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1.发明授权Method for preparing aqueous dispersion of developer and pressure-sensitive recording paper 失效制备显影剂和压敏记录纸的水性分散体的方法
公开(公告)号：US5204190A
公开(公告)日：1993-04-20
申请号：US905834
申请日：1992-06-29
IPC分类号： B41M5/155
CPC分类号： B41M5/155 , Y10S428/913 , Y10T428/26 , Y10T428/31536 , Y10T428/31967 , Y10T428/31996
摘要： Herein disclosed are a method for preparing an aqueous developer dispersion which comprises the steps of dissolving, in an organic solvent, a developer which comprises a nuclear-substituted salicylic acid salt represented by the following general formula (I): ##STR1## wherein R.sub.1, R.sub.2, R.sub.3 and R.sub.4 may be the same or different and each represents a hydrogen atom, a halogen atom, an alkyl group having not more than 15 carbon atoms, a cycloalkyl group, a phenyl group, a nuclear-substituted phenyl group, an aralkyl group or a nculear-substituted aralkyl group, or two adjacent groups selected from R.sub.1 to R.sub.4 may be bonded together to form a ring; n is an integer of not less than 1; and M represents magnesium, calcium, zinc, aluminum, iron, cobalt, nickel or a basic ion thereof; emulsifying and dispersing the resulting solution in an aqueous solution of an acrylamide copolymer having a degree of polymerization of not less than 100 obtained by copolymerizing 96 to 70 mole % of acrylamide with 4 to 30 mole % of an alkyl or alkoxyalkyl, having not more than 4 carbon atoms, ester of acrylic acid, methacrylic acid, itaconic acid or maleic acid; then heating the emulsified dispersion to remove the organic solvent by distillation; and optionally finely wet-pulverizing the resulting aqueous dispersion to an extent that reduction in the average particle size of the developer dispersed in the dispersion does not exceed 10%; as well as pressure-sensitive recording paper obtained using the aqueous developer dispersion. The recording paper is substantially improved in the developing density, developing velocity and printability.
摘要翻译： 本文公开了一种制备水性显影剂分散体的方法，其包括以下步骤：在有机溶剂中溶解包含由以下通式（I）表示的核取代的水杨酸盐的显影剂： 其中R1，R2，R3和R4可以相同或不同，表示氢原子，卤素原子，碳原子数不超过15个的烷基，环烷基，苯基，核取代的苯基 ，芳烷基或仲胺取代的芳烷基或选自R 1至R 4的两个相邻基团可以结合在一起形成环; n为不小于1的整数; M表示镁，钙，锌，铝，铁，钴，镍或其碱性离子; 将得到的溶液乳化分散在丙烯酰胺共聚物的水溶液中，聚丙烯酰胺共聚物的水溶液中聚合度不低于100，通过共聚96〜70摩尔％的丙烯酰胺与4〜30摩尔％的烷基或烷氧基烷基不同 4个碳原子，丙烯酸，甲基丙烯酸，衣康酸或马来酸的酯; 然后加热乳化分散液通过蒸馏除去有机溶剂; 并且任选地将得到的水分散体精细地湿粉碎至分散在分散体中的显影剂的平均粒径的降低不超过10％的程度; 以及使用含水显影剂分散体获得的压敏记录纸。 记录纸在显影密度，显影速度和可印刷性方面显着提高。
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2.发明授权
公开(公告)号：US5328884A
公开(公告)日：1994-07-12
申请号：US27987
申请日：1993-03-08
IPC分类号： B41M5/155
CPC分类号： B41M5/155
摘要： The present invention provides a color developer composition characterized in that the composition contains a color developer comprising as its main component a nucleus-substituted salicylic acid salt represented by the formula (1) given below, and at least one amide compound selected from the group consisting of the compounds of represented by the formula (2) and formula (3) given below. ##STR1## wherein R.sub.1 to R.sub.10 are as defined in the specification.
摘要翻译： 本发明提供了一种彩色显影剂组合物，其特征在于该组合物含有着色显影剂，其包含以下述式（1）表示的核取代的水杨酸盐作为其主要成分，以及至少一种选自以下的酰胺化合物： 的由下式给出的式（2）和式（3）表示的化合物。 式（1）
式（2）其中R 1至R 10如说明书中所定义的式（3）。 -
3.发明授权
公开(公告)号：US5164001A
公开(公告)日：1992-11-17
申请号：US616788
申请日：1990-11-21
CPC分类号： B41M5/155
摘要： Herein disclosed are a method for preparing an aqueous developer dispersion which comprises the steps of dissolving, in an organic solvent, a developer which comprises a nuclear-substituted salicylic acid salt represented by the following general formula (I): ##STR1## wherein R.sub.1, R.sub.2, R.sub.3 and R.sub.4 may be the same or different and each represents a hydrogen atom, a halogen atom, an alkyl group having not more than 15 carbon atoms, a cycloalkyl group, a phenyl group, a nuclear-substituted phenyl group, an aralkyl group or a nuclear-substituted aralkyl group, or two adjacent groups selected from R.sub.1 to R.sub.4 may be bonded together to form a ring; n is an integer of not less than 1; and M represents magnesium, calcium, zinc, aluminum, iron, cobalt, nickel or a basic ion thereof; emulsifying and dispersing the resulting solution in an aqueous solution of an acrylamide copolymer having a degree of polymerization of not less than 100 obtained by copolymerizing 96 to 70 mol % of acrylamide with 4 to 30 mol % of an alkyl or alkoxyalkyl, having not more than 4 carbon atoms, ester of acrylic acid, methacrylic acid, itaconic acid or maleic acid; then heating the emulsified dispersion to remove the organic solvent by distillation; and optionally finely wet-pulverizing the resulting aqueous dispersion to an extent that reduction in the average particle size of the developer dispersed in the dispersion does not exceed 10%. The recording paper is substantially improved in the developing density, developing velocity and printability.
