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公开(公告)号：US4153608A
公开(公告)日：1979-05-08
申请号：US851308
申请日：1977-11-14
摘要： Anthraquinone dyestuffs of the general formula ##STR1## wherein IN EACH OF THE TWO ANTHRAQUINONE RADICALS SUBSTITUTED BY X, one X denotes chlorine and the other denotes hydrogen andR represents hydrogen or an optionally substituted benzoylamino group,And mixtures of the dyestuffs, in which the constituents of the mixture are 6-chloroanthraquinone and 7-chloroanthraquinone derivatives are suitable as a vat dyestuff for the dyeing of cotton in strong brown color shades with excellent fastness to light and vat processing.
摘要翻译： 通式（I）的蒽醌染料其中在由X取代的两个蒽醌基中的每一个，一个X表示氯，另一个表示氢，R表示氢或任选取代的苯甲酰基氨基，以及DYESTUFFS的混合物， 混合物为六氯代四氢呋喃和7-氯代四氢呋喃衍生物的组成可适用于在强烈的棕色色调中对棉花进行增白剂染色，具有极佳的轻度和增值加工性能。
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2.发明授权Process for producing 1,5-dinitroanthraquinone and 1,8-dinitroanthraquinone 失效1,5-二硝基蒽醌和1,8-二硝基蒽醌的制备方法
公开(公告)号：US3963762A
公开(公告)日：1976-06-15
申请号：US513907
申请日：1974-10-10
申请人： Walter Hohmann
发明人： Walter Hohmann
IPC分类号： C07C205/47 , C07C20060101 , C07C67/00 , C07C201/00 , C07C49/68
摘要： Substantially pure 1,5- and/or 1,8-dinitroanthraquinone is recovered from dinitration mixtures which may contain sulfuric acid or a perfluoralkane sulfonic acid by adjusting the nitric acid concentration in the nitration mixture to a value of 91 to 96% for a ratio by weight of nitric acid to solids of from 2.5 : 1 to 10 : 1; separating off the insoluble crude 1,5-dinitroanthranthraquinone at 15.degree. to 50.degree.C; taking up the 1,5-dinitroanthraquinone with 90 to 100% nitric acid in a ratio by weight of nitric acid to solids of from 0.5 : 1 to 3.5 : 1; stirring at 15.degree. to 80.degree. C; separating off the insoluble pure 1,5-dinitroanthraquinone thus obtained; adjusting the mother liquid left following separation of the crude 1,5-dinitroanthraquinone to a nitric acid concentration of from 88 to 94% for a ratio by weight of nitric acid to solids of from 3.0 : 1 to 12 : 1, with the proviso that the nitric acid concentration is at least 1.5% lower than in the preceding separation of crude 1,5-dinitroanthraquinone; and separating off the pure 1,8-dinitroanthraquinone obtained in this way at a temperature in the range of from 20.degree. to 50.degree.C and freeing it from the nitric acid adhering thereto.
摘要翻译： 通过将硝化混合物中的硝酸浓度调节至91至96％的比例，从可能含有硫酸或全氟烷基磺酸的二硝化混合物回收基本上纯的1,5-和/或1,8-二硝基蒽醌 的硝酸至2.5:1至10:1的固体; 在15〜50℃下分离不溶性粗制1,5-二硝基蒽醌; 以0.5：1至3.5：1的比例将硝酸与固体的重量比为90至100％硝酸1,5-二硝基蒽醌; 在15℃至80℃下搅拌; 分离得到的不溶性纯1,5-二硝基蒽醌; 在将粗制的1,5-二硝基蒽醌分离出硝酸浓度为88至94％，硝酸与固体的重量比为3.0:1至12:1之后留下的母体液体，条件是 硝酸浓度比原来的1,5-二硝基蒽醌分离低至少1.5％; 并将这样获得的纯的1,8-二硝基蒽醌分离出在20℃至50℃的温度范围内，并将其从附着于其上的硝酸释放出来。
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公开(公告)号：US4492790A
公开(公告)日：1985-01-08
申请号：US339943
申请日：1982-01-18
申请人： Walter Hohmann , Klaus Wunderlich
发明人： Walter Hohmann , Klaus Wunderlich
IPC分类号： C09B15/00 , C09B1/467 , C09B5/36 , C07D401/12 , C07D401/14
摘要： Vat dyestuffs containing at least 80% by weight of one or more of the compounds of the formula ##STR1## wherein A and B independently of one another represent --NHV, --NHW or --NHZ,in whichV represents a radical of the formula ##STR2## W represents a radical of the formula ##STR3## and Z represents a radical of the formula ##STR4## R.sub.1 and R.sub.2 denote hydrogen or acylamino, but do not simultaneously denote acylamino,Hal denotes a halogen atom andn denotes the numbers 0, 1 or 2,yield deep and light-fast dyeings on cellulose fibres.They are advantageously obtained by the stepwise condensation of cyanuric chloride with corresponding aminoanthraquinones in the presence of a phenol.
