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公开(公告)号：US20100075134A1
公开(公告)日：2010-03-25
申请号：US12543206
申请日：2009-08-18
CPC分类号： C08J5/08 , C08G59/502 , C08J2363/00 , C08L63/00 , D06M23/12 , Y10T428/249997 , Y10T428/2984 , Y10T428/30
摘要： A reinforced composite material includes a solid polymer matrix, a reinforcing material in the solid polymer matrix, and a first plurality of capsules. The reinforcing material includes a surface. The capsules are on the surface of the reinforcing material, and include a liquid healing agent. The amount of the healing agent of the capsules is at least 0.01 milligrams per square centimeter of the surface area of the reinforcing material.
摘要翻译： 增强复合材料包括固体聚合物基质，固体聚合物基体中的增强材料和第一多个胶囊。 增强材料包括表面。 胶囊在增强材料的表面上，并且包括液体愈合剂。 胶囊的愈合剂的量为增强材料的表面积至少0.01毫克/平方厘米。
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2.发明申请CAPSULES, METHODS FOR MAKING CAPSULES, AND SELF-HEALING COMPOSITES INCLUDING THE SAME 审中-公开胶囊，制造胶囊的方法和包括其的自愈合复合物公开(公告)号：US20080299391A1
公开(公告)日：2008-12-04
申请号：US11756280
申请日：2007-05-31
CPC分类号： C08F2/22 , B01J13/14 , B29C73/163 , B29C73/22 , C08F255/00 , C08F265/04 , C08F277/00 , C08F279/02 , C08F289/00 , C08G59/502 , C08L51/003 , C08L51/08 , C08L61/24 , C08L63/00 , C08L75/04 , Y10T428/2985 , C08L2666/02
摘要： A composition includes a plurality of capsules, and a polymerizer in the capsules. The capsules have an average outer diameter less than 10 micrometers. The capsules can be made by sonicating an emulsion to form a microemulsion, where the emulsion includes water, a surfactant, a first polymerizer and a second polymerizer, and then polymerizing the first polymerizer. The capsules may be present in a composite material that includes a polymer matrix and an activator.
摘要翻译： 组合物包括多个胶囊，以及胶囊中的聚合反应器。 胶囊具有小于10微米的平均外径。 胶囊可以通过超声处理乳液形成微乳液，其中乳液包括水，表面活性剂，第一聚合反应器和第二聚合器，然后聚合第一聚合反应器。 胶囊可以存在于包括聚合物基质和活化剂的复合材料中。
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公开(公告)号：US09108364B2
公开(公告)日：2015-08-18
申请号：US12739537
申请日：2008-10-27
申请人： Mary M. Caruso , David A. Delafuente , Benjamin J. Blaiszik , Jason M. Kamphaus , Nancy R. Sottos , Scott R. White , Jeffrey S. Moore
发明人： Mary M. Caruso , David A. Delafuente , Benjamin J. Blaiszik , Jason M. Kamphaus , Nancy R. Sottos , Scott R. White , Jeffrey S. Moore
CPC分类号： B29C73/163 , B29C73/22
摘要： A composite material includes a solid polymer matrix, a plurality of capsules and a liquid, in the capsules. The liquid includes from 50 to 100 wt % of a solvent, and from 0 to 50 wt % of a polymerizer. There is no polymerizer outside of the capsules. The solid polymer matrix may include a native activating moiety for the polymerizer. The solvent may have a swelling ratio with the solid polymer matrix of at least 1.1 and/or may have a polarity ET of from 0.10 to 0.50.
