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    Multifunctional Hyperbranched Organic Intercalating Agent, Method for Its Manufacture and Its Use
    1.
    发明申请
    Multifunctional Hyperbranched Organic Intercalating Agent, Method for Its Manufacture and Its Use 有权
    多功能超支化有机插层剂，其制造方法及其应用

    公开(公告)号：US20140171590A1

    公开(公告)日：2014-06-19

    申请号：US13714150

    申请日：2012-12-13

    申请人： Wen-Chiung Su ,  Ru-Jong Jeng ,  Tzong-Yuan Juang ,  Shi-Min Shau ,  Guan-Liang Chen ,  Han-Sheng Lin

    发明人： Wen-Chiung Su ,  Ru-Jong Jeng ,  Tzong-Yuan Juang ,  Shi-Min Shau ,  Guan-Liang Chen ,  Han-Sheng Lin

    IPC分类号： C08G69/40 ,  C08K3/20

    CPC分类号： C08G69/40 ,  C01B32/20 ,  C08G73/1032 ,  C08G73/1046 ,  C08G73/1075 ,  C08G73/1082 ,  C08K3/20 ,  C08K9/04 ,  C08K9/12

    摘要： A facile synthesis of amphiphilic hyperbranched polymers consisting of poly(amic acid) and polyimide was developed via “A2+B3” approach from difunctional anhydride and trifunctional hydrophilic poly(oxyalkylene)triamine. Various amphiphilic hyperbranched poly(amic acid)s (HBPAAs) with terminal amine functionalities and amic acid structures were prepared through ring-opening polyaddition at room temperature, followed by thermal imidization process for the formation of hyperbranched polyimides (HBPIs), accordingly. The resulting HBPIs were analyzed by GPC, indicating the molecule weights of 5000˜7000 g/mol with a distribution of polydispersity between 2.0 and 3.8. The amine titration for HBPIs indicated the peripheral total-amine contents to be 8.32˜18.32 mequiv/g dependent on compositions.

    摘要翻译： 通过“A2 + B3”方法从双官能酐和三官能亲水性聚（氧化烯）三胺开发了由聚（酰胺酸）和聚酰亚胺组成的两亲性超支化聚合物的容易合成。 通过在室温下开环加聚制备了具有末端胺官能团和酰胺酸结构的各种两亲性超支化聚（酰胺酸）（HBPAA），然后进行用于形成超支化聚酰亚胺（HBPI）的热酰亚胺化方法。 通过GPC分析所得到的HBPI，表明分子量为5000〜7000g / mol，多分散性分布在2.0〜3.8之间。 HBPI的胺滴定表明，根据成分，外周总胺含量为8.32〜18.32mequiv / g。

    Method for Making Waterborne Polyurethane with a Reactive Functional Group and a Nanocomposite Made of the Same
    2.
    发明申请
    Method for Making Waterborne Polyurethane with a Reactive Functional Group and a Nanocomposite Made of the Same 审中-公开
    制备具有活性官能团的水性聚氨酯和由其制成的纳米复合材料的方法

    公开(公告)号：US20130131301A1

    公开(公告)日：2013-05-23

    申请号：US13420511

    申请日：2012-03-14

    申请人： Wen-Chiung Su ,  Shi-Min Shau ,  Sheng-hong Dai ,  Ru-Jong Jeng

    发明人： Wen-Chiung Su ,  Shi-Min Shau ,  Sheng-hong Dai ,  Ru-Jong Jeng

    IPC分类号： C08G18/32

    CPC分类号： C08G18/4854 ,  C08G18/0823 ,  C08G18/10 ,  C08G18/348 ,  C08G18/4238 ,  C08G18/6659 ,  C08G18/6692 ,  C08G18/755 ,  C08G18/7664 ,  C08G18/8041 ,  C08K3/346 ,  C08K9/04 ,  C08L75/04 ,  C08G18/3206 ,  C08G18/3228

    摘要： Disclosed is a method for making waterborne polyurethane with a reactive functional group. The method includes the step of introducing a short-chain diol monomer with a reactive functional group into waterborne polyurethane polymer by pre-polymerization to provide a polyurethane pre-polymer with the reactive functional group connected to a side chain and the step of reacting the pre-polymer with hydrophilic diamine for chain extension and inter-crosslink to provide waterborne polyurethane with different crosslink degree. The short-chain diol monomer is expressed by structural formula (I) and the polyurethane pre-polymer with the reactive functional group connected to the side chain is expressed by structural formula (II) as follows: A is azetidine-2,4-dione functional group  or malonamide-linked alkyl group  and B is nitrogen-linked di-hydroxy terminal group  or tertiary amine-linked di-hydroxy terminal group  R1 is diisocyanate, and R2 is a polyol backbone and wherein IG is a neutralized ionic group.