摘要翻译： 其中A和B彼此独立地表示-NHV，-NHW或-NHZ，其中V代表下式的基团： 图像W表示式“IMAGE”的基团，Z表示下式的基团R 1和R 2表示氢或酰氨基，但不同时表示酰氨基，Hal表示卤素原子，n表示数字0， 1或2，在纤维素纤维上产生深而轻的染色。 它们有利地通过在苯酚存在下通过氰尿酰氯与相应的氨基蒽醌的逐步缩合得到。
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公开(公告)号：US4408056A
公开(公告)日：1983-10-04
申请号：US454300
申请日：1982-12-29
申请人： Walter Hohmann , Josef Stawitz
发明人： Walter Hohmann , Josef Stawitz
摘要： Nitrotrianthrimidecarbazoles of the formula ##STR1## in which the NO.sub.2 group is in the .alpha.- or .beta.-position and R.sub.1, r.sub.2 ; R.sub.3 and R.sub.4 designate hydrogen or halogen such as chlorine and bromine,their use as vat dyestuffs, a process for their preparation, and the use, as vat dyestuffs, of compounds which in the formula (I) have an NH.sub.2 group in place of the NO.sub.2 group.
摘要翻译： 其中NO 2基团位于α位或β位且R1，r2中的式（I）所示的硝基三苯甲基咔唑： R3和R4表示氢或卤素如氯和溴，它们作为饮料染料的用途，它们的制备方法和用作大容量染料的式（I）中具有NH 2基团的化合物代替 NO2组。
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公开(公告)号：US4206130A
公开(公告)日：1980-06-03
申请号：US898262
申请日：1978-04-20
申请人： Helmut Herzog , Walter Hohmann , Helmut Seidler
发明人： Helmut Herzog , Walter Hohmann , Helmut Seidler
摘要： A process has been invented for the preparation of 1,5-dichloroanthraquinone which comprises reacting 1,5-dichloroanthraquinone with chlorine in the presence of at least 50% by weight of liquid phthalic anhydride, relative to the weight of 1,5-dinitroanthraquinone employed. The 1,5-dichloroanthraquinone is known to be a valuable starting material for the preparation of various dyestuffs.
摘要翻译： 已经发明了一种制备1,5-二氯蒽醌的方法，该方法包括在至少50重量％的液体邻苯二甲酸酐存在下使1,5-二氯蒽醌与氯反应，相对于所用的1,5-二硝基蒽醌的重量 。 已知1,5-二氯蒽醌是制备各种染料的有价值的起始原料。
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公开(公告)号：US3971812A
公开(公告)日：1976-07-27
申请号：US279756
申请日：1972-08-11
摘要： Compounds of formula ##SPC1##Wherein R.sub.1 and R.sub.2 independently of one another denote optionally substituted alkyl radicals with 1-3 C atoms and R.sub.3 represents hydrogen or an optionally substituted alkyl radical with 1-5 C atoms, as well as compounds of the formula ##SPC2##Wherein R.sub.4 represents an alkyl group which is optionally substituted by hydroxyl or alkoxy groups, and R.sub.5 and R.sub.6 represent hydrogen or an amino group which is monosubstituted or disubstituted by a straight-chain alkyl group or a cycloalkyl group, with the proviso that R.sub.5 and R.sub.6 do not simultaneously represent hydrogen, and processes for their production.