摘要翻译： 复合材料包括胶囊中的固体聚合物基质，多个胶囊和液体。 液体包含50-100重量％的溶剂和0-50重量％的聚合反应器。 胶囊外没有聚合反应器。 固体聚合物基质可以包括用于聚合反应器的天然活化部分。 溶剂可以具有至少1.1的固体聚合物基质的溶胀比和/或可以具有0.10-0.50的极性ET。
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公开(公告)号：US20090181254A1
公开(公告)日：2009-07-16
申请号：US12014573
申请日：2008-01-15
申请人： Scott R. White , Steven Mookhoek , Sybrand van der Zwaag , Nancy R. Sottos , Benjamin J. Blaiszik
发明人： Scott R. White , Steven Mookhoek , Sybrand van der Zwaag , Nancy R. Sottos , Benjamin J. Blaiszik
CPC分类号： B01J13/14 , B01J13/10 , B01J13/20 , Y10T428/2984
摘要： A multi-capsule composition includes a first capsule, which includes a first capsule wall defining a first interior volume and a first fluid in the first interior volume, and a plurality of second capsules, at least partially embedded in the first capsule wall. The second capsules include a second capsule wall defining a second interior volume and a second fluid in the second interior volume. The multi-capsule composition may include at least one active agent, such as pharmaceutical agents, food additives, cleaning agents, complexing agents, personal care substances, lubricants, adhesives, heating/cooling agents, colorants, indicators, superabsorbents, agricultural additives, and healing agents.
摘要翻译： 多胶囊组合物包括第一胶囊，其包括限定第一内部容积的第一胶囊壁和第一内部容积中的第一流体，以及至少部分地嵌入第一胶囊壁中的多个第二胶囊。 第二胶囊包括限定第二内部体积的第二胶囊壁和在第二内部体积中的第二流体。 多胶囊组合物可以包括至少一种活性剂，例如药剂，食品添加剂，清洁剂，络合剂，个人护理物质，润滑剂，粘合剂，加热/冷却剂，着色剂，指示剂，超吸收剂，农业添加剂和 愈合剂。
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公开(公告)号：US08703285B2
公开(公告)日：2014-04-22
申请号：US12543206
申请日：2009-08-18
CPC分类号： C08J5/08 , C08G59/502 , C08J2363/00 , C08L63/00 , D06M23/12 , Y10T428/249997 , Y10T428/2984 , Y10T428/30
摘要： A reinforced composite material includes a solid polymer matrix, a reinforcing material in the solid polymer matrix, and a first plurality of capsules. The reinforcing material includes a surface. The capsules are on the surface of the reinforcing material, and include a liquid healing agent. The amount of the healing agent of the capsules is at least 0.01 milligrams per square centimeter of the surface area of the reinforcing material.
摘要翻译： 增强复合材料包括固体聚合物基质，固体聚合物基体中的增强材料和第一多个胶囊。 增强材料包括表面。 胶囊在增强材料的表面上，并且包括液体愈合剂。 胶囊的愈合剂的量为增强材料的表面积至少0.01毫克/平方厘米。
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公开(公告)号：US20130171484A1
公开(公告)日：2013-07-04
申请号：US13489871
申请日：2012-06-06
申请人： Marta B. Baginska , Benjamin J. Blaiszik , Aaron Esser-Kahn , Susan A. Odom , Wei Weng , Zhengcheng Zhang , Nancy R. Sottos , Scott R. White , Jeffrey S. Moore , Khalil Amine
发明人： Marta B. Baginska , Benjamin J. Blaiszik , Aaron Esser-Kahn , Susan A. Odom , Wei Weng , Zhengcheng Zhang , Nancy R. Sottos , Scott R. White , Jeffrey S. Moore , Khalil Amine
IPC分类号： H01M10/056 , H01M10/0525
CPC分类号： H01M10/056 , H01M10/0525 , H01M10/4235
摘要： An autonomous battery shutdown system includes a battery including an anode and a cathode, and an electrolyte composition between the anode and the cathode. The electrolyte composition includes an ionically conductive liquid containing lithium ions, and temperature-sensitive particles including a polymer having a melting temperature between 60° C. and 120° C. When the temperature of the battery exceeds 120° C., the temperature-sensitive particles form an ion barrier that traverses the battery. The resulting shutdown battery may have a specific charge capacity that is more than 98% lower than the specific charge capacity of the original battery.