    摘要翻译： 公开了制备具有反应性官能团的水性聚氨酯的方法。 该方法包括通过预聚合将具有反应性官能团的短链二醇单体引入水性聚氨酯聚合物的步骤，以提供具有与侧链连接的反应性官能团的聚氨酯预聚物和使前体 聚合物与亲水二胺用于链延伸和交联，以提供具有不同交联度的水性聚氨酯。 短链二醇单体由结构式（I）表示，具有与侧链连接的反应性官能团的聚氨酯预聚物由结构式（II）表示如下：A是氮杂环丁烷-2,4-二酮 官能团或丙二酰胺连接的烷基，B是氮连接的二羟基端基或叔胺连接的二羟基端基R1是二异氰酸酯，R2是多元醇主链，其中IG是中和的离子基团。

    Organic polyurethane shape memory material and a preparation method thereof
    5.
    发明授权
    Organic polyurethane shape memory material and a preparation method thereof 有权
    有机聚氨酯形状记忆材料及其制备方法

    公开(公告)号：US08318889B2

    公开(公告)日：2012-11-27

    申请号：US11889867

    申请日：2007-08-17

    申请人： Wen-Chiung Su ,  Cheng-Che Tsai ,  Ching-Shiang Yu ,  Shenghong A Dai ,  Ru-Jong Jeng

    发明人： Wen-Chiung Su ,  Cheng-Che Tsai ,  Ching-Shiang Yu ,  Shenghong A Dai ,  Ru-Jong Jeng

    IPC分类号： C08G18/00

    CPC分类号： C08G18/4277 ,  C08G18/2825 ,  C08G18/3275 ,  C08G18/714 ,  C08G18/7671 ,  C08G83/003 ,  C08G2280/00

    摘要： An organic polyurethane shape memory material includes a C10 chain or C18 chain and consists of hard segment and soft segment. The material is produced by reacting the single-chain type dendrimer with diethylenetriamine to produce dendrimer. Then dendrimer reacts with N-(3-aminopropyl)diethanolamine to produce dendritic diols. Next, polymer HO(C6H10O2)xC2H4OC2H4(C6H10O2)yOH, where x+y=25˜26, reacts with methylenedi-p-phenyl diisocyanate, and at least one type of dendritic diols is added to produce the organic polyurethane shape memory material.

    摘要翻译： 有机聚氨酯形状记忆材料包括C10链或C18链，由硬链段和软链段组成。 该材料通过使单链型树枝状聚合物与二亚乙基三胺反应制备树枝状聚合物而制备。 然后树枝状大分子与N-（3-氨基丙基）二乙醇胺反应产生枝状二醇。 接下来，将聚合物HO（C6H10O2）xC2H4OC2H4（C6H10O2）yOH（其中x + y = 25〜26）与亚甲基二苯基二异氰酸酯反应，并加入至少一种类型的树枝状二醇以制备有机聚氨酯形状记忆材料。

    Organic polyurethane shape memory material and a preparation method thereof
    8.
    发明申请
    Organic polyurethane shape memory material and a preparation method thereof 有权
    有机聚氨酯形状记忆材料及其制备方法

    公开(公告)号：US20090048418A1

    公开(公告)日：2009-02-19

    申请号：US11889867

    申请日：2007-08-17

    申请人： Wen-Chiung Su ,  Cheng-Che Tsai ,  Ching-Shiang Yu ,  Shenghong A. Dai ,  Ru-jong Jeng

    发明人： Wen-Chiung Su ,  Cheng-Che Tsai ,  Ching-Shiang Yu ,  Shenghong A. Dai ,  Ru-jong Jeng

    IPC分类号： C08G18/72 ,  C08G18/18

    CPC分类号： C08G18/4277 ,  C08G18/2825 ,  C08G18/3275 ,  C08G18/714 ,  C08G18/7671 ,  C08G83/003 ,  C08G2280/00

    摘要： An organic polyurethane shape memory material and a preparation method thereof are disclosed. The organic polyurethane shape memory material includes a C10 chain or C18 chain and it consists of hard segment and soft segment. The preparation method thereof includes the steps of:The single-chain type dendrimer reacts with diethylenetriamine to produce multiple chains type dendrimer. And then at least one type dendrimer reacts with N-(3-aminopropyl)diethanolamine to produce at least one type dendritic diols. Next polymer HO(C6H10O2)xC2H4OC2H4(C6H10O2)yOH, x+y=25˜26 reacts with methylenedi-p-phenyl diisocyanate and then at least one type dendritic diols is added to react so as to get organic polyurethane shape memory material. The material of the present invention overcomes shortcoming of metal alloy and ceramic such as poor processability, difficulty in modification and high cost. Moreover, it also increase mechanical properties of polymer.

