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    Carboxylation of indene
    2.
    发明授权
    Carboxylation of indene 失效
    羧酸的羧基

    公开(公告)号：US3734955A

    公开(公告)日：1973-05-22

    申请号：US3734955D

    申请日：1971-11-10

    Applicant: TEXACO INC

    Inventor： PATMORE E ,  SIEGART W ,  CHAFETZ H

    IPC: C07C51/14 ,  C07C51/15 ,  C07C57/42

    CPC classification number: C07C255/00 ,  C07C51/15 ,  C07C57/42 ,  C07C61/29

    Abstract: (X-O-),R1-BENZENE

    WHERE X IS SODIUM OR POTASSIUM, R IS HYDROGEN OR ALKYL, AND SUBSEQUENTLY ACIDIFYING THE RESULTANT INTERMEDIATE PRODUCT TO FORM THE CARBOXYLATED PRODUCT.
    METHOD OF CARBOXYLATING AN ORGANIC COMPOUND OFTHE GROUP OF RC$CH, RCH2CN, INDENE OR CYCLOPERTADIENE WHERE R IS HYDROCARBYL COMPRISING CONTACTING UNDER ANHYDROUS CONDITIONS IN AN INERT ATMOSPHERE AND IN THE PRESENCE OF AN INERT, APROTIC, DIPOLAR, LIQUID SOLVENT, SAID COMPOUND WITH A CARBONATE METAL PHENOXIDE, THE METAL PHENOXIDE OF THE FORMULA:

    Overbased sulfurized calcium alkylphenolate manufacture
    3.
    发明授权
    Overbased sulfurized calcium alkylphenolate manufacture 失效
    过硫酸钙烷基酚钠制造

    公开(公告)号：US3810837A

    公开(公告)日：1974-05-14

    申请号：US26683672

    申请日：1972-06-27

    Applicant: TEXACO INC

    Inventor： CHAFETZ H ,  CHANNING W ,  MORISSETTE B

    IPC: C10M159/22 ,  C10M1/54

    CPC classification number: C10M159/22

    Abstract: A METHOD OF PREPARING OVERBASED SULFURIZED ALKYLPHENOLATE OF ANTIOXIDANT PROPERTIES IN HYDROCARBON LUBRICATING OIL COMPRISING FIRST HEATING A MIXTURE OF SULFURIZED NORMAL CALCIUM ALKYLPHENOLATE, CALCIUM OXIDE, ALKANOIC ACID OF FROM 2 TO 3 CARBONS, ALKOXYETHANOL OF THE FORMULA ROCH2CH2OH WHERE R IS ALKYL OF FROM 1 TO 4 CARBONS, AND LUBRICATING OIL AND SUBSEQUENTLY CONTACTING THE HEATED MIXTURE WITH CARBON DIOXIDE.

    Method for preparing amine derivatives of fluorinated polystyrenes
    4.
    发明授权
    Method for preparing amine derivatives of fluorinated polystyrenes 失效
    制备氟化聚苯乙烯胺衍生物的方法

    公开(公告)号：US3793266A

    公开(公告)日：1974-02-19

    申请号：US3793266D

    申请日：1971-10-13

    Applicant: TEXACO INC

    Inventor： BIALY J ,  SIEGART W ,  BLACKLEY W ,  CHAFETZ H

    IPC: C08F8/32 ,  C10L1/22 ,  C08F7/04 ,  C08F27/08

    CPC classification number: C10L1/221 ,  C08F8/32 ,  C08F112/14

    Abstract: ANTI-STATIC FUEL COMPOSITION COMPRISING A MIXTURE OF HYDROCARBONS IN THE GASOLINE, KEROSENE AND OR FURNACE OIL BOILING RANGES AND A MINRO AMOUNT OF A REACTION PRODUCT OF AN ALIPHATIC MONOAMINE HAVING THE FORMULA RHN2 IN WHICH R IS AN ALIPHATIC RADICAL HAVING FROM 8 TO 20 CARBON ATOMS AND EITHER A FLUORINATED POLYSTYRENE HAVING THE EMPIRICAL FORMULA: (C16H3F25)X IN WHICH X IS AN AVERAGE INTEGER BETWEEN 3 TO 5, OR A FLUORINATED POLYPROPYLENE HAVING THE EMPIRICAL FORMULA: (C3HF5)X IN WHICH X HAS A VALUE FROM 20 TO 40, AND A METHOD FOR PREPARING THE ABOVE-NOTED ALIPHATIC MONOAMINE DERIVATIVES.

