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    Process for producing fluorinated organic compounds
    2.
    发明申请
    Process for producing fluorinated organic compounds 有权
    氟化有机化合物的制备方法

    公开(公告)号：US20130256588A1

    公开(公告)日：2013-10-03

    申请号：US13993154

    申请日：2011-12-16

    申请人： Vito Tortelli ,  Marco Galimberti ,  Cristiano Monzani ,  Piero Gavezotti

    发明人： Vito Tortelli ,  Marco Galimberti ,  Cristiano Monzani ,  Piero Gavezotti

    IPC分类号： C07C41/22 ,  C09K5/00

    CPC分类号： C07C41/22 ,  C07C41/48 ,  C08G65/007 ,  C08G65/3236 ,  C09K5/00 ,  C07C43/126 ,  C07C43/315

    摘要： A process for fluorinating hydrocarbon compounds, which comprises: A. providing a compound selected from the group consisting of straight-chain, branched-chain and cyclic alkanes, straight-chain, branched-chain and cyclic ethers, said compound comprising at least one carbon-hydrogen bond and being free from C(O)— functional groups; B. reacting said compound with fluorine in the presence of at least one (per)haloolefin comprising at least one carbon-carbon double bond and having at least one fluorine or chlorine atom on either one of the carbon atoms of said double bond, to obtain a compound wherein at least one carbon-hydrogen bond has been replaced by a carbon-fluorine bond. Compositions of partially fluorinated compounds obtained with the process are also disclosed.

    摘要翻译： 一种氟化烃化合物的方法，其包括：A.提供选自直链，支链和环烷烃，直链，支链和环醚的化合物，所述化合物包含至少一个碳 - 氢键并且不含C（O） - 官能团; 在至少一种包含至少一个碳 - 碳双键并且在所述双键的碳原子上具有至少一个氟或氯原子的（全）卤代烯烃存在下，使所述化合物与氟反应，得到 其中至少一个碳 - 氢键已被碳 - 氟键取代的化合物。 还公开了通过该方法获得的部分氟化化合物的组合物。

    HYDRO-FLUOROCOMPOUNDS
    6.
    发明申请
    HYDRO-FLUOROCOMPOUNDS 审中-公开
    氢氟化合物

    公开(公告)号：US20140350181A1

    公开(公告)日：2014-11-27

    申请号：US14118312

    申请日：2012-05-24

    申请人： Vito Tortelli ,  Ivan Wlassics ,  Cristiano Monzani ,  Bradley Lane Kent ,  Alessandro Veneroni

    发明人： Vito Tortelli ,  Ivan Wlassics ,  Cristiano Monzani ,  Bradley Lane Kent ,  Alessandro Veneroni

    IPC分类号： C07C59/135 ,  C08K3/20 ,  C07C51/377

    CPC分类号： C07C59/135 ,  C07C51/00 ,  C07C51/377 ,  C07C51/41 ,  C07C59/115 ,  C08K3/20

    摘要： The invention pertains to certain hydro-fluorocompounds of the following formula (I): RfO—RH—O—(CH2)m-[CF(X)n]—COOXa wherein: —Xa is H, a monovalent metal (preferably an alkaline metal) or an ammonium group of formula —N(R′n)4, wherein each of R′n, equal to or different from each other, independently represents a hydrogen atom or a C1-6 hydrocarbon group (preferably an alkyl group); —Rf is a C1-C6 (per)fluoroalkyl optionally comprising one or more catenary oxygen atoms, preferably Rf is a group of formula Rf—CH2—, wherein R′f is a C1-C5 perfluorinated group, possibly comprising one or more ethereal oxygens, preferably a C1-C3 perfluorinated group, possibly comprising one or more ethereal oxygens; —RH is a fluorine-free hydrocarbon group optionally comprising one or more catenary oxygen atoms; —X is F or CF3, preferably X is F; -m is 0 or 1; -n is 1 to 3, to a process for the manufacture of said hydro-fluorocompounds, to a method of making fluoropolymers in the presence of said hydro-fluorocompounds, and to fluoropolymer dispersions comprising said hydro-fluorocompound.

    摘要翻译： 本发明涉及以下式（I）的某些含氟化合物：RfO-RH-O-（CH2）m- [CF（X）n] -COOXa其中：-Xa为H，一价金属（优选碱 金属）或式-N（R'n）4的铵基，其中R'n彼此相同或不同，各自独立地表示氢原子或C1-6烃基（优选烷基） ; -R f是任选地包含一个或多个链状氧原子的C 1 -C 6（全）氟代烷基，优选Rf是式Rf-CH 2 - 的基团，其中R 1f是C 1 -C 5全氟化基团，可能包含一个或多个醚 氧，优选C1-C3全氟化基团，可能包含一个或多个醚类氧; -RH是任选地包含一个或多个链状氧原子的无氟烃基; -X是F或CF 3，优选X是F; -m为0或1; -n为1至3，涉及一种制备所述含氟化合物的方法，涉及一种在所述含氟化合物存在下制备含氟聚合物的方法，以及含有所述氢氟化合物的含氟聚合物分散体。

    Process for preparing dichlorofluoroacetyl halides
    8.
    发明授权
    Process for preparing dichlorofluoroacetyl halides 失效
    制备二氯氟乙酰卤的方法

    公开(公告)号：US6166252A

    公开(公告)日：2000-12-26

    申请号：US226121

    申请日：1999-01-07

    申请人： Piero Gavezotti ,  Julio A. Abusleme ,  Vito Tortelli

    发明人： Piero Gavezotti ,  Julio A. Abusleme ,  Vito Tortelli

    IPC分类号： B01J23/26 ,  C07B61/00 ,  C07C51/58 ,  C07C51/60 ,  C07C51/62 ,  C07C51/64 ,  C07C55/40 ,  C07C53/21

    CPC分类号： C07C51/60 ,  C07C51/62 ,  Y02P20/582 ,  C07C53/48

    摘要： Process for preparing dichlorofluoroacetylfluoride (CFCl.sub.2 COF) comprising the following steps:a) fluorination with hydrofluoric acid (HF) of the trichloroacetyl halide in a fixed or fluidized tubular bed reactor, filled with fluorination catalysts and having a temperature profile between the inlet of the reactants and the outlet of the reaction products, in the range from 175.degree. C. to 275.degree. C.b) distillation of the reaction products with trichloroacetylfluoride recycle and recovery of a mixture formed by HF and CFCl.sub.2 COF;c) separation of the HF/CFCl.sub.2 COF mixture components by cooling at temperatures lower than -10.degree. C., and optionally the HF recycle.

    摘要翻译： 制备二氯氟乙酰氟（CFCl2COF）的方法包括以下步骤：a）在固定或流化的管式床反应器中用三氟乙酰卤的氢氟酸（HF）氟化，填充氟化催化剂，并且在反应物入口和 反应产物的出口在175℃至275℃的范围内。b）用三氯乙酰氟循环蒸馏反应产物并回收由HF和CFCl 2 COF形成的混合物; c）通过在低于-10℃的温度下冷却并任选地HF再循环来分离HF / CFCl 2 COF混合物组分。