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1.发明授权公开(公告)号：US08834603B2
公开(公告)日：2014-09-16
申请号：US13579375
申请日：2011-02-14
申请人： Tue Johannessen , Johnny Johansen , Jacob Hjerrild Zeuthen , Henning Schmidt , Ulrich Joachim Quaade
发明人： Tue Johannessen , Johnny Johansen , Jacob Hjerrild Zeuthen , Henning Schmidt , Ulrich Joachim Quaade
CPC分类号： B01D53/9495 , C01C1/006 , F01N3/208 , F01N2610/02 , F01N2610/06 , F01N2610/10 , F01N2610/1406 , F01N2900/0408 , F01N2900/1808 , F01N2900/1811 , G01N7/16 , Y02A50/2325 , Y02T10/24
摘要： A method is provided for estimating the degree of saturation (S) of a reversible solid ammonia storage material (3) in a storage unit (1). The storage unit (1) is equipped with a heater (2) to release ammonia and a connected tube (4) for ammonia flow. The initial temperature (TINIT) is measured with a sensor (9) in or around the storage unit (1) before any heating is initiated. Heating is initiated while recording the active time of heating (t) or the amount of energy (Q) released by the heater. The desorption pressure created by solid storage material in the storage unit (1) is measured via a pressure sensor (8) in fluid communication with the storage unit (1). The time (tTARGET), or the heat (QTARGET) where the pressure reaches a certain target pressure (PTARGET) is recorded. The values of the target-pressure time (tTARGET), or the target-pressure heat (QTARGET), and the initial temperature (TINIT) are used to compute an approximate degree of saturation (S).
摘要翻译： 提供了一种用于估计存储单元（1）中的可逆固体氨储存材料（3）的饱和度（S）的方法。 存储单元（1）配备有用于释放氨的加热器（2）和用于氨流动的连接管（4）。 在开始任何加热之前，用存储单元（1）中或周围的传感器（9）测量初始温度（TINIT）。 在记录加热的活动时间（t）或由加热器释放的能量（Q）的量时开始加热。 通过与存储单元（1）流体连通的压力传感器（8）测量由储存单元（1）中的固体储存材料产生的解吸压力。 记录压力达到一定目标压力（PTARGET）的时间（tTARGET）或热量（QTARGET）。 使用目标压力时间（tTARGET）或目标压力热（QTARGET）和初始温度（TINIT）的值来计算近似饱和度（S）。
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2.发明申请METHOD FOR DETERMINING THE DEGREE OF SATURATION OF SOLID AMMONIA STORAGE MATERIALS IN CONTAINERS 有权用于确定容器中固体氨质储存材料饱和度的方法公开(公告)号：US20130209316A1
公开(公告)日：2013-08-15
申请号：US13579375
申请日：2011-02-14
申请人： Tue Johannessen , Johnny Johansen , Jacob Hjerrild Zeuthen , Henning Schmidt , Ulrich Joachim Quaade
发明人： Tue Johannessen , Johnny Johansen , Jacob Hjerrild Zeuthen , Henning Schmidt , Ulrich Joachim Quaade
CPC分类号： B01D53/9495 , C01C1/006 , F01N3/208 , F01N2610/02 , F01N2610/06 , F01N2610/10 , F01N2610/1406 , F01N2900/0408 , F01N2900/1808 , F01N2900/1811 , G01N7/16 , Y02A50/2325 , Y02T10/24
摘要： A method is provided for estimating the degree of saturation (S) of a reversible solid ammonia storage material (3) in a storage unit (1). The storage unit (1) is equipped with a heater (2) to release ammonia and a connected tube (4) for ammonia flow. The initial temperature (TINIT) is measured with a sensor (9) in or around the storage unit (1) before any heating is initiated. Heating is initiated while recording the active time of heating (t) or the amount of energy (Q) released by the heater. The desorption pressure created by solid storage material in the storage unit (1) is measured via a pressure sensor (8) in fluid communication with the storage unit (1). The time (tTARGET), or the heat (QTARGET) where the pressure reaches a certain target pressure (PTARGET) is recorded. The values of the target-pressure time (tTARGET), or the target-pressure heat (QTARGET), and the initial temperature (TINIT) are used to compute an approximate degree of saturation (S).