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4.发明授权Color developer composition, process for preparing aqueous dispersion thereof and pressure sensitive manifold sheet using thereof 失效彩色显影剂组合物，其水分散体的制备方法和使用其的压力敏感性歧管片
公开(公告)号：US5250108A
公开(公告)日：1993-10-05
申请号：US679690
申请日：1991-04-01
CPC分类号： B41M5/155
摘要： The present invention provides a color developer composition characterized in that the composition contains a color developer comprising as its main component a nucleus-substituted salicylic acid salt represented by the formula (1) given below, and at least one amide compound selected from the group consisting of the compounds of represented by the formula (2) and formula (3) given below. ##STR1## wherein R.sub.1 to R.sub.10 are as defined in the specification.
摘要翻译： 本发明提供了一种彩色显影剂组合物，其特征在于该组合物含有着色显影剂，其包含以下述式（1）表示的核取代的水杨酸盐作为其主要成分，以及至少一种选自以下的酰胺化合物： 的由下式给出的式（2）和式（3）表示的化合物。 式（1）
式（2）其中R 1至R 10如说明书中所定义的式（3）。 -
公开(公告)号：US4688060A
公开(公告)日：1987-08-18
申请号：US826016
申请日：1986-02-04
申请人： Masato Tanaka , Shinsuke Irii , Tomoharu Shiozaki
发明人： Masato Tanaka , Shinsuke Irii , Tomoharu Shiozaki
摘要： Disclosed is a pressure sensitive manifold paper prepared by coating a substrate with a coating composition containing microcapsules of polyurethane resin or polyurea resin wall film and drying the resulting coating, the pressure sensitive manifold paper being characterized in that a latex of copolymer of comonomers comprising about 10 to about 50% by weight of styrene, about 15 to about 55% by weight of butadiene, about 10 to about 40% by weight of methyl methacrylate and up to about 15% by weight of acrylonitrile is incorporated in the coating composition in an amount of about 5 to about 30% by weight (calculated as solids) based on the microcapsules (calculated as solids).The pressure sensitive manifold paper has an adequate balance between the color forming ability and susceptibility to color smudges due to contact or friction.
摘要翻译： 公开了一种通过用包含聚氨酯树脂或聚脲树脂壁膜的微胶囊的涂料组合物涂覆基材并干燥所得涂层而制备的压敏集成纸，其特征在于包含约10个共聚单体的共聚单体的胶乳 至约50重量％的苯乙烯，约15至约55重量％的丁二烯，约10至约40重量％的甲基丙烯酸甲酯和至多约15重量％的丙烯腈，其量以 约5至约30重量％（以固体计算），基于微胶囊（以固体计算）。 压敏集成纸在成色能力和由于接触或摩擦引起的颜色污迹的易感性之间具有足够的平衡。
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公开(公告)号：US5393332A
公开(公告)日：1995-02-28
申请号：US164483
申请日：1993-12-09
CPC分类号： C07C51/15
摘要： Herein disclosed is a method for preparing a nuclear-substituted salicylic acid or a metal salt thereof represented by the following general formula (1): ##STR1## [wherein R.sub.1 and R.sub.2 each represents a t-butyl group, a t-amyl group, a t-octyl group, an isononyl group or an isododecyl group, provided that at least one of R.sub.1 and R.sub.2 represents an isononyl group or an isododecyl group; M represents a hydrogen atom or a metal atom; and n is the atomic valency of the metal atom M] which comprises the step of subjecting, to a Kolbe-Schmitt reaction, an alkali metal salt of a nuclear-substituted phenol represented by the following general formula (2): ##STR2## [wherein R.sub.1 and R.sub.2 are the same as those defined above] in which 100 to 50% of the alkali metal salt is potassium salt and 0 to 50% thereof is sodium salt, in a substantially water-insoluble solvent as a reaction medium. The method makes it possible to improve the yield of the specific nuclear-substituted salicylic acid and metal salts thereof and to provide such products having high purity without any post-treatment. The compounds can be used in color developers for pressure-sensitive recording sheets without any additional purification treatment.
