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1.发明授权Process for preparing yarn derived from aramid copolymer fiber having low residual sulfur 有权用于制备具有低残留硫的芳族聚酰胺共聚物纤维得到的纱线的方法公开(公告)号：US09315923B2
公开(公告)日：2016-04-19
申请号：US14371444
申请日：2012-01-11
Applicant: Steven R. Allen , Vlodek Gabara , Joseph Lenning Lowery , Steven Raymond Lustig , Christopher William Newton , David J. Rodini , Andrew J. Sitter
Inventor： Steven R. Allen , Vlodek Gabara , Joseph Lenning Lowery , Steven Raymond Lustig , Christopher William Newton , David J. Rodini , Andrew J. Sitter
CPC classification number: D01F8/16 , D01D5/06 , D01D10/06 , D01F6/74 , D01F6/805 , D01F11/08 , D10B2331/14
Abstract: The present invention concerns processes for producing a yarn comprising polymer comprising imidazole groups, the process having the following steps: (a) spinning a solution of polymer in sulfuric acid to give rise to a plurality of dope filaments; (b) coagulating the plurality of dope filaments into a multi-filament as-spun yarn; and (c) washing the as-spun multi-filament yarn with an aqueous acid comprising a halide or an aqueous salt comprising a halide or combination thereof.
Abstract translation: 本发明涉及生产包含咪唑基团的聚合物的纱线的方法，该方法具有以下步骤：（a）将聚合物溶液在硫酸中纺丝以产生多个涂料丝; （b）将多根纺丝原丝凝结成纺丝纱; 和（c）用包含卤化物或包含卤化物或其组合的盐水的含水酸洗涤初纺复丝纱线。
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公开(公告)号：US08671524B2
公开(公告)日：2014-03-18
申请号：US13349611
申请日：2012-01-13
Applicant: Steven R. Allen , Christopher William Newton
Inventor： Steven R. Allen , Christopher William Newton
IPC: D01B9/00
Abstract: The present invention concerns processes for reducing water in never-dried fiber comprising copolymer derived from the copolymerization of para-phenylenediamine, 5(6)-amino-2-(p-aminophenyl)benzimidazole; and terephthaloyl dichloride, the process having the following steps in a continuous process, (a) a step of drying a never-dried fiber having at least 0.1% sulfur at less than 150° C. until the moisture content of the fiber is less than 60 weight percent; and (b) a step of further drying the fiber above 150° C. while the moisture content of the fiber is no more than 60 weight percent; and the fiber being further heated to at least 350° C. in either an additional continuous or separate step.
Abstract translation: 本发明涉及减少未干燥纤维中水分的方法，包括由对苯二胺，5（6） - 氨基-2-（对氨基苯基）苯并咪唑的共聚得到的共聚物; 和对苯二甲酰氯，该方法在连续方法中具有以下步骤，（a）在小于150℃下干燥具有至少0.1％硫的未干燥纤维，直到纤维的水分含量低于 60％ 和（b）当纤维的水分含量不超过60重量％时，纤维进一步干燥150℃以上的步骤; 并且在额外的连续或分开的步骤中将纤维进一步加热至至少350℃。
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公开(公告)号：US20130012679A1
公开(公告)日：2013-01-10
申请号：US13516755
申请日：2010-12-21
Applicant: Rajiv Dhawan , Joachim C. Ritter , Frederick K. Mallon , Steven R. Allen , David J. Rodini , Roger K. Siamionko
Inventor： Rajiv Dhawan , Joachim C. Ritter , Frederick K. Mallon , Steven R. Allen , David J. Rodini , Roger K. Siamionko
IPC: C08G65/38
CPC classification number: C08G73/18 , C08G61/123 , C08G73/22
Abstract: New triaminophenol compositions and related compounds are disclosed, as are processes for their preparation and for the preparation of novel salts and diacid complexes from such compounds. Polymers prepared from these compositions can be made into high strength fiber, film, and tape and are useful in applications such as protective apparel, aircraft, automotive components, personal electronics, and sports equipment.
