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    Hydrosilylation process
    1.
    发明授权
    Hydrosilylation process 有权
    氢化硅烷化过程

    公开(公告)号：US07208619B2

    公开(公告)日：2007-04-24

    申请号：US10484413

    申请日：2002-07-18

    申请人： Timothy Rex Bunce ,  Avril Surgenor ,  Stephen Westall

    发明人： Timothy Rex Bunce ,  Avril Surgenor ,  Stephen Westall

    IPC分类号： C07F7/08

    CPC分类号： C08G77/045 ,  C07F7/0879 ,  C08G77/38

    摘要： A silane or siloxane containing at least one organic group is prepared by a hydrosilylation reaction between a silane or siloxane (A) containing at least one Si—H group and an allyl compound (B) in the presence of a noble metal catalyst. The silane or siloxane (A) and the allyl compound (B) are fed continuously through a reaction zone which is maintained at a temperature in the range 115–200° C. and which is provided with heat exchanger means to dissipate the heat from the exothermic hydrosilylation reaction. The residence time of (A) and (B) in the reaction zone is less than 20 minutes.

    摘要翻译： 含有至少一个有机基团的硅烷或硅氧烷是在贵金属催化剂存在下，通过含有至少一个Si-H基团和烯丙基化合物（B）的硅烷或硅氧烷（A）之间的氢化硅烷化反应来制备的。 将硅烷或硅氧烷（A）和烯丙基化合物（B）连续进料通过保持在115-200℃范围内的温度的反应区，并且设置有热交换器装置以从 放热氢化硅烷化反应。 反应区中（A）和（B）的停留时间少于20分钟。

    Manufacture of resins
    2.
    发明授权
    Manufacture of resins 有权
    树脂制造

    公开(公告)号：US07893182B2

    公开(公告)日：2011-02-22

    申请号：US10575920

    申请日：2004-10-08

    申请人： Timothy Rex Bunce ,  Bhukandas Parbhoo ,  Pierre Chevalier

    发明人： Timothy Rex Bunce ,  Bhukandas Parbhoo ,  Pierre Chevalier

    IPC分类号： C08G77/00

    CPC分类号： B01J8/1863 ,  B01J8/1818 ,  B01J8/42 ,  B01J19/088 ,  B01J2219/0809 ,  B01J2219/0828 ,  B01J2219/083 ,  B01J2219/0896 ,  C01B33/16

    摘要： A method of forming a powder and/or discrete gel particles of a compound selected from the group of a metallic oxide, a metalloid oxide, a mixed oxide, an organometallic oxide, an organometalloid oxide, an organomixed oxide resin, and/or an organic resin from one or more respective organometallic precursor(s), organometalloid precursor(s) and/or organic precursors and mixtures thereof, comprising the steps of passing a gas into a means for forming excited and/or unstable gas species (1a), typically an atmospheric plasma generating means; treating said gas such that upon leaving said means the gas comprises excited and/or unstable gas species which are substantially free of electrical charges at a temperature of between 10° C. and 500° C. A gaseous and/or liquid precursor is then introduced (50a,50b) into said excited and unstable gas species in a downstream region external (20) to the means for forming excited and/or unstable gas. The interaction between the precursor and the excited and unstable gas species results in the formation of a powder and/or discrete gelled particles which are subsequently collected. The particles prepared by the method may be subsequently functionalised.

    摘要翻译： 形成选自金属氧化物，准金属氧化物，混合氧化物，有机金属氧化物，有机金属氧化物，有机金属氧化物树脂和/或有机金属氧化物的化合物的粉末和/或离散凝胶颗粒的方法 一种或多种相应的有机金属前体，有机金属前体和/或有机前体及其混合物的树脂，包括将气体通入用于形成激发和/或不稳定气体物质（1a）的装置的步骤，通常 大气等离子体发生装置; 处理所述气体使得在离开所述装置时气体包括在10℃和500℃之间基本上不含电荷的激发和/或不稳定的气体物质。然后引入气体和/或液体前体 （50a，50b）与形成激发和/或不稳定气体的装置的外部（20）的下游区域中的所述激发和不稳定的气体物质混合。 前体与激发和不稳定气体物质之间的相互作用导致随后收集的粉末和/或离散凝胶颗粒的形成。 通过该方法制备的颗粒可以随后被官能化。

    Functionalisation of particles
    3.
    发明授权
    Functionalisation of particles 失效
    颗粒的功能化

