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公开(公告)号：US4330593A
公开(公告)日：1982-05-18
申请号：US206732
申请日：1980-11-13
CPC分类号： H01L41/1876 , H01L41/183 , Y10T29/42 , Y10T428/2998
摘要： PZT/polymer composites and a simplified method of their fabrication are dribed. Commercially available PZT Pb(Zr, Ti)O.sub.3 powder is thoroughly mixed with a binder such as polyvinylalcohol and polymethyl methacrylate (PMM) spheres and pressed into pellets. The binder and PMM spheres are burnt out by heating pellets slowly and the porous pellets so obtained are sintered by heating them in closed high-purity alumina crucibles and lead zirconate as a source of lead is added thereto. The highly porous pellets thus obtained are impregnated with a suitable polymer such as silicone rubber elastomer or vinylcyclohexene dioxide epoxy.
摘要翻译： 描述了PZT /聚合物复合材料及其制造的简化方法。 将市售的PZT Pb（Zr，Ti）O 3粉末与粘合剂如聚乙烯醇和聚甲基丙烯酸甲酯（PMM）球充分混合并压制成颗粒。 粘合剂和PMM球体通过缓慢加热颗粒而被烧制，并且将如此得到的多孔颗粒通过在封闭的高纯度氧化铝坩埚中加热而烧结，并将铅锆酸铅作为铅源加入其中。 由此获得的高度多孔的颗粒用合适的聚合物如硅橡胶弹性体或乙烯基环己烷二氧化物环氧树脂浸渍。
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公开(公告)号：US5716565A
公开(公告)日：1998-02-10
申请号：US495222
申请日：1995-06-27
申请人： Gregory C. Stangle , Koththavasal R. Venkatachari , Steven P. Ostrander , Walter A. Schulze , Amy B. Jedlicka
发明人： Gregory C. Stangle , Koththavasal R. Venkatachari , Steven P. Ostrander , Walter A. Schulze , Amy B. Jedlicka
IPC分类号： C01B13/32 , C01B13/34 , C01G3/00 , C01G23/00 , C01G23/047 , C01G25/02 , C01G49/00 , C04B35/45 , H01L39/24 , C04B35/622
CPC分类号： C01B13/324 , B82Y30/00 , C01B13/34 , C01G23/006 , C01G23/047 , C01G25/02 , C01G3/006 , C01G49/0036 , C01G49/0054 , C04B35/4508 , H01L39/2419 , C01P2004/64 , C01P2006/10 , C01P2006/12 , C01P2006/40
摘要： A process for producing ultra-fine particles of calcia-stabilized zirconia in which a precursor mixture (which contains from about 80 to about 96 mole percent of zirconium ion, from about 20 to about 4 mole percent of calcium ion, a nitrogen-containing fuel, and a solvent) is dried and then subjected to a temperature of from about 275 to about 750 degrees centigrade and an atmosphere with a relative humidity of less than about 60 percent, thereby causing the dried particles to react in a vigorous manner and to form a combusted powder.
摘要翻译： 一种用于生产氧化钙稳定化氧化锆的超细颗粒的方法，其中前体混合物（其含有约80至约96摩尔％的锆离子，约20至约4摩尔％的钙离子，含氮燃料 和溶剂）干燥，然后经受约275至约750摄氏度的温度和相对湿度小于约60％的气氛，从而使干燥的颗粒以剧烈的方式反应并形成 一种燃烧的粉末。
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公开(公告)号：US5468427A
公开(公告)日：1995-11-21
申请号：US127637
申请日：1993-09-27
IPC分类号： C01B13/32 , C01B13/34 , C01G3/00 , C01G23/00 , C01G23/047 , C01G25/02 , C01G49/00 , C04B35/45 , H01L39/24 , C01F1/00 , C01G1/00
CPC分类号： B82Y30/00 , C01B13/324 , C01B13/34 , C01G23/006 , C01G23/047 , C01G25/02 , C01G3/006 , C01G49/0036 , C01G49/0054 , C04B35/4508 , H01L39/2419 , C01P2004/64 , C01P2006/10 , C01P2006/12 , C01P2006/40
摘要： A process for producing ultra-fine ceramic particles in which droplets are formed from a ceramic precursor mixture containing a metal cation, a nitrogen-containing fuel, a solvent, and an anion capable of participating in an anionic oxidation-reduction reaction with the nitrogen containing fuel. The nitrogen-containing fuel contains at least three nitrogen atoms, at least one oxygen atom, and at least one carbon atom. The ceramic precursor mixture is dried to remove at least 85 weight percent of the solvent, and the dried mixture is then ignited to form a combusted powder.