摘要翻译： 自主的电池关闭系统包括包括阳极和阴极的电池，以及在阳极和阴极之间的电解质组合物。 电解质组合物包含含有锂离子的离子导电性液体，以及包含熔点为60℃〜120℃的聚合物的温度敏感性粒子。当电池温度超过120℃时，温度敏感 颗粒形成穿过电池的离子屏障。 所产生的关闭电池可能具有比原始电池的特定充电容量低98％以上的特定充电容量。
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7.发明申请公开(公告)号：US20130072596A1
公开(公告)日：2013-03-21
申请号：US13421986
申请日：2012-03-16
CPC分类号： C08L75/04 , B01J13/20 , B01J13/22 , Y10T428/2982 , Y10T428/2984 , Y10T428/2989
摘要： A method of making capsules includes forming a mixture including a core liquid, a polyurethane precursor system, a first component of a two-component poly(urea-formaldehyde) precursor system, and a solvent. The method further includes emulsifying the mixture, adding a second component of the two-component poly(urea-formaldehyde) precursor system to the emulsified mixture, and maintaining the emulsified mixture at a temperature and for a time sufficient to form a plurality of capsules that encapsulate at least a portion of the core liquid. The capsules made by the method may include a polymerizer in the capsules, where the capsules have an inner capsule wall including a polyurethane, and an outer capsule wall including a poly(urea-formaldehyde). The capsules may include in the solid polymer matrix of a composite material.
摘要翻译： 制备胶囊的方法包括形成包括核心液体，聚氨酯前体体系，双组分聚（脲 - 甲醛）前体体系的第一组分和溶剂的混合物。 该方法还包括乳化混合物，向乳化混合物中加入双组分聚（脲 - 甲醛）前体体系的第二组分，并将乳化混合物保持在足以形成多个胶囊的温度和时间 封装至少一部分芯液。 通过该方法制备的胶囊可以包括在胶囊中的聚合反应器，其中胶囊具有包括聚氨酯的内胶囊壁和包含聚（脲 - 甲醛）的外胶囊壁。 胶囊可以包括在复合材料的固体聚合物基质中。
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8.发明申请公开(公告)号：US20120067615A1
公开(公告)日：2012-03-22
申请号：US13164144
申请日：2011-06-20
申请人： Benjamin J. Blaiszik , Susan A. Odom , Mary M. Caruso , Aaron C. Jackson , Marta B. Baginska , Joshua A. Ritchey , Aaron D. Finke , Scott R. White , Jeffrey S. Moore , Nancy R. Sottos , Paul V. Braun , Khalil Amine
发明人： Benjamin J. Blaiszik , Susan A. Odom , Mary M. Caruso , Aaron C. Jackson , Marta B. Baginska , Joshua A. Ritchey , Aaron D. Finke , Scott R. White , Jeffrey S. Moore , Nancy R. Sottos , Paul V. Braun , Khalil Amine
IPC分类号： H01B3/30
CPC分类号： H01B1/02 , Y10T428/249997
摘要： An autonomic conductivity restoration system includes a solid conductor and a plurality of particles. The particles include a conductive fluid, a plurality of conductive microparticles, and/or a conductive material forming agent. The solid conductor has a first end, a second end, and a first conductivity between the first and second ends. When a crack forms between the first and second ends of the conductor, the contents of at least a portion of the particles are released into the crack. The cracked conductor and the released contents of the particles form a restored conductor having a second conductivity, which may be at least 90% of the first conductivity.