    摘要翻译： 公开了一种有机聚氨酯形状记忆材料及其制备方法。 有机聚氨酯形状记忆材料包括C10链或C18链，它由硬链段和软链段组成。 其制备方法包括以下步骤：单链型树枝状聚合物与二亚乙基三胺反应产生多链型树枝状聚合物。 然后至少一种类型的树枝状大分子与N-（3-氨基丙基）二乙醇胺反应以产生至少一种类型的树枝状二醇。 下一个聚合物HO（C6H10O2）xC2H4OC2H4（C6H10O2）yOH，x + y = 25〜26与亚甲基二苯基二异氰酸酯反应，然后加入至少一种类型的枝状二醇进行反应，得到有机聚氨酯形状记忆材料。 本发明的材料克服了金属合金和陶瓷的缺点，如加工性差，改性困难，成本高等问题。 此外，它还增加了聚合物的机械性能。

    Method for preparing a biphenylphosphonate compound
    9.
    发明授权
    Method for preparing a biphenylphosphonate compound 有权
    联苯膦酸盐化合物的制备方法

    公开(公告)号：US07626051B2

    公开(公告)日：2009-12-01

    申请号：US11797936

    申请日：2007-05-09

    申请人： Wen-Chiung Su ,  Chin-Shang Sheng

    发明人： Wen-Chiung Su ,  Chin-Shang Sheng

    IPC分类号： C07F9/02

    CPC分类号： C07F9/657163

    摘要： A method for preparing a biphenylphosphonate compound of the following formula (I): wherein n is 2 or 3; Ar is a C6-C16 aromatic group; which comprising (a) reacting an o-phenylphenol with a phosphorus trichloride in the presence of a zinc chloride catalyst to form a 6-chloro-6H-dibenz [c,e] [1,2]oxaphosphorin of the following formula (II); (b) reacting a polyhydroxybenzene compound of the formula (III) (HO)n—Ar  (III) wherein n and Ar are defined the same as the above, with the compound of formula (II) to form a compound of the following formula (IV) wherein n and Ar are defined the same as the above; and (c) oxidizing the compound of formula (IV) in the presence of water and ozone to form the compound of formula (I).

    摘要翻译： 一种制备下式（I）的联苯膦酸酯化合物的方法：其中n为2或3; Ar为C6-C16芳族基团; 其包括（a）在氯化锌催化剂存在下使邻苯基苯酚与三氯化磷反应以形成下式（II）的6-氯-6H-二苯并[c，e] [1,2]氧杂磷杂环戊烯， ; （b）使式（III）（HO）n -Ar（III）的多羟基苯化合物（其中n和Ar与上述定义相同）与式（II）化合物反应，形成下式的化合物 （IV）其中n和Ar的定义与上述相同; 和（c）在水和臭氧存在下氧化式（Ⅳ）化合物以形成式（I）化合物。

    Method for preparing a biphenylphosphonate compound
    10.
    发明授权
    Method for preparing a biphenylphosphonate compound 有权
    联苯膦酸盐化合物的制备方法

    公开(公告)号：US07232921B2

    公开(公告)日：2007-06-19

    申请号：US10972396

    申请日：2004-10-26

    申请人： Wen-Chiung Su ,  Chin-Shang Sheng

    发明人： Wen-Chiung Su ,  Chin-Shang Sheng

    IPC分类号： C07F9/02

    CPC分类号： C07F9/657163

    摘要： A method for preparing a biphenylphosphonate compound of the following formula (I): wherein n is 2 or 3; Ar is a C6–C16 aromatic group; which comprising (a) reacting an o-phenylphenol with a phosphorus trichloride in the presence of a zinc chloride catalyst to form a 6-chloro-6H-dibenz [c,e][1,2] oxaphosphorin of the following formula (II); (b) reacting a polyhydroxybenzene compound of the formula (III) (HO)n—Ar   (III) wherein n and Ar are defined the same as the above, with the compound of formula (II) to form a compound of the following formula (IV) wherein n and Ar are defined the same as the above; and (c) oxidizing the compound of formula (IV) in the presence of water and ozone to form the compound of formula (I).

    摘要翻译： 一种制备下式（I）的联苯膦酸酯化合物的方法：其中n为2或3; Ar是C 6 -C 16芳基; 其包括（a）在氯化锌催化剂存在下使邻苯基苯酚与三氯化磷反应以形成下式（II）的6-氯-6H-二苯并[c，e] [1,2]氧杂磷杂环戊烯， ; （b）使式（III）的多羟基苯化合物<？in-line-formula description =“In-line Formulas”end =“lead”→（HO）n -Ar（III ）其中n和Ar与上述定义相同，与式（II）的化合物反应形成下列化合物： 式（Ⅳ）其中n和Ar定义与上述相同; 和（c）在水和臭氧存在下氧化式（Ⅳ）化合物以形成式（I）化合物。