摘要翻译： 本文公开了一种由以下通式（1）表示的核取代的水杨酸或其金属盐的制备方法：其中R1和R2各自表示叔丁基，t- 戊基，叔辛基，异壬基或异十二烷基，条件是R 1和R 2中的至少一个表示异壬基或异十二烷基; M表示氢原子或金属原子; 并且n是金属原子M的原子价，其包括以下通式（2）表示的核取代苯酚的碱金属盐进行Kolbe-Schmitt反应的步骤：＆lt; IMAGE＆gt; 2）[其中R1和R2与上述定义相同]，其中100〜50％的碱金属盐为钾盐，0〜50％为钠盐，在基本不溶于水的溶剂中作为反应介质 。 该方法可以提高特定的核取代的水杨酸及其金属盐的产率，并提供具有高纯度的这种产品，而不需要后处理。 这些化合物可以用于彩色显影剂，用于压敏记录片材，而无需任何额外的纯化处理。
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7.发明授权公开(公告)号：US11003124B2
公开(公告)日：2021-05-11
申请号：US16903734
申请日：2020-06-17
申请人： Masato Tanaka , Keiji Kunimi , Masaki Yoshino , Kazumi Suzuki
发明人： Masato Tanaka , Keiji Kunimi , Masaki Yoshino , Kazumi Suzuki
摘要： An image forming apparatus including an image forming unit, a fixing device, and circuitry is provided. The image forming unit is configured to perform a special image forming operation that forms a color toner image and a special toner image with a color toner and a special toner, respectively, on a recording medium and a normal image forming operation that forms the color toner image without forming the special toner image on the recording medium. The fixing device is configured to fix the color toner image and the special toner image on the recording medium. The circuitry is configured to perform, in the special image forming operation, a toner amount suppression control that makes an amount of the color toner on the recording medium per unit area smaller than that in the normal image forming operation.
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8.发明授权Electrophotographic photosensitive member, process cartridge and electrophotographic apparatus, and process for producing electrophotographic photosensitive member 有权电子照相感光构件，处理盒和电子照相设备，以及用于制造电子照相感光构件的方法公开(公告)号：US08865382B2
公开(公告)日：2014-10-21
申请号：US13102541
申请日：2011-05-06
申请人： Masaki Nonaka , Masato Tanaka
发明人： Masaki Nonaka , Masato Tanaka
CPC分类号： G03G5/0609 , G03G5/0542 , G03G5/0546 , G03G5/071 , G03G5/1473 , G03G5/14734 , G03G5/14786 , G03G5/14791 , G03G5/14795
摘要： An electrophotographic photosensitive member having a surface layer containing a polymeric product obtained by polymerizing a specific adamantane compound, a process cartridge and an electrophotographic apparatus which have the electrophotographic photosensitive member, and a process for producing the electrophotographic photosensitive member.
摘要翻译： 具有包含通过聚合特定金刚烷化合物获得的聚合物的表面层的电子照相感光构件，具有电子照相感光构件的处理盒和电子照相设备以及用于制造电子照相感光构件的方法。
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9.发明授权公开(公告)号：US08859174B2
公开(公告)日：2014-10-14
申请号：US13477876
申请日：2012-05-22
申请人： Masaki Nonaka , Masato Tanaka
发明人： Masaki Nonaka , Masato Tanaka
IPC分类号： G03G5/00
CPC分类号： G03G5/0575 , G03G5/0618 , G03G5/14769
摘要： An electrophotographic photosensitive member has a surface layer that contains a urea compound having two or more urea moieties. Each of the urea moieties has a carbonyl group and two nitrogen atoms. Each of the two nitrogen atoms connects to an alkyl group and a substituted or unsubstituted aryl group or a substituted or unsubstituted arylene group.
摘要翻译： 电子照相感光构件具有包含具有两个或更多个脲部分的脲化合物的表面层。 每个脲部分具有羰基和两个氮原子。 两个氮原子中的每一个连接到烷基和取代或未取代的芳基或取代或未取代的亚芳基。
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10.发明授权公开(公告)号：US08859172B2
公开(公告)日：2014-10-14
申请号：US13477561
申请日：2012-05-22
申请人： Hideaki Nagasaka , Masaki Nonaka , Masato Tanaka
发明人： Hideaki Nagasaka , Masaki Nonaka , Masato Tanaka
IPC分类号： G03G5/047
CPC分类号： G03G5/0517 , G03G5/0546 , G03G5/0592 , G03G5/0596 , G03G5/0614 , G03G5/071 , G03G5/14708 , G03G5/14734 , G03G5/14791
摘要： An electrophotographic photosensitive member has a surface layer that contains a polymer produced by the polymerization of a charge transporting substance having two or more methacryloyloxy groups per molecule. The surface layer contains a quinone derivative at a concentration of 5 ppm or more and 1500 ppm or less of the total mass of the polymer. The quinone derivative is a compound represented by the following formula (1) or a compound represented by the following formula (2) or both.
摘要翻译： 电子照相感光构件具有包含通过每分子具有两个以上甲基丙烯酰氧基的电荷输送物质的聚合而生成的聚合物的表面层。 表面层含有聚合物总质量为5ppm以上且1500ppm以下的醌衍生物。 醌衍生物是由下式（1）表示的化合物或由下式（2）表示的化合物或两者。
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