MULTIPLE SAMPLE DIFFERENTIAL SCANNING CALORIMETER

    公开(公告)号:US20200064209A1

    公开(公告)日:2020-02-27

    申请号:US16454951

    申请日:2019-06-27

    Inventor: Robert L. Danley

    Abstract: A heat flow rate measurement method for use with a differential scanning calorimeter sensor is provided. The method includes calculating a heat exchange between a plurality of sample containers and a reference container placed on a plurality of sample calorimeter units and a reference calorimeter unit, respectively, and determining a heat flow rate of samples within the sample containers using the calculated heat exchange between the plurality of sample containers and the reference container. A multiple sample differential scanning calorimeter sensor and calorimeter system are also provided.

    Multiple sample differential scanning calorimeter

    公开(公告)号:US11204289B2

    公开(公告)日:2021-12-21

    申请号:US16454951

    申请日:2019-06-27

    Inventor: Robert L. Danley

    Abstract: A heat flow rate measurement method for use with a differential scanning calorimeter sensor is provided. The method includes calculating a heat exchange between a plurality of sample containers and a reference container placed on a plurality of sample calorimeter units and a reference calorimeter unit, respectively, and determining a heat flow rate of samples within the sample containers using the calculated heat exchange between the plurality of sample containers and the reference container. A multiple sample differential scanning calorimeter sensor and calorimeter system are also provided.

    Multiple sample differential scanning calorimeter

    公开(公告)号:US11796399B2

    公开(公告)日:2023-10-24

    申请号:US17523667

    申请日:2021-11-10

    Inventor: Robert L. Danley

    CPC classification number: G01K17/00 G01K7/02 G01K19/00

    Abstract: A heat flow rate measurement method for use with a differential scanning calorimeter sensor is provided. The method includes calculating a heat exchange between a plurality of sample containers and a reference container placed on a plurality of sample calorimeter units and a reference calorimeter unit, respectively, and determining a heat flow rate of samples within the sample containers using the calculated heat exchange between the plurality of sample containers and the reference container. A multiple sample differential scanning calorimeter sensor and calorimeter system are also provided.

    MULTIPLE SAMPLE DIFFERENTIAL SCANNING CALORIMETER

    公开(公告)号:US20220065711A1

    公开(公告)日:2022-03-03

    申请号:US17523667

    申请日:2021-11-10

    Inventor: Robert L. Danley

    Abstract: A heat flow rate measurement method for use with a differential scanning calorimeter sensor is provided. The method includes calculating a heat exchange between a plurality of sample containers and a reference container placed on a plurality of sample calorimeter units and a reference calorimeter unit, respectively, and determining a heat flow rate of samples within the sample containers using the calculated heat exchange between the plurality of sample containers and the reference container. A multiple sample differential scanning calorimeter sensor and calorimeter system are also provided.

    Dynamic mechanical analyzer and sample fixtures for a dynamic mechanical analyzer

    公开(公告)号:US09933249B2

    公开(公告)日:2018-04-03

    申请号:US15104022

    申请日:2014-12-04

    Inventor: Robert L. Danley

    CPC classification number: G01B11/16 G01L1/2206 G01L3/101

    Abstract: A dynamic mechanical analyzer and a sample fixture for a dynamic mechanical analyzer that attaches fixed clamps in the sample fixture to a rigid frame using mounts that are compliant in the direction perpendicular to the sample displacement but which at the same time are resistant to rotation about the transverse direction of the sample. The compliant mounts include a pair of flexures that are attached to each fixed clamp and to the frame of the sample fixture. In an embodiment, the pair of flexures are thin flat members such that each pair constitutes two parallel leaf springs. The flexures flex to allow the fixed clamps to move perpendicularly to the sample displacement, but at the same time prevent rotation of the fixed clamps.

    Dynamic Mechanical Analyzer and Sample Fixtures For A Dynamic Mechanical Analyzer
    8.
    发明申请
    Dynamic Mechanical Analyzer and Sample Fixtures For A Dynamic Mechanical Analyzer 有权
    动态机械分析仪和动态机械分析仪的样品夹具

    公开(公告)号:US20160349041A1

    公开(公告)日:2016-12-01

    申请号:US15104022

    申请日:2014-12-04

    Inventor: Robert L. Danley

    CPC classification number: G01B11/16 G01L1/2206 G01L3/101

    Abstract: A dynamic mechanical analyzer and a sample fixture for a dynamic mechanical analyzer that attaches fixed clamps in the sample fixture to a rigid frame using mounts that are compliant in the direction perpendicular to the sample displacement but which at the same time are resistant to rotation about the transverse direction of the sample. The compliant mounts include a pair of flexures that are attached to each fixed clamp and to the frame of the sample fixture. In an embodiment, the pair of flexures are thin flat members such that each pair constitutes two parallel leaf springs. The flexures flex to allow the fixed clamps to move perpendicularly to the sample displacement, but at the same time prevent rotation of the fixed clamps.

    Abstract translation: 动态机械分析仪和用于动态机械分析仪的样品固定器,其将样品固定器中的固定夹具附接到刚性框架,其使用在垂直于样品位移的方向上顺应的安装件,但是同时抵抗围绕 样品的横向。 柔性安装件包括连接到每个固定夹具和样品夹具框架的一对挠曲件。 在一个实施例中,该对挠性件是薄平的构件,使得每一对构成两个平行的板簧。 弯曲部弯曲以允许固定夹具垂直于样品位移移动,但同时防止固定夹具旋转。

    QUASIADIABATIC DIFFERENTIAL SCANNING CALORIMETER
    9.
    发明申请
    QUASIADIABATIC DIFFERENTIAL SCANNING CALORIMETER 有权
    质谱差示扫描量热仪

    公开(公告)号:US20150253206A1

    公开(公告)日:2015-09-10

    申请号:US14425473

    申请日:2013-08-30

    Inventor: Robert L. Danley

    CPC classification number: G01K17/08 G01N25/20 G01N25/4833

    Abstract: A method of operating a differential scanning calorimeter wherein errors in the heat flow rate measurement are reduced by operating the calorimeter in a quasiadiabatic mode and by employing a heat flow rate measurement algorithm that includes the leakage heat flow rate. The temperature of the DSC enclosure is controlled independently of the temperature of the measuring system, which allows the temperature difference between the sample and reference containers and the enclosure to be minimized, thus minimizing leakage heat flow.

    Abstract translation: 一种操作差示扫描量热计的方法,其特征在于,通过在准半辐射模式下操作量热计,并采用包括泄漏热流量的热流量测量算法来降低热流量测量中的误差。 DSC外壳的温度独立于测量系统的温度进行控制,这样可以使样品和参考容器与外壳之间的温差最小化,从而将泄漏热流最小化。

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