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    PROCESS FOR THE PREPARATION OF DOPO-DERIVED COMPOUNDS AND COMPOSITIONS THEREOF
    6.
    发明申请
    PROCESS FOR THE PREPARATION OF DOPO-DERIVED COMPOUNDS AND COMPOSITIONS THEREOF 审中-公开
    制备DOPO衍生化合物及其组合物的方法

    公开(公告)号：US20150126762A1

    公开(公告)日：2015-05-07

    申请号：US14594703

    申请日：2015-01-12

    申请人： ALBEMARLE CORPORATION

    发明人： Qiang Yao ,  Junuzo Wang ,  Arthur G. Mack

    IPC分类号： C07F9/6574 ,  C08K5/5313

    CPC分类号： C07F9/657163 ,  B01J27/138 ,  B01J31/0225 ,  C07B2200/07 ,  C07F9/657172 ,  C07F9/65746 ,  C08K5/5313

    摘要： This invention relates to a process for producing compounds derived from 9,10-Dihydro-9-Oxa-10-Phosphaphenantrene-10-oxide (DOPO). In particular, the invention relates to producing DOPO-derived compounds by reacting DOPO with diol compounds in the presence of a catalyst. This invention also relates to DOPO derived composition containing a high melting point diastereomer. The DOPO derived compounds may be useful as flame-retardants.

    摘要翻译： 本发明涉及一种生产衍生自9,10-二氢-9-氧杂-10-磷杂蒽-10-氧化物（DOPO）的化合物的方法。 特别地，本发明涉及通过在催化剂存在下使DOPO与二醇化合物反应制备DOPO衍生的化合物。 本发明还涉及含有高熔点非对映异构体的DOPO衍生组合物。 DOPO衍生的化合物可用作阻燃剂。

    Method for preparing a biphenylphosphonate compound
    8.
    发明授权
    Method for preparing a biphenylphosphonate compound 有权
    联苯膦酸盐化合物的制备方法

    公开(公告)号：US07626051B2

    公开(公告)日：2009-12-01

    申请号：US11797936

    申请日：2007-05-09

    申请人： Wen-Chiung Su ,  Chin-Shang Sheng

    发明人： Wen-Chiung Su ,  Chin-Shang Sheng

    IPC分类号： C07F9/02

    CPC分类号： C07F9/657163

    摘要： A method for preparing a biphenylphosphonate compound of the following formula (I): wherein n is 2 or 3; Ar is a C6-C16 aromatic group; which comprising (a) reacting an o-phenylphenol with a phosphorus trichloride in the presence of a zinc chloride catalyst to form a 6-chloro-6H-dibenz [c,e] [1,2]oxaphosphorin of the following formula (II); (b) reacting a polyhydroxybenzene compound of the formula (III) (HO)n—Ar  (III) wherein n and Ar are defined the same as the above, with the compound of formula (II) to form a compound of the following formula (IV) wherein n and Ar are defined the same as the above; and (c) oxidizing the compound of formula (IV) in the presence of water and ozone to form the compound of formula (I).

    摘要翻译： 一种制备下式（I）的联苯膦酸酯化合物的方法：其中n为2或3; Ar为C6-C16芳族基团; 其包括（a）在氯化锌催化剂存在下使邻苯基苯酚与三氯化磷反应以形成下式（II）的6-氯-6H-二苯并[c，e] [1,2]氧杂磷杂环戊烯， ; （b）使式（III）（HO）n -Ar（III）的多羟基苯化合物（其中n和Ar与上述定义相同）与式（II）化合物反应，形成下式的化合物 （IV）其中n和Ar的定义与上述相同; 和（c）在水和臭氧存在下氧化式（Ⅳ）化合物以形成式（I）化合物。

    Method for preparing a biphenylphosphonate compound
    9.
    发明授权
    Method for preparing a biphenylphosphonate compound 有权
    联苯膦酸盐化合物的制备方法

    公开(公告)号：US07232921B2

    公开(公告)日：2007-06-19

    申请号：US10972396

    申请日：2004-10-26

    申请人： Wen-Chiung Su ,  Chin-Shang Sheng

    发明人： Wen-Chiung Su ,  Chin-Shang Sheng

    IPC分类号： C07F9/02

    CPC分类号： C07F9/657163

    摘要： A method for preparing a biphenylphosphonate compound of the following formula (I): wherein n is 2 or 3; Ar is a C6–C16 aromatic group; which comprising (a) reacting an o-phenylphenol with a phosphorus trichloride in the presence of a zinc chloride catalyst to form a 6-chloro-6H-dibenz [c,e][1,2] oxaphosphorin of the following formula (II); (b) reacting a polyhydroxybenzene compound of the formula (III) (HO)n—Ar   (III) wherein n and Ar are defined the same as the above, with the compound of formula (II) to form a compound of the following formula (IV) wherein n and Ar are defined the same as the above; and (c) oxidizing the compound of formula (IV) in the presence of water and ozone to form the compound of formula (I).

    摘要翻译： 一种制备下式（I）的联苯膦酸酯化合物的方法：其中n为2或3; Ar是C 6 -C 16芳基; 其包括（a）在氯化锌催化剂存在下使邻苯基苯酚与三氯化磷反应以形成下式（II）的6-氯-6H-二苯并[c，e] [1,2]氧杂磷杂环戊烯， ; （b）使式（III）的多羟基苯化合物<？in-line-formula description =“In-line Formulas”end =“lead”→（HO）n -Ar（III ）其中n和Ar与上述定义相同，与式（II）的化合物反应形成下列化合物： 式（Ⅳ）其中n和Ar定义与上述相同; 和（c）在水和臭氧存在下氧化式（Ⅳ）化合物以形成式