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    Process for the preparation of carbon fibers
    1.
    发明授权
    Process for the preparation of carbon fibers 失效
    碳纤维制备方法

    公开(公告)号：US4554148A

    公开(公告)日：1985-11-19

    申请号：US611152

    申请日：1984-05-17

    申请人： Shimpei Gomi ,  Tomio Arai ,  Fumio Mogi ,  Kunio Miura ,  Sugio Otani

    发明人： Shimpei Gomi ,  Tomio Arai ,  Fumio Mogi ,  Kunio Miura ,  Sugio Otani

    IPC分类号： D01F9/155 ,  C10C3/00 ,  D01F9/145 ,  D01F9/12

    CPC分类号： D01F9/145 ,  C10C3/00

    摘要： A process for the preparation of carbon fibers, including the steps of:subjecting a raw material oil to thermal cracking conditions at a temperature of between 400.degree. to 500.degree. C. while removing cracked, light hydrocarbon components to obtain a pitch product containing at least 5 weight % of mesophase and not more than 10 weight % of light hydrocarbon components with a boiling point at 60 mmHg (absolute) of 300.degree. C. or less and having a softening point of between 140.degree. and 220.degree. C., the raw material oil having a boiling point of at least 500.degree. C. and containing at least 30 weight % of a residual oil which has a boiling point of at least 500.degree. C. and a metal content of at least 200 weight ppm and which is derived from a napthene base and/or intermediate base petroleum crude;removing the mesophase having a particle size of more than 10 .mu.m from the pitch product to obtain a substantially mesophase-free carbonaceous pitch;spinning the substantially mesophase-free pitch into fibers;rendering the spun fibers infusible; andcarbonizing the infusible fibers.

    摘要翻译： 一种制备碳纤维的方法，包括以下步骤：在400-500℃的温度下对原料油进行热裂解条件，同时除去裂化的轻烃组分，得到至少含有 5重量％的中间相和不超过10重量％的沸点在60mmHg（绝对值）为300℃或更低，软化点在140-220℃之间的轻烃组分，原料 沸点至少为500℃，含有至少30重量％的沸点为至少500℃，金属含量至少为200重量ppm的残油的材料油，其衍生物 来自一个萘环和/或中间基石油原油; 从沥青产物中除去具有大于10μm的粒度的中间相，以获得基本上不含中间相的碳质沥青; 将基本上无中间相沥青纺丝成纤维; 使纺丝纤维不可渗透; 并将可熔纤维碳化。

    Method of preparing carbonaceous pitch
    2.
    发明授权
    Method of preparing carbonaceous pitch 失效
    碳质沥青的制备方法

    公开(公告)号：US4591424A

    公开(公告)日：1986-05-27

    申请号：US611072

    申请日：1984-05-17

    申请人： Shimpei Gomi ,  Tomio Arai ,  Fumio Mogi ,  Takao Nakagawa ,  Kunio Miura ,  Sugio Otani

    发明人： Shimpei Gomi ,  Tomio Arai ,  Fumio Mogi ,  Takao Nakagawa ,  Kunio Miura ,  Sugio Otani

    IPC分类号： C10C3/04 ,  C10C3/00 ,  C10C3/10 ,  D01F9/145 ,  D01F9/155 ,  C10C3/18

    CPC分类号： C10C3/00 ,  D01F9/145

    摘要： A method of preparing an carbonaceous pitch, including the steps of:subjecting a raw material oil to thermal cracking conditions while removing cracked, light hydrocarbon components to obtain a pitch product containing at least 5 weight % of mesophase and not more than 10 weight % of light hydrocarbon components with a boiling point at 60 mmHg of 300.degree. C. or less and having a softening point of between 160.degree. and 220.degree. C., the raw material oil being composed mainly of a residual oil which has a boiling point of 350.degree. C. or more and which is derived from a naphthene base petroleum crude; andremoving the mesophase from the pitch product to obtain a substantially mesophase-free carbonaceous pitch.

    摘要翻译： 一种制备碳质沥青的方法，包括以下步骤：将原料油进行热裂解处理，同时除去裂化的轻烃组分，得到含有至少5重量％的中间相的沥青产物，并且不超过10重量％ 沸点在60mmHg的轻质烃成分为300℃以下，软化点为160〜220℃，原料油主要由沸点为350℃的残油组成 ℃以上，衍生自环烷烃基石油原油; 并从沥青产物中除去中间相以获得基本上无中间相的碳质沥青。

    Carbonaceous pitch, process for the preparation thereof and use thereof to make carbon fibers
    3.
    发明授权
    Carbonaceous pitch, process for the preparation thereof and use thereof to make carbon fibers 失效
    碳质沥青，其制备方法及其制备碳纤维的用途