摘要翻译： 提供了一种用于估计存储单元（1）中的可逆固体氨储存材料（3）的饱和度（S）的方法。 存储单元（1）配备有用于释放氨的加热器（2）和用于氨流动的连接管（4）。 在开始任何加热之前，用存储单元（1）中或周围的传感器（9）测量初始温度（TINIT）。 在记录加热的活动时间（t）或由加热器释放的能量（Q）的量时开始加热。 通过与存储单元（1）流体连通的压力传感器（8）测量由储存单元（1）中的固体储存材料产生的解吸压力。 记录压力达到一定目标压力（PTARGET）的时间（tTARGET）或热量（QTARGET）。 使用目标压力时间（tTARGET）或目标压力热（QTARGET）和初始温度（TINIT）的值来计算近似饱和度（S）。
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3.发明授权Method and device for controlling effective heat transfer in a solid gas storage system 有权用于控制固体气体存储系统中有效传热的方法和装置公开(公告)号：US08931262B2
公开(公告)日：2015-01-13
申请号：US13634298
申请日：2011-03-16
IPC分类号： F01N3/00 , F01N3/10 , B01D53/02 , B01D53/12 , B65D85/00 , B65B3/00 , F01N3/20 , B01D53/04 , C01C1/00 , F17C11/00
CPC分类号： F01N3/208 , B01D53/0438 , B01D53/0454 , B01D2251/2062 , B01D2259/4525 , C01C1/006 , F17C11/00 , Y02P20/129
摘要： A method for controlling the effective heat transfer from a storage unit (1). During gas release from storage material (3) in the storage unit the storage material is heated by a heater (2). During re-saturation of the storage material (3) with gas the heater is off. Controlling of the effective heat transfer from the storage unit (1) is performed, during gas release, by ceasing convection of a convection gas and, during re-saturation, by performing or enabling convection of a convection gas to cool the storage unit (1).
摘要翻译： 一种用于控制来自存储单元（1）的有效热传递的方法。 在从存储单元中的储存材料（3）释放气体期间，储存材料由加热器（2）加热。 在用气体重新饱和存储材料（3）时，加热器关闭。 在气体释放期间，通过停止对流气体的对流并且在再饱和期间，通过执行或使对流气体对流以冷却存储单元（1）来控制来自存储单元（1）的有效热传递 ）。
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4.发明申请METHOD AND DEVICE FOR CONTROLLING EFFECTIVE HEAT TRANSFER IN A SOLID GAS STORAGE SYSTEM 有权用于控制固体气体储存系统中的有效热传递的方法和装置公开(公告)号：US20130118152A1
公开(公告)日：2013-05-16
申请号：US13634298
申请日：2011-03-16
CPC分类号： F01N3/208 , B01D53/0438 , B01D53/0454 , B01D2251/2062 , B01D2259/4525 , C01C1/006 , F17C11/00 , Y02P20/129
摘要： A method for controlling the effective heat transfer from a storage unit (1). During gas release from storage material (3) in the storage unit the storage material is heated by a heater (2). During re-saturation of the storage material (3) with gas the heater is off. Controlling of the effective heat transfer from the storage unit (1) is performed, during gas release, by ceasing convection of a convection gas and, during re-saturation, by performing or enabling convection of a convection gas to cool the storage unit (1).