摘要翻译： 一种制造超细陶瓷颗粒的方法，其中由含有金属阳离子，含氮燃料，溶剂和能够参与与含氮的阴离子氧化还原反应的阴离子的陶瓷前体混合物形成液滴 汽油。 含氮燃料含有至少三个氮原子，至少一个氧原子和至少一个碳原子。 将陶瓷前体混合物干燥以除去至少85重量％的溶剂，然后将干燥的混合物点燃以形成燃烧的粉末。
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公开(公告)号：US5385882A
公开(公告)日：1995-01-31
申请号：US966019
申请日：1992-12-09
CPC分类号： C01G3/006 , C01P2004/20 , C01P2004/22 , C01P2004/61 , Y10S505/729 , Y10S505/733 , Y10S505/782 , Y10S505/783
摘要： There is disclosed a process for preparing a thallium-containing superconductive composition. In the first step of the process, a mixture of an inorganic salt (such as potassium chloride) and a powder compositon is provided; the powder composition contains at least three separate compounds which, in combination, correspond to the stoichiometry of the super-conductor to be produced. This mixture is then charged to a closed container, raised to a temperature of from 800-959 degrees Centigrade, and heated for from about 1 to about 12 hours; thereafter, it is cooled to a temperature of 600 degrees Centigrade at a rate of at least 300 degrees Celsius per hour.
摘要翻译： 公开了一种制备含铊的超导组合物的方法。 在该方法的第一步中，提供无机盐（如氯化钾）和粉末组合物的混合物; 粉末组合物含有至少三种分开的化合物，其组合对应于待生产的超导体的化学计量。 然后将该混合物装入密封容器中，升温至800-959摄氏度的温度，并加热约1至约12小时; 然后以至少300摄氏度/小时的速度将其冷却至600摄氏度的温度。
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5.发明授权
公开(公告)号：US5660774A
公开(公告)日：1997-08-26
申请号：US495796
申请日：1995-06-27
申请人： Gregory C. Stangle , Koththavasal R. Venkatachari , Steven P. Ostrander , Walter A. Schulze , John D. Pietras
发明人： Gregory C. Stangle , Koththavasal R. Venkatachari , Steven P. Ostrander , Walter A. Schulze , John D. Pietras
IPC分类号： C01B13/32 , C01B13/34 , C01G3/00 , C01G23/00 , C01G23/047 , C01G25/02 , C01G49/00 , C04B35/45 , H01L39/24 , C04B33/32 , C04B35/622
CPC分类号： C01B13/324 , B82Y30/00 , C01B13/34 , C01G23/006 , C01G23/047 , C01G25/02 , C01G3/006 , C01G49/0036 , C01G49/0054 , C04B35/4508 , H01L39/2419 , C01P2004/64 , C01P2006/10 , C01P2006/12 , C01P2006/40
摘要： A process for producing a sintered body from untra-fine superconductive particles. In the first step of this process, a ceramic precursor material containing yttrium, barium and copper cations, a nitrogen-containing material, a solvent, and an anion capable of participating in an anionic oxidation-reduction reaction with the nitrogen-containing material, is provided; the nitrogen-containing material contains at least three nitrogen atoms, at least one oxygen atom, and at least one carbon atom. In the second step of the process, droplets of such ceramic precursor material are formed. In the third step of the process, the droplets are dried until particles which contain less than about 15 weight percent of solvent are produced. In the fourth step of this process, such particles are ignited in an atmosphere which contains substantially less than about 60 weight percent of the solvent's saturation value in such atmosphere. A green body is formed from the calcined particles which is subjected to temperature to form a sintered body.