    公开(公告)号：US4504455A

    公开(公告)日：1985-03-12

    申请号：US577695

    申请日：1984-02-07

    申请人： Sugio Otani ,  Shimpei Gomi ,  Fumio Mogi

    发明人： Sugio Otani ,  Shimpei Gomi ,  Fumio Mogi

    IPC分类号： C10C3/02 ,  D01F9/145 ,  D01F9/155 ,  C10C3/06 ,  C10C3/08

    CPC分类号： D01F9/145

    摘要： A novel reformed mesophase pitch having a mesophase content MC of between 40 and 100%, a quinoline-insoluble content QI of between 5 and 70 weight % and anisotropic domains forming a continuous phase. The reformed mesophase pitch is obtained by heat-treating a dormant mesophase pitch which comprises dormant anisotropic components which are partially hydrogenated, polycyclic polycondensed ring aromatic hydrocarbons derived from the mesophase of a mesophase pitch by hydrogenation of the mesophase and which are soluble in quinoline. The dormant mesophase pitch is optically isotropic in nature but, upon being subjected to shear forces in one direction, capable of being oriented in said direction. Preferably, the reformed mesophase pitch has a softening point SP in .degree.C. satisfying the following conditions:when 40 .ltoreq.MC

    摘要翻译： 中间相含量MC为40〜100％，喹啉不溶成分QI为5〜70重量％，形成连续相的各向异性畴的新型中间相沥青。 重整的中间相沥青是通过热处理休眠中间相沥青得到的，该休眠中间相沥青包括由中间相氢化得到的中间相沥青的衍生自中间相沥青的部分氢化的多环缩聚环芳烃的休眠各向异性成分，并且可溶于喹啉。 休眠中间相沥青本质上是光学各向同性的，但是在一个方向受到剪切力时，能够沿所述方向取向。 优选地，重整的中间相沥青具有在℃下的软化点SP，满足以下条件：当40 = MC <100，＆lt; IMAGE＆gt;当MC = 100时，重整的中间相沥青可用作前体材料 用于碳纤维。

    Dormant mesophase pitch
    4.
    发明授权
    Dormant mesophase pitch 失效
    休眠中间相沥青

    公开(公告)号：US4472265A

    公开(公告)日：1984-09-18

    申请号：US329432

    申请日：1981-12-10

    申请人： Sugio Otani

    发明人： Sugio Otani

    IPC分类号： D01F9/155 ,  C10C3/00 ,  C10C3/02 ,  D01F9/145 ,  D01F9/14

    CPC分类号： C10C3/00 ,  D01F9/145

    摘要： A novel carbonaceous pitch which is optically isotropic in nature and which turns into optically anisotropic when shear forces are applied thereto. The carbonaceous pitch may be obtained by hydrogenating the mesophase of a mesophase pitch to the extent that the mesophase is rendered soluble in quinoline. The carbonaceous pitch is useful as a binder and an impregnator and as a precursor material for a highly oriented, high-strength and high-modulus carbon fiber, needle coke or the like carbonaceous materials.

    摘要翻译： 一种新颖的碳质沥青，其本质上是光学各向同性的，并且当施加剪切力时变成光学各向异性。 可以通过将中间相沥青的中间相氢化为使中间相溶于喹啉的程度来获得碳质沥青。 碳质沥青可用作粘合剂和浸渍剂以及用作高取向，高强度和高模量碳纤维，针状焦碳等碳质材料的前体材料。

    Production of carbon fibers having high anisotropy
    7.
    发明授权
    Production of carbon fibers having high anisotropy 失效
    生产具有高各向异性的碳纤维

    公开(公告)号：US4115527A

    公开(公告)日：1978-09-19

    申请号：US755603

    申请日：1976-12-29

    申请人： Sugio Otani ,  Shoji Watanabe ,  Tadashi Araki

    发明人： Sugio Otani ,  Shoji Watanabe ,  Tadashi Araki

    IPC分类号： C01B31/00 ,  C04B35/524 ,  C10C1/19 ,  D01F9/145 ,  D01F9/14

    CPC分类号： D01F9/145 ,  C01B31/00 ,  C04B35/524 ,  C10C1/19

    摘要： In the production of carbon shaped articles such as fibers having high molecular orientation, anisotropy, strength, and modulus of elasticity through the steps of forming raw material pitch into fibers, infusibilization of the same followed by carbonization optionally graphitization, a raw material pitch having particular physical properties such as melt viscosity of 0.4 to 700 poises at a temperature range of 320.degree. to 480.degree. C, eminent structural anisotropy, and fluidity is used to produce such fibers product.

    摘要翻译： 在通过将原料沥青形成纤维的步骤，随后进行碳化可任意石墨化的步骤中生产碳形物品如具有高分子取向，各向异性，强度和弹性模量的纤维，具有特定的原料沥青 在320〜480℃的温度范围内的熔融粘度为0.4〜700泊的物理性质，显着的结构各向异性和流动性用于制造这种纤维制品。