损伤性或吸水速度，而不需要改变原料或昂贵的设备投资 在大量的吸水树脂的制造方法中。 解决问题的手段通过在表面交联工序之前的粉碎工序中使吸水性树脂循环一定量以上来解决。 也就是说，在表面交联步骤之前，将分类的聚合物的至少一部分再次供给到相同或不同的粉碎步骤，其中由下式表示的粉碎步骤中的循环粉碎比为1.10至1.50：（ 循环粉碎比）=（粉碎步骤中的吸水性树脂的总供给量）/（干燥工序中的吸水性树脂的总排出量）（其中，吸水性树脂与粉碎的总供给量 步骤）=（干燥步骤中的吸水性树脂的总排出量）+（再次供给相同或不同的粉碎步骤的分类聚合物的量））。
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