    公开(公告)号：US07758928B2

    公开(公告)日：2010-07-20

    申请号：US10575919

    申请日：2004-10-08

    申请人： Timothy Rex Bunce ,  Bhukandas Parbhoo ,  Pierre Chevalier

    发明人： Timothy Rex Bunce ,  Bhukandas Parbhoo ,  Pierre Chevalier

    IPC分类号： B05D3/14

    CPC分类号： B82Y30/00 ,  B01J8/1818 ,  B01J8/1863 ,  B01J8/42 ,  B01J19/088 ,  B01J2219/0809 ,  B01J2219/0828 ,  B01J2219/083 ,  B01J2219/0896 ,  C01P2004/84 ,  C09C1/3615 ,  C09C1/3684

    摘要： This invention relates to a method of functionalizing a powdered substrate. The method comprises the following steps, which method comprises passing a gas into a means for forming excited and/or unstable gas species, typically an atmospheric pressure plasma or the like and treating the gas such that, upon leaving said means, the gas comprises excited and/or unstable gas species which are substantially free of electric charge. The gas comprising the excited and/or unstable gas species which are substantially free of electric charge is then used to treat a powdered substrate and a functionalizing precursor in a downstream region external to the means for forming excited and/or unstable gas, wherein neither the powdered substrate nor the functionalizing precursor have been subjected to steps (i) and (ii) and wherein said functionalizing precursor is introduced simultaneously with or subsequent to introduction of the powdered substrate. Preferably the method takes place in a fluidized bed.

    摘要翻译： 本发明涉及一种使粉末状基质官能化的方法。 该方法包括以下步骤：该方法包括使气体进入用于形成激发和/或不稳定气体物质（通常为大气压等离子体等）的装置，并处理气体，使得在离开所述装置时，气体包括激发 和/或基本上不含电荷的不稳定气体物质。 包括基本上不含电荷的被激发和/或不稳定的气体物质的气体然后用于处理形成激发和/或不稳定气体的装置外部的下游区域中的粉末基质和官能化前体，其中， 已经对粉末状基质和官能化前体进行了步骤（i）和（ii），并且其中所述官能化前体与引入粉末基质同时或之后引入。 优选地，该方法在流化床中进行。

    Functionalisation of Particles
    6.
    发明申请
    Functionalisation of Particles 失效
    颗粒的功能化

    公开(公告)号：US20080056928A1

    公开(公告)日：2008-03-06

    申请号：US10575919

    申请日：2004-10-08

    申请人： Timothy Rex Bunce ,  Bhukandas Parbhoo ,  Pierre Chevalier

    发明人： Timothy Rex Bunce ,  Bhukandas Parbhoo ,  Pierre Chevalier

    IPC分类号： B01J19/08 ,  B01J8/18 ,  B01J8/42 ,  C01B33/16 ,  C01B33/18 ,  C08G77/06

    CPC分类号： B82Y30/00 ,  B01J8/1818 ,  B01J8/1863 ,  B01J8/42 ,  B01J19/088 ,  B01J2219/0809 ,  B01J2219/0828 ,  B01J2219/083 ,  B01J2219/0896 ,  C01P2004/84 ,  C09C1/3615 ,  C09C1/3684

    摘要： This invention relates to a method of functionalising a powdered substrate. The method comprises the following steps, which method comprises passing a gas into a means for forming excited and/or unstable gas species, typically an atmospheric pressure plasma or the like and treating the gas such that, upon leaving said means, the gas comprises excited and/or unstable gas species which are substantially free of electric charge. The gas comprising the excited and/or unstable gas species which are substantially free of electric charge is then used to treat a powdered substrate and a functionalising precursor in a downstream region external to the means for forming excited and/or unstable gas, wherein neither the powdered substrate nor the functionalising precursor have been subjected to steps (i) and (ii) and wherein said functionalising precursor is introduced simultaneously with or subsequent to introduction of the powdered substrate. Preferably the method takes place in a fluidised bed.

    摘要翻译： 本发明涉及一种功能化粉末状基材的方法。 该方法包括以下步骤：该方法包括使气体进入用于形成激发和/或不稳定气体物质（通常为大气压等离子体等）的装置，并处理气体，使得在离开所述装置时，气体包括激发 和/或基本上不含电荷的不稳定气体物质。 包括基本上不含电荷的被激发和/或不稳定的气体物质的气体然后用于处理形成激发和/或不稳定气体的装置外部的下游区域中的粉末状基质和官能化前体，其中， 粉末基质和功能化前体已经经受步骤（i）和（ii），并且其中所述官能化前体在引入粉末基质的同时或之后引入。 优选地，该方法在流化床中进行。