    Sulfurized calcium alkylphenolate lubricants
    5.
    发明授权
    Sulfurized calcium alkylphenolate lubricants 失效
    硫酸钙烷基酚酚醛润滑剂

    公开(公告)号：US3761414A

    公开(公告)日：1973-09-25

    申请号：US3761414D

    申请日：1971-09-15

    Applicant: TEXACO INC

    Inventor： HAUGEN H ,  CHAFETZ H

    IPC: C07C67/00 ,  C07C313/00 ,  C07C319/14 ,  C07C323/20 ,  C10M135/20 ,  C10M135/30 ,  C10M159/22 ,  C10M169/00 ,  C10N10/04 ,  C10N30/04 ,  C10N30/10 ,  C10N30/12 ,  C10N40/25 ,  C10M1/20

    CPC classification number: C07C323/00 ,  C10M135/20 ,  C10M135/30 ,  C10M159/22 ,  C10M2219/02 ,  C10M2219/087 ,  C10M2219/088 ,  C10M2219/089 ,  C10M2221/00 ,  C10M2221/02 ,  C10M2221/043 ,  C10M2225/041 ,  C10N2270/02

    Abstract: A LUBRICATING OIL COMPOSITION CONTAINING SULFURIZED NORMAL CALCIUM ALKYLPHENOLATE DETERGENT DISPERSANT OF IMPROVED ANTICORROSIVE PROPERTIES AND RESISTANCE TO OXIDATION, SAID DISPERSANT PREPARED BY A THREE-STEP PROCEDURE COMPRISING (1) REACTING AT A TEMPERATURE BETWEEN ABOUT 200 AND 425* F. IN THE PRESENCE OF A HYDROCARBON LUBRICATING OIL AN ALKYLPHENOL WITH A FIRST ADDITION OF CALCIUM ALKOXYALKOXIDE UTILIZING BETWEEN ABOUT 45 AND 90 WT. PERCENT OF THE STOICHIOMETRIC AMOUNT REQUIRED TO CONVERT THE ALKYLPHENOL TO CALCIUM ALKYLPHENOLATE, (2) CONTACTING AT A TEMPERATURE BETWEEN ABOUT 350 AND 425*F. THE RESULTANT REACTION MIXTURE WITH SULFUR UTILIZING A MOLE RATIO OF SULFURTO INITIAL ALKYLPHENOL OF BETWEEN ABOUT 0.5:1 AND 8:1 WHILE PASSING AN INERT GAS THROUGH THE REACTION MIXTURE AT A RATE OF BETWEEN ABOUT 0.1 AND 10 S.C.F.H./GALLON AT BETWEEN ABOUT 350 AND 425*F. UNTIL HYDROGEN SULFIDE CONTENT OF LESS THAN ABOUT 3 P.P.M. IS OBTAINED, (3) REACTING THE BLOWN MIXTURE WITH A SECOND ADDITION OF CALCIUM ALKOXYALKOXIDE AT A TEMPERATURE OF BETWEEN ABOUT 350 AND 425*F., SAID FIRST AND SECOND ADDITION TOTALING BETWEEN ABOUT 100 AND 120% OF THE STOICHIOMETRIC AMOUNT OF CALCIUM ALKOXYALKOXIDE TO FORM SAID CALCIUM ALKYLPHENOLATE, SAID COMPOSITION PREFERABLY CONTAINING A SUPPLEMENTARY DETERGENT DISPERSANT COMPRISING AN ETHYLENE OXIDE DERIVTIVE OF AN INORGANIC PHOSPHORUS ACID FREE, STEAM HYDROLYZED, POLYBUTENE-P2S5 REACTION PRODUCT.

    Process for preparing hydroxy derivatives of fluorinated polymers
    6.
    发明授权
    Process for preparing hydroxy derivatives of fluorinated polymers 失效
    制备氟化聚合物的羟基衍生物的方法