摘要翻译： 式WHEREIN R1和R2彼此独立地表示任选取代的具有1-3个C原子的烷基，R 3表示氢或任选取代的具有1-5个C原子的烷基，以及下式的化合物，其中R 4表示 任选被羟基或烷氧基取代的烷基，R 5和R 6表示氢或被直链烷基或环烷基单取代或二取代的氨基，条件是R 5和R 6不同时表示 氢气及其生产方法。
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公开(公告)号：US4210413A
公开(公告)日：1980-07-01
申请号：US891843
申请日：1978-03-30
申请人： Gunter Gehrke , Walter Hohmann
发明人： Gunter Gehrke , Walter Hohmann
CPC分类号： C09D11/037 , C09B1/515 , D06P5/006
摘要： Fabrics of synthetic fibres, preferably polyester fibres, can be printed in clear blue shades in accordance with the transfer printing principle if dyestuffs of the formula ##STR1## wherein R represents an alkyl radical with 2-6 C-atoms, are used.
摘要翻译： 使用合成纤维，优选聚酯纤维的织物，如果使用其中R表示2-6个C原子的烷基的式“IMAGE”的染料，则可根据转印原理印刷为透明的蓝色色调。
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公开(公告)号：US4155921A
公开(公告)日：1979-05-22
申请号：US850509
申请日：1977-11-10
申请人： Walter Hohmann , Klaus Wunderlich
发明人： Walter Hohmann , Klaus Wunderlich
IPC分类号： C07C205/47 , C07C67/00 , C07C201/00 , C07C201/16 , C07C49/68
CPC分类号： C07C201/16 , C07C205/47
摘要： A process has been invented for the isolation of 1,6- and 1,7-dinitroanthraquinone by treating mixtures containing these isomers with nitrobenzene.
摘要翻译： 已经发明了通过用硝基苯处理含有这些异构体的混合物来分离1,6-和1,7-二硝基蒽醌的方法。
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公开(公告)号：US4115412A
公开(公告)日：1978-09-19
申请号：US762479
申请日：1977-01-26
申请人： Walter Hohmann , Werner Kuhnel
发明人： Walter Hohmann , Werner Kuhnel
摘要： Use of the dyestuffs of the formula ##STR1## wherein R, Y and X have the meaning given in the description, for the dyeing of synthetic textiles, especially those of aromatic polyesters, by the transfer printing process.Prints obtained are distinguished by good fastness in use properties.
摘要翻译： 使用式“IMAGE”的染料，其中R，Y和X具有描述中给出的含义，用于通过转印印刷方法染色合成纺织品，特别是芳族聚酯的染料。
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公开(公告)号：US3980677A
公开(公告)日：1976-09-14
申请号：US614524
申请日：1975-09-18
摘要： Dyestuffs which contain sulphonic acid groups and correspond to the formula ##SPC1##In which R.sub.1 and R.sub.2 denote lower alkyl radicals with 1 - 3 carbon atoms, which may be substituted; A means an optionally substituted aliphatic, cycloaliphatic, araliphatic, aromatic or heterocyclic radical; n stands for 0, 1 or 2; and R.sub.4 denotes a sulphonic acid group when n = 0 and denotes hydrogen or a sulphonic acid when n = 1 or 2.The dyestuffs are eminently suitable for the dyeing and printing of natural and synthetic polyamide fiber materials.
摘要翻译： 含有磺酸基团并符合下式的染料：其中R 1和R 2表示可被取代的具有1-3个碳原子的低级烷基; A表示任选取代的脂族，脂环族，芳脂族，芳族或杂环基; n代表0,1或2; 当n = 0时，R 4表示磺酸基，当n = 1或2时，表示氢或磺酸。
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