摘要翻译： 一种由未精细的超导颗粒制造烧结体的方法。 在该方法的第一步骤中，含有钇，钡和铜阳离子的陶瓷前体材料，含氮材料，溶剂和能够参与与含氮材料的阴离子氧化还原反应的阴离子是 提供; 含氮材料含有至少三个氮原子，至少一个氧原子和至少一个碳原子。 在该方法的第二步骤中，形成这种陶瓷前体材料的液滴。 在该方法的第三步骤中，将液滴干燥直到产生含有小于约15重量％溶剂的颗粒。 在该方法的第四步骤中，这种颗粒在气氛中被点燃，其气氛中含有基本上小于约60重量％的溶剂饱和度值。 由经过温度的煅烧颗粒形成生坯以形成烧结体。
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公开(公告)号：US5660772A
公开(公告)日：1997-08-26
申请号：US495223
申请日：1995-06-27
申请人： Gregory C. Stangle , Koththavasal R. Venkatachari , Steven P. Ostrander , Walter A. Schulze , John D. Pietras
发明人： Gregory C. Stangle , Koththavasal R. Venkatachari , Steven P. Ostrander , Walter A. Schulze , John D. Pietras
IPC分类号： C01B13/32 , C01B13/34 , C01G3/00 , C01G23/00 , C01G23/047 , C01G25/02 , C01G49/00 , C04B35/45 , H01L39/24 , C04B35/622
CPC分类号： C01B13/324 , B82Y30/00 , C01B13/34 , C01G23/006 , C01G23/047 , C01G25/02 , C01G3/006 , C01G49/0036 , C01G49/0054 , C04B35/4508 , H01L39/2419 , C01P2004/64 , C01P2006/10 , C01P2006/12 , C01P2006/40
摘要： A process for producing ultra-fine barium hexaferrite particles. In the first step of this process, a ceramic precursor material containing barium and trivalent ferric cations, a nitrogen-containing material, a solvent, and an anion capable of participating in an anionic oxidation-reduction reaction with the nitrogen-containing material, is provided. In the second step of the process, droplets of such ceramic precursor material are formed. In the third step of the process, the droplets are dried until particles which contain less than about 15 weight percent of solvent are produced. In the fourth step of this process, such particles are ignited in an atmosphere which contains substantially less than about 60 weight percent of the solvent's saturation value in such atmosphere.
摘要翻译： 一种生产超细六硼酸钡颗粒的方法。 在该方法的第一步中，提供了含有钡和三价三价阳离子的陶瓷前体材料，含氮材料，溶剂和能够与含氮材料进行阴离子氧化还原反应的阴离子 。 在该方法的第二步骤中，形成这种陶瓷前体材料的液滴。 在该方法的第三步骤中，将液滴干燥直到产生含有小于约15重量％溶剂的颗粒。 在该方法的第四步骤中，这种颗粒在气氛中被点燃，其气氛中含有基本上小于约60重量％的溶剂饱和度值。
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公开(公告)号：US5297438A
公开(公告)日：1994-03-29
申请号：US992241
申请日：1992-12-14
申请人： Aldo B. Alles , Walter A. Schulze
发明人： Aldo B. Alles , Walter A. Schulze
IPC分类号： C04B35/462 , C04B35/468 , G01L1/22 , G01L9/06
CPC分类号： G01L1/2293 , C04B35/462 , C04B35/4682 , C04B35/4684
摘要： An electrical circuit containing novel piezoresistive sensor is disclosed. The sensor is connected to a source of direct current, and a manometric pressure of at least about 15 p.s.i.g. is applied to the sensor.
摘要翻译： 公开了一种包含新型压阻传感器的电路。 传感器连接到直流电源，并且压力测量压力至少约为15 p.s.g. 被应用于传感器。
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公开(公告)号：US5660773A
公开(公告)日：1997-08-26
申请号：US495787
申请日：1995-06-27
申请人： Gregory C. Stangle , Koththavasal R. Venkatachari , Steven P. Ostrander , Walter A. Schulze , John D. Pietras
发明人： Gregory C. Stangle , Koththavasal R. Venkatachari , Steven P. Ostrander , Walter A. Schulze , John D. Pietras
IPC分类号： C01B13/32 , C01B13/34 , C01G3/00 , C01G23/00 , C01G23/047 , C01G25/02 , C01G49/00 , C04B35/45 , H01L39/24 , C01G49/02 , C04B35/622
CPC分类号： C01B13/324 , B82Y30/00 , C01B13/34 , C01G23/006 , C01G23/047 , C01G25/02 , C01G3/006 , C01G49/0036 , C01G49/0054 , C04B35/4508 , H01L39/2419 , C01P2004/64 , C01P2006/10 , C01P2006/12 , C01P2006/40
摘要： A process for producing ultra-fine yttrium-iron-garnet particles. In the first step of this process, a ceramic precursor material containing yettrium and ferric cations, a nitrogen-containing material, a solvent, and an anion capable of participating in an anionic oxidation-reduction reaction with the nitrogen-containing material, is provided. In the second step of the process, droplets of such ceramic precursor material are formed. In the third step of the process, the droplets are dried until particles which contain less than about 15 weight percent of solvent are produced. In the fourth step of this process, such particles are ignited in an atmosphere which contains substantially less than about 60 weight percent of the solvent's saturation value in such atmosphere.
