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    Processes for selective dehydrohalogenation of halogenated alkanes
    5.
    发明授权
    Processes for selective dehydrohalogenation of halogenated alkanes 有权
    用于卤代烷烃选择性脱卤化氢的方法

    公开(公告)号：US08530708B2

    公开(公告)日：2013-09-10

    申请号：US11588465

    申请日：2006-10-27

    申请人： Haiyou Wang ,  Hsueh Sung Tung ,  Sudip Mukhopadhyay

    发明人： Haiyou Wang ,  Hsueh Sung Tung ,  Sudip Mukhopadhyay

    IPC分类号： C07C17/25

    CPC分类号： C07C17/206 ,  C07C17/25 ,  C07C19/08 ,  C07C21/18

    摘要： Disclosed are processes for producing halogenated olefins, and preferably tetrafluorinated propene(s), from one or more alkanes having both fluorine substituents and non-fluorine substituents, preferably with a high degree of conversion and selectivity. Preferably the process comprises the use of a catalyzed reaction in which the catalyst is selected from the group consisting of activated carbons, halogentated mono- and di-valent metal oxides, mono- and di-valent Lewis acid metal halides, zero-valent metals, and combinations of these.

    摘要翻译： 公开了一种或多种具有氟取代基和非氟取代基的烷烃的卤代烯烃，优选四氟化丙烯的制备方法，优选具有高转化率和选择性。 优选地，该方法包括使用催化反应，其中催化剂选自活性炭，卤化的一价和二价金属氧化物，一价和二价路易斯酸金属卤化物，零价金属， 以及这些的组合。

    Direct one-step synthesis of CF3-I
    6.
    发明授权
    Direct one-step synthesis of CF3-I 失效
    直接一步合成CF3-I

    公开(公告)号：US07071367B1

    公开(公告)日：2006-07-04

    申请号：US11007919

    申请日：2004-12-09

    申请人： Sudip Mukhopadhyay ,  Hsueh Sung Tung

    发明人： Sudip Mukhopadhyay ,  Hsueh Sung Tung

    IPC分类号： C07C17/00

    CPC分类号： C07C17/093 ,  C07C17/158 ,  C07C17/204 ,  C07C19/16

    摘要： The present invention provides a process for the preparation of trifluoromethyl iodide. The process includes the step of: contacting in a reactor a compound represented by the formula: CF3—W and a compound represented by the formula: Z-I wherein W is selected from CF3, hydrogen and bromine; Z is selected from hydrogen, iodine and chlorine. The step of contacting is carried out, optionally in the presence of a catalyst and further optionally in the presence of air, at a temperature, pressure and for a length of time sufficient to produce the trifluoromethyl iodide.

    摘要翻译： 本发明提供了制备三氟甲基碘的方法。 该方法包括以下步骤：在反应器中接触由下式表示的化合物：<？in-line-formula description =“In-line Formulas”end =“lead”？> CF 3 - W <？in-line-formula description =“In-line Formulas”end =“tail”？>和由以下公式表示的化合物：<？in-line-formula description =“In-line Formulas”end =“lead “？”ZI <？in-line-formula description =“In-line Formulas”end =“tail”？>其中W选自CF 3，氢和溴; Z选自氢，碘和氯。 任选地在催化剂存在下进一步任选地在空气存在下，在足以产生三氟甲基碘的温度，压力和一段时间内进行接触步骤。

    One-step synthesis of CF3-1
    8.
    发明授权
    One-step synthesis of CF3-1 有权
    一步合成CF3-1