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公开(公告)号：US20080203610A1
公开(公告)日：2008-08-28
申请号：US11909950
申请日：2006-03-27
Applicant: Christopher William Newton , Steven R. Allen , Stephen D. Moore
Inventor： Christopher William Newton , Steven R. Allen , Stephen D. Moore
CPC classification number: D01F6/74
Abstract: The present invention relates to processes for hydrolyzing polyphosphoric acid in spun multifilament yarns.
Abstract translation: 本发明涉及在纺丝复丝纱中水解多磷酸的方法。
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5.发明授权公开(公告)号：US09080261B2
公开(公告)日：2015-07-14
申请号：US14371535
申请日：2012-01-11
Applicant: Steven R. Allen , Vlodek Gabara , Joseph Lenning Lowery , Christopher William Newton , David J. Rodini
Inventor： Steven R. Allen , Vlodek Gabara , Joseph Lenning Lowery , Christopher William Newton , David J. Rodini
CPC classification number: D01F6/805 , D01D10/06 , D10B2331/021
Abstract: The present invention concerns methods for removing sulfur from a fiber made from a polymer comprising imidazole groups, said method comprising: a) contacting never-dried sulfate anion containing polymeric-fiber with aqueous salt having monovalent anions to displace at least a portion of the sulfate anions; and b) rinsing the fiber to remove displaced sulfate anions.
Abstract translation: 本发明涉及从由包含咪唑基团的聚合物制成的纤维中除去硫的方法，所述方法包括：a）将含有聚合纤维的未干燥硫酸根阴离子与含有一价阴离子的盐水接触，以置换至少一部分硫酸盐 阴离子 和b）漂洗纤维以除去置换的硫酸根阴离子。
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Patent Agency Ranking
6.发明申请公开(公告)号：US20150073119A1
公开(公告)日：2015-03-12
申请号：US14371535
申请日：2012-01-11
Applicant: Steven R. Allen , Vlodek Gabara , Joseph Lenning Lowery , Christopher William Newton , David J. Rodini
Inventor： Steven R. Allen , Vlodek Gabara , Joseph Lenning Lowery , Christopher William Newton , David J. Rodini
CPC classification number: D01F6/805 , D01D10/06 , D10B2331/021
Abstract: The present invention concerns methods for removing sulfur from a fiber made from a polymer comprising imidazole groups, said method comprising: a) contacting never-dried sulfate anion containing polymeric-fiber with aqueous salt having monovalent anions to displace at least a portion of the sulfate anions; and b) rinsing the fiber to remove displaced sulfate anions.
Abstract translation: 本发明涉及从由包含咪唑基团的聚合物制成的纤维中除去硫的方法，所述方法包括：a）将含有聚合纤维的未干燥硫酸根阴离子与含有一价阴离子的盐水接触，以置换至少一部分硫酸盐 阴离子 和b）漂洗纤维以除去置换的硫酸根阴离子。
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7.发明申请SULFUR AND ALKALI METAL CONTAINING IMIDAZOLE FIBER HAVING IONICALLY BOUND HALIDES 有权含硫离子和碱性金属的咪唑啉纤维具有离子键公开(公告)号：US20140356611A1
公开(公告)日：2014-12-04
申请号：US14371768
申请日：2012-01-11
Applicant: Steven R. Allen , Vlodek Gabara , Joseph Lenning Lowery , Christopher William Newton , David J. Rodini , Andrew J. Sitter
Inventor： Steven R. Allen , Vlodek Gabara , Joseph Lenning Lowery , Christopher William Newton , David J. Rodini , Andrew J. Sitter
IPC: D01F6/78
CPC classification number: D01F6/78 , D01F6/74 , D01F6/805 , Y10T428/249921
Abstract: The present invention concerns fiber made from a polymer comprising imidazole groups, the polymer further having: i) halide anions being present in an amount in the range of 0.05 to 20.1 weight percent, based on weight of fiber; ii) sulfur, wherein the sulfur is present in the fiber in an amount in the range of 0.05 to 3 weight percent, based on weight of fiber; and iii) alkali metal ion, wherein the alkali metal ion is present in the fiber in an amount in the range of 0.05 to 2 weight percent, based on weight of fiber.