摘要翻译： 自主导电恢复系统包括固体导体和多个颗粒。 颗粒包括导电流体，多个导电微粒和/或导电材料形成剂。 固体导体具有在第一和第二端之间的第一端，第二端和第一导电性。 当在导体的第一和第二端之间形成裂纹时，至少一部分颗粒的内容物被释放到裂纹中。 破裂的导体和释放的颗粒的内容物形成具有第二导电性的恢复的导体，其可以是第一导电率的至少90％。
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9.发明授权公开(公告)号：US08951639B2
公开(公告)日：2015-02-10
申请号：US13421986
申请日：2012-03-16
申请人： Scott R. White , Jeffrey S. Moore , Nancy R. Sottos , Benjamin J. Blaiszik , Mary M. Caruso , Christian L. Mangun
发明人： Scott R. White , Jeffrey S. Moore , Nancy R. Sottos , Benjamin J. Blaiszik , Mary M. Caruso , Christian L. Mangun
CPC分类号： C08L75/04 , B01J13/20 , B01J13/22 , Y10T428/2982 , Y10T428/2984 , Y10T428/2989
摘要： A method of making capsules includes forming a mixture including a core liquid, a polyurethane precursor system, a first component of a two-component poly(urea-formaldehyde) precursor system, and a solvent. The method further includes emulsifying the mixture, adding a second component of the two-component poly(urea-formaldehyde) precursor system to the emulsified mixture, and maintaining the emulsified mixture at a temperature and for a time sufficient to form a plurality of capsules that encapsulate at least a portion of the core liquid. The capsules made by the method may include a polymerizer in the capsules, where the capsules have an inner capsule wall including a polyurethane, and an outer capsule wall including a poly(urea-formaldehyde). The capsules may include in the solid polymer matrix of a composite material.
摘要翻译： 制备胶囊的方法包括形成包括核心液体，聚氨酯前体体系，双组分聚（脲 - 甲醛）前体体系的第一组分和溶剂的混合物。 该方法还包括乳化混合物，向乳化混合物中加入双组分聚（脲 - 甲醛）前体体系的第二组分，并将乳化混合物保持在足以形成多个胶囊的温度和时间 封装至少一部分芯液。 通过该方法制备的胶囊可以包括在胶囊中的聚合反应器，其中胶囊具有包括聚氨酯的内胶囊壁和包含聚（脲 - 甲醛）的外胶囊壁。 胶囊可以包括在复合材料的固体聚合物基质中。
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10.发明授权公开(公告)号：US08679621B2
公开(公告)日：2014-03-25
申请号：US13164144
申请日：2011-06-20
申请人： Benjamin J. Blaiszik , Susan A. Odom , Mary M. Caruso , Aaron C. Jackson , Marta B. Baginska , Joshua A. Ritchey , Aaron D. Finke , Scott R. White , Jeffrey S. Moore , Nancy R. Sottos , Paul V. Braun , Khalil Amine
发明人： Benjamin J. Blaiszik , Susan A. Odom , Mary M. Caruso , Aaron C. Jackson , Marta B. Baginska , Joshua A. Ritchey , Aaron D. Finke , Scott R. White , Jeffrey S. Moore , Nancy R. Sottos , Paul V. Braun , Khalil Amine
IPC分类号： H01B3/30
CPC分类号： H01B1/02 , Y10T428/249997
摘要： An autonomic conductivity restoration system includes a solid conductor and a plurality of particles. The particles include a conductive fluid, a plurality of conductive microparticles, and/or a conductive material forming agent. The solid conductor has a first end, a second end, and a first conductivity between the first and second ends. When a crack forms between the first and second ends of the conductor, the contents of at least a portion of the particles are released into the crack. The cracked conductor and the released contents of the particles form a restored conductor having a second conductivity, which may be at least 90% of the first conductivity.
摘要翻译： 自主导电恢复系统包括固体导体和多个颗粒。 颗粒包括导电流体，多个导电微粒和/或导电材料形成剂。 固体导体具有在第一和第二端之间的第一端，第二端和第一导电性。 当在导体的第一和第二端之间形成裂纹时，至少一部分颗粒的内容物被释放到裂纹中。 破裂的导体和释放的颗粒的内容物形成具有第二导电性的恢复的导体，其可以是第一导电率的至少90％。
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