    公开(公告)号：US07132578B1

    公开(公告)日：2006-11-07

    申请号：US11181311

    申请日：2005-07-14

    申请人： Sudip Mukhopadhyay ,  Hsueh Sung Tung

    发明人： Sudip Mukhopadhyay ,  Hsueh Sung Tung

    IPC分类号： C07C17/00

    CPC分类号： C07C17/204 ,  C07C17/093 ,  C07C17/10 ,  C07C17/158 ,  C07C17/361 ,  C07C19/07

    摘要： A process for the preparation of trifluoromethyl iodide is provided. The process includes the step of contacting in a reactor a compound represented by the formula: CF3—W and a compound represented by the formula: IFn wherein W can be H, Br, Cl, COOH, COCl, COOCH3, COOC2H5, COCH3, COPh, CF3, Si(CH3)3, SPh, SCH3, SSCF3, SSPh, SSCH3, or SO2Cl, wherein n is 1, 3, 5, or 7, and wherein the step of contacting is carried out, at a temperature, pressure and for a length of time sufficient to produce trifluoromethyl iodide. The contacting step can be carried out in the presence or absence of a catalyst and the contacting step can be carried out in the presence or absence of air.

    摘要翻译： 提供了制备三氟甲基碘的方法。 该方法包括在反应器中接触由下式表示的化合物的步骤：<？in-line-formula description =“In-line Formulas”end =“lead”？> CF 3 -W <？in-line-formula description =“In-line Formulas”end =“tail”？>和由下式表示的化合物：<？in-line-formula description =“In-line Formulas”end =“lead” 其中W可以是H，Br，Cl，COOH，COCl，COOCH CO 3，H 3，COCH 3，CO 2，CO 3，SO 3， 3，3个，3个，3个，3个，3个，3个，3个，3个，3个，3个，3个，3个，3个，3个， SUB或SO 2 Cl，其中n为1,3,5或7，并且其中接触步骤在温度，压力和时间长度下进行，足以 产生三氟甲基碘。 接触步骤可以在催化剂存在或不存在下进行，并且接触步骤可以在空气存在或不存在下进行。

    Method for producing fluorinated organic compounds
    10.
    发明申请
    Method for producing fluorinated organic compounds 有权
    氟化有机化合物的制备方法

    公开(公告)号：US20070129580A1

    公开(公告)日：2007-06-07

    申请号：US11592442

    申请日：2006-11-03

    申请人： Sudip Mukhopadhyay ,  Haridasan Nair ,  Hsueh Tung ,  Michael Van Der Puy ,  Rajiv Singh ,  Haiyou Wang ,  Robert Johnson

    发明人： Sudip Mukhopadhyay ,  Haridasan Nair ,  Hsueh Tung ,  Michael Van Der Puy ,  Rajiv Singh ,  Haiyou Wang ,  Robert Johnson

    IPC分类号： C07C17/25 ,  C07C21/18

    CPC分类号： C07C17/25 ,  C07C21/18

    摘要： Disclosed is a method for producing fluorinated organic compounds, including hydrofluoropropenes, which preferably comprises converting at least one compound of formula (I): CF3CFnCHmXa-m  (I)to at least one compound of formula (II) CF3CZCHZ  (II).where each X is independently Cl, I or Br; each Z is independently H or F; n is 1 or 2; m is 1, 2 or 3, provided that when n is 1, m is 1 or 2; a is 2 or 3, and a-m≧0. Certain embodiments include the step of reacting fluorinated C2 olefin, such as tetrafluoroethylene, with a Cl addition agent under conditions effective to produce a compound of formula (I).

    摘要翻译： 公开了一种包括氢氟丙烯的氟化有机化合物的制备方法，其优选包括转化至少一种式（I）的化合物：<？in-line-formula description =“In-line formula”end =“lead”→> CF （I）<？in-line-formula description =“In-line-formula description =”In-line-formula description =“In- 至少一种式（II）的化合物<？in-line-formula description =“In-line Formulas”end =“lead”？> CF 3 > CZCHZ（II）。<？in-line-formula description =“In-line Formulas”end =“tail”？>其中每个X独立为Cl，I或Br; 每个Z独立地为H或F; n为1或2; m为1,2或3，条件是当n为1时，m为1或2; a为2或3，a-m> = 0。 某些实施方案包括在有效产生式（I）化合物的条件下，将氟化C 2烯烃如四氟乙烯与Cl加成剂反应的步骤。