摘要翻译： 一种用于控制来自存储单元（1）的有效热传递的方法。 在从存储单元中的储存材料（3）释放气体期间，储存材料由加热器（2）加热。 在用气体重新饱和存储材料（3）时，加热器关闭。 在气体释放期间，通过停止对流气体的对流并且在再饱和期间，通过执行或使对流气体对流以冷却存储单元（1）来控制来自存储单元（1）的有效热传递 ）。
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5.发明授权Method for saturating and re-saturating ammonia storage material in containers 有权将容器中的氨储存材料饱和并重新饱和的方法公开(公告)号：US08449857B2
公开(公告)日：2013-05-28
申请号：US12899667
申请日：2010-10-07
IPC分类号： F17C11/00
CPC分类号： B01D53/0454 , B01D53/0438 , B01D2257/406 , B01D2259/4525 , C01C1/006 , F17C11/00
摘要： A method for saturating or re-saturating ammonia storage material (1) capable of reversibly absorbing and desorbing ammonia in one or more storage containers (2), wherein said material is partly or fully depleted of ammonia, with ammonia to a predetermined saturation degree comprises a. placing the storage container(s) (2) in direct or indirect contact with a thermostatting medium (4) at a temperature level TT≦ about 65° C.; and b. connecting the storage container(s) (2) to a source of gaseous ammonia wherein at least during a part of the method the gaseous ammonia during saturating or re-saturation of the ammonia storage material (1) is at a pressure PS≦ about PT, wherein PS is the ammonia pressure during saturating or re-saturating of the ammonia storage material (1) and PT is the equilibrium vapor pressure of liquid ammonia at the temperature level TT.
摘要翻译： 一种用于使氨储存材料（1）饱和或再饱和的方法，其能够在一个或多个储存容器（2）中可逆地吸收和解吸氨，其中所述材料部分或全部耗尽氨，氨与预定的饱和度包括 一个。 将储存容器（2）放置在温度等级TT约为65℃的恒温培养基（4）中直接或间接接触; 和b。 将所述储存容器（2）连接到气态氨源，其中至少在所述方法的一部分期间，氨储存材料（1）的饱和或再饱和期间的气态氨处于约PT的压力 其中PS是在氨储存材料（1）的饱和或再饱和期间的氨压力，PT是在液温TT下液氨的平衡蒸气压。
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6.发明申请公开(公告)号：US20110284121A1
公开(公告)日：2011-11-24
申请号：US12899667
申请日：2010-10-07
IPC分类号： B65B31/00
CPC分类号： B01D53/0454 , B01D53/0438 , B01D2257/406 , B01D2259/4525 , C01C1/006 , F17C11/00
摘要： A method for saturating or re-saturating ammonia storage material (1) capable of reversibly absorbing and desorbing ammonia in one or more storage containers (2), wherein said material is partly or fully depleted of ammonia, with ammonia to a predetermined saturation degree comprises a. placing the storage container(s) (2) in direct or indirect contact with a thermostatting medium (4) at a temperature level TT≦ about 65° C.; and b. connecting the storage container(s) (2) to a source of gaseous ammonia wherein at least during a part of the method the gaseous ammonia during saturating or re-saturation of the ammonia storage material (1) is at a pressure PS≦ about PT, wherein PS is the ammonia pressure during saturating or re-saturating of the ammonia storage material (1) and PT is the equilibrium vapor pressure of liquid ammonia at the temperature level TT.
摘要翻译： 一种用于使氨储存材料（1）饱和或再饱和的方法，其能够在一个或多个储存容器（2）中可逆地吸收和解吸氨，其中所述材料部分或全部耗尽氨，氨与预定的饱和度包括 一个。 将储存容器（2）放置在温度等级TT＆amp; NlE下与恒温介质（4）直接或间接接触; 约65°C。 和b。 将所述储存容器（2）连接到气态氨源，其中至少在所述方法的一部分期间，所述氨储存材料（1）的饱和或再饱和期间的气态氨处于压力PS＆amp; 关于PT，其中PS是在氨储存材料（1）的饱和或再饱和期间的氨压力，PT是在温度水平TT下的液氨的平衡蒸气压。
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7.发明授权公开(公告)号：US08473226B2
公开(公告)日：2013-06-25
申请号：US12884527
申请日：2010-09-17
CPC分类号： H01M8/04208 , C01C1/006 , F01N3/2066 , F01N9/005 , F01N11/00 , F01N2550/05 , F01N2610/02 , F01N2610/06 , F01N2610/10 , F01N2900/1808 , F17C11/00 , Y02A50/2325
摘要： A method of determining an average degree of saturation with ammonia (X) of a solid ammonia storage medium porous or not and capable of ad- or absorbing and desorbing ammonia reversibly in a storage container is described. A part of the volume (Vcon) of the container is occupied by gaseous ammonia of a pressure (p) and defines a free volume (Vfree)). Ammonia flows out of the container with a flow (f). n pairs ((fi, pi), (Fi, pi)) of flows (fi), or accumulated flows (Fi), and pressures (pi) are sampled at a sequence of points of time (ti), i=1 . . . n and n≧2; an estimate volume value (Vfit) on the basis of the sampled pairs ((fi, pi), (Fi, pi)) is determined;and the degree of saturation with ammonia (X) is determined by applying a predetermined relationship (Rel) between a plurality of estimate volume values (Vfit) and a plurality of values of the average degree of saturation with ammonia (X) to the determined estimate volume value (Vfit).