Abstract translation: 本发明涉及由包含咪唑基的聚合物制成的纤维，所述聚合物还具有：i）卤化物阴离子的存在量为基于纤维重量的0.05至20.1重量％; ii）硫，其中基于纤维的重量，所述纤维中存在的硫的量在0.05至3重量％的范围内; 和iii）碱金属离子，其中碱金属离子以纤维的重量计在0.05至2重量％的范围内存在于纤维中。
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公开(公告)号：US20140356610A1
公开(公告)日：2014-12-04
申请号：US14371742
申请日：2012-01-11
Applicant: Steven R. Allen , Vlodek Gabara , Joseph Lenning Lowery , Steven Raymond Lustig , Christopher William Newton , David J. Rodini , Andrew J. Sitter
Inventor： Steven R. Allen , Vlodek Gabara , Joseph Lenning Lowery , Steven Raymond Lustig , Christopher William Newton , David J. Rodini , Andrew J. Sitter
CPC classification number: C08K3/30 , C08K2003/309 , D01D10/06 , D01F6/74 , D01F6/805 , D01F11/08 , Y10T428/249921
Abstract: The present invention concerns fiber made from a polymer comprising imidazole groups, fiber further having: i) a halide anion, the halide anion being present in an amount of 0.05 to 20.1 weight percent, based on weight of fiber; and ii) sulfur, wherein the sulfur is present in the fiber in an amount of 0.05 to 3 weight percent.
Abstract translation: 本发明涉及由包含咪唑基团的聚合物制成的纤维，纤维还具有：i）卤化物阴离子，卤化物阴离子的存在量为纤维重量的0.05至20.1重量％; 和ii）硫，其中硫在0.05至3重量％的量存在于纤维中。
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9.发明申请公开(公告)号：US20140353858A1
公开(公告)日：2014-12-04
申请号：US14371746
申请日：2012-01-11
Applicant: Steven R. Allen , Vlodek Gabara , Joseph Lenning Lowery , Steven Raymond Lustig , Christopher William Newton , David J. Rodini , Andrew J. Sitter
Inventor： Steven R. Allen , Vlodek Gabara , Joseph Lenning Lowery , Steven Raymond Lustig , Christopher William Newton , David J. Rodini , Andrew J. Sitter
CPC classification number: D01D5/06 , B29D99/0078 , D01F6/805 , D01F11/08
Abstract: The present invention concerns methods for producing a yarn comprising the steps of: (a) producing a plurality of dope filaments by spinning a polymer solution in sulfuric acid through a multi-hole spinneret, the polymer comprising imidazole groups; (b) coagulating the plurality of dope filaments into an as-spun yarn; (c) contacting the yarn with an aqueous base having a pKa less than or equal to 11; and (d) rinsing the yarn.
Abstract translation: 本发明涉及用于生产纱线的方法，包括以下步骤：（a）通过多孔喷丝头纺丝硫酸中的聚合物溶液制备多根纺丝原丝，该聚合物包含咪唑基; （b）将多根纺丝纤维凝结成短纤纱; （c）使纱线与pKa小于或等于11的水性碱接触; 和（d）漂洗纱线。
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10.发明申请公开(公告)号：US20140331415A1
公开(公告)日：2014-11-13
申请号：US14371760
申请日：2012-01-11
Applicant: Steven R. Allen , Vlodek Gabara , Joseph Lenning Lowery , Christopher William Newton , David J. Rodini , Andrew J. Sitter
Inventor： Steven R. Allen , Vlodek Gabara , Joseph Lenning Lowery , Christopher William Newton , David J. Rodini , Andrew J. Sitter
IPC: D06M11/26
Abstract: The present invention concerns methods for removing sulfur from yarn comprising the steps of: a) contacting never-dried polymeric yarn with an aqueous base, the polymer comprising imidazole groups and said polymer comprising sulfur atoms characterized as being in the form of sulfate anions; b) contacting the yarn with an aqueous acid comprising a halide; and c) rinsing the yarn.
Abstract translation: 本发明涉及从纱线中除去硫的方法，包括以下步骤：a）使未干燥的聚合纱线与碱水溶液接触，所述聚合物包含咪唑基团，所述包含硫原子的聚合物以硫酸根阴离子的形式表征; b）使纱线与包含卤化物的含水酸接触; 和c）冲洗纱线。
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