    公开(公告)号：US3847887A

    公开(公告)日：1974-11-12

    申请号：US37747573

    申请日：1973-07-09

    Applicant: TEXACO INC

    Inventor： SIEGART W ,  BLACKLEY W ,  CHAFETZ H

    IPC: C08F8/00 ,  C10L1/20 ,  C08F7/04 ,  C08F27/00 ,  C08F27/02

    CPC classification number: C10L1/206 ,  C08F8/00 ,  C08F112/08 ,  C08F110/06

    Abstract: 1. A METHOD FOR PREPARING AN ORGANIC HYDROXY COMPOUND DERIVATIVE OF A FLUORINATED POLYMER WHICH COMPRISES REACTING AT 50 TO 200*C. A FLUORINATED POLYMER FROM THE GROUP CONSISTING OF (1) A FLUORINATED POLYSTYRENE HAVING THE EMPIRICAL FORMULA (C16H3F25)X IN WHICH IS HAS A VALUE FROM 3 TO 5, AND (2) A FLUORINATED POLYPROPYLENE HAVING THE EMPRICAL FORMULA (C3HF5)X IN WHICH X HAS A VALUE FROM 20 TO 40, WITH A COMPOUND HAVING THE FORMULA ROH IN WHICH R IS A HYDROCARBYL RADICAL HAVING FROM 2 TO 30 CARBON ATOMS, IN THE PRESENCE OF A CATALYST SELECTED FROM THE GROUP CONSISTING OF: (1) A TERTIARY AMINE HAVING THE FORMULA R3N IN WHICH R IS AN ALIPHATI RADICAL HAVING FROM 1 TO 30 CARBON ATOMS, AND, (2) AN ALKALI METAL SALT HAVING THE FORMULA ROM IN WHICH M REPRESENTS AN ALKALI METAL AND R HAS THE VALUE NOTED ABOVE, SAID REACTION BEING CONDUCTED USING ABOUT ONE MOIETY OF SAID ORGANIC HYDROXY COMPOUND AND TWO MOIETIES OF SAID TERTIARY AMINE OR ALKALI METAL SALT CATALYST FOR EACH HYDROGEN ATOM IN SAID FLUORINATED POLYMER.

    Lubricant composition containing sulfurized and chlorinated alkylene polyamine reaction product
    7.
    发明授权
    Lubricant composition containing sulfurized and chlorinated alkylene polyamine reaction product 失效
    含有硫化和氯化亚烷基聚氨酯反应产物的润滑剂组合物

    公开(公告)号：US3843533A

    公开(公告)日：1974-10-22

    申请号：US31431572

    申请日：1972-12-12

    Applicant: TEXACO INC

    Inventor： CULLEN W ,  CHAFETZ H ,  HELLMUTH W

    IPC: C07D339/04 ,  C08F8/32 ,  C10M169/00 ,  C10M1/38

    CPC classification number: C10M1/08 ,  C07D339/04 ,  C08F8/22 ,  C08F8/32 ,  C08F8/48 ,  C10M2219/10 ,  C10M2219/102 ,  C10M2219/104 ,  C10M2219/106 ,  C10M2221/04 ,  C08F8/34 ,  C08F110/10

    Abstract: 1. A LUBRICATING COMPOSITION COMPRISING A MAJOR PROPORTION OF A MINERAL OIL LUBRICATING VISCOSITY CONTAINING A MINOR DETERGENT AMOUNT OF AN OIL-SOLUBLE ASHLESS SULFURIZED AND CHLORINATED ALKYLENE POLYAMIDE REACTION PRODUCT PREPARED BY CHLORINATING A REACTION PRODUCT OF SULFUR AND A POLYOLEFIN CONTAINING A TRITHIONE USING AT LEAST A MOLE OF CHLORINE PER MOLE OF TRITHIONE AT A TEMPERATURE RANGING FROM ABOUT 20 TO 95*C. TO FORM A CHLORINATED INTERMEDIATE PRODUCT, SAID TRITHIONE BEING REPRESENTED BY THE FORMULA:

    3-(S=),4-R'',5-R-3H-1,2-DITHIOLE

    IN WHICH R AND R'' REPRESENT HYDROGEN OR A HYDROCARBYL RADICAL HAVING FROM ABOUT 50 TO 125 CARBON ATOMS, AT LEAST ONE OF R AND R'' REPRESENTING AN ALIPHATIC HYDROCARBON RADICAL, AND, REACTING INTERMEDIATE PRODUCT WITH A POLYAMIDE IN THE PROPORTION OF 1 TO 5 MOLE OF SAID POLYAMINE PER MOLE OF SAID INTERMEDIATE PRODUCT AT A TEMPERATURE IN THE RANGE OF 100 TO 275*C., SAID POLYAMIDE BEING REPRESENTED BY THE FORMULA

    H2N-(R"-NH)XH

    IN WHICH R" IS A DIVALENT ALKYLENE RADICAL HAVING FROM 2 TO 6 CARBON ATOMS AND X IS AN INTEGER RANGING FROM 1 TO 6.

    Anti-static fuel composition
    10.
    发明授权
    Anti-static fuel composition 失效
    防静电燃料组合物

    公开(公告)号：US3784362A

    公开(公告)日：1974-01-08

    申请号：US3784362D

    申请日：1972-06-21

    Applicant: TEXACO INC

    Inventor： SIEGART W ,  BLACKLEY W ,  CHAFETZ H

    IPC: C08F8/00 ,  C08F8/02 ,  C10L1/20 ,  C10L1/16

    CPC classification number: C10L1/206 ,  C08F8/00 ,  C08F8/02 ,  C08F10/06 ,  C08F112/14 ,  C08F114/18

    Abstract: Anti-static fuel composition containing the reaction product of an organic hydroxy compound having the formula ROH in which R is a hydrocarbyl radical having from 2 to 30 carbon atoms and a fluorinated polymer from the group consisting of fluorinated polystyrene and fluorinated polypropylene.

    Abstract translation: 含有ROH为碳原子数为2〜30的烃基的式ROH的有机羟基化合物与氟化聚苯乙烯和氟化聚丙烯的含氟聚合物的反应产物的防静电燃料组合物。

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