摘要翻译： 描述了一种使用多孔或不多孔的固体氨储存介质用氨（X）确定平均饱和度的方法，其能够在储存容器中可逆地吸附或吸收和解吸氨。 容器的一部分体积（Vcon）由压力（p）的气态氨占据并限定自由体积（Vfree））。 氨以流（f）流出容器。 流（fi）或累积流（Fi）的n对（（fi，pi），（Fi，pi））或累积流（Fi），并且压力（pi）在时间点（ti），i = 1的序列被采样。 的。 的。 n和n> = 2; 确定基于采样对（（fi，pi），（Fi，pi））的估计体积值（Vfit） 并且通过将多个估计体积值（Vfit）和具有氨（X）的平均饱和度的多个值之间的预定关系（Rel）应用于所确定的估计来确定与氨（X）的饱和度 体积值（Vfit）。
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8.发明申请公开(公告)号：US20120072135A1
公开(公告)日：2012-03-22
申请号：US12884527
申请日：2010-09-17
IPC分类号： G01F23/14
CPC分类号： H01M8/04208 , C01C1/006 , F01N3/2066 , F01N9/005 , F01N11/00 , F01N2550/05 , F01N2610/02 , F01N2610/06 , F01N2610/10 , F01N2900/1808 , F17C11/00 , Y02A50/2325
摘要： A method of determining an average degree of saturation with ammonia (X) of a solid ammonia storage medium porous or not and capable of ad- or absorbing and desorbing ammonia reversibly in a storage container is described. A part of the volume (Vcon) of the container is occupied by gaseous ammonia of a pressure (p) and defines a free volume (Vfree)). Ammonia flows out of the container with a flow (f). n pairs ((fi, pi), (Fi, pi)) of flows (fi), or accumulated flows (Fi), and pressures (pi) are sampled at a sequence of points of time (ti), i=1 . . . n and n≧2; an estimate volume value (Vfit) on the basis of the sampled pairs ((fi, pi), (Fi, pi)) is determined;and the degree of saturation with ammonia (X) is determined by applying a predetermined relationship (Rel) between a plurality of estimate volume values (Vfit) and a plurality of values of the average degree of saturation with ammonia (X) to the determined estimate volume value (Vfit).
摘要翻译： 描述了一种使用多孔或不多孔的固体氨储存介质用氨（X）确定平均饱和度的方法，其能够在储存容器中可逆地吸附或吸收和解吸氨。 容器的一部分体积（Vcon）由压力（p）的气态氨占据并限定自由体积（Vfree））。 氨以流（f）流出容器。 流（fi）或累积流（Fi）的n对（（fi，pi），（Fi，pi））或累积流（Fi），并且压力（pi）在时间点（ti），i = 1的序列被采样。 。 。 n和n≥2; 确定基于采样对（（fi，pi），（Fi，pi））的估计体积值（Vfit） 并且通过将多个估计体积值（Vfit）和具有氨（X）的平均饱和度的多个值之间的预定关系（Rel）应用于所确定的估计来确定与氨（X）的饱和度 体积值（Vfit）。
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