摘要翻译： 一种生产超细钇 - 铁 - 石榴石颗粒的方法。 在该方法的第一步骤中，提供了含有还原剂和三价阳离子的陶瓷前体材料，含氮材料，溶剂和能够与含氮材料进行阴离子氧化还原反应的阴离子。 在该方法的第二步骤中，形成这种陶瓷前体材料的液滴。 在该方法的第三步骤中，将液滴干燥直到产生含有小于约15重量％溶剂的颗粒。 在该方法的第四步骤中，这种颗粒在气氛中被点燃，其气氛中含有基本上小于约60重量％的溶剂饱和度值。
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公开(公告)号：US5523065A
公开(公告)日：1996-06-04
申请号：US495786
申请日：1995-06-27
IPC分类号： C01B13/32 , C01B13/34 , C01G3/00 , C01G23/00 , C01G23/047 , C01G25/02 , C01G49/00 , C04B35/45 , H01L39/24 , C01G25/00 , C01G27/00
CPC分类号： C01B13/324 , B82Y30/00 , C01B13/34 , C01G23/006 , C01G23/047 , C01G25/02 , C01G3/006 , C01G49/0036 , C01G49/0054 , C04B35/4508 , H01L39/2419 , C01P2004/64 , C01P2006/10 , C01P2006/12 , C01P2006/40
摘要： A process for producing ultra-fine barium titanate particles. In the first step of this process, a ceramic precursor material containing a metal cation, a nitrogen-containing material, a solvent, and an anion capable of participating in an anionic oxidation-reduction reaction with the nitrogen-containing material, is provided; the nitrogen-containing material contains at least three nitrogen atoms, at least one oxygen atom, and at least one carbon atom. In the second step of the process, droplets of such ceramic precursor material are formed. In the third step of the process, the droplets are dried until particles which contain less than about 15 weight percent of solvent are produced. In the fourth step of this process, such particles are ignited in an atmosphere which contains substantially less than about 60 weight percent of the solvent's saturation value in such atmosphere.
摘要翻译： 一种制造超细钛酸钡颗粒的方法。 在该方法的第一步骤中，提供了含有能够与含氮材料进行阴离子氧化还原反应的金属阳离子，含氮材料，溶剂和阴离子的陶瓷前体材料; 含氮材料含有至少三个氮原子，至少一个氧原子和至少一个碳原子。 在该方法的第二步骤中，形成这种陶瓷前体材料的液滴。 在该方法的第三步骤中，将液滴干燥直到产生含有小于约15重量％溶剂的颗粒。 在该方法的第四步骤中，这种颗粒在气氛中被点燃，其气氛中含有基本上小于约60重量％的溶剂饱和度值。
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公开(公告)号：US5270293A
公开(公告)日：1993-12-14
申请号：US684309
申请日：1991-04-12
CPC分类号： C01G3/006 , C01P2004/20 , C01P2004/22 , C01P2004/61 , Y10S505/725 , Y10S505/78
摘要： A process for preparing a superconducting, ceramic material with an increased critical current is described. In this process, the materials used to form the superconducting material are mixed with at least one inorganic salt, and the mixture containing the salt is then heat treated. The salt is then leached from the heat-treated mixture.
摘要翻译： 描述了一种制备具有临界电流增加的超导陶瓷材料的方法。 在该方法中，用于形成超导材料的材料与至少一种无机盐混合，然后对含有盐的混合物进行热处理。 然后将盐从热处理的混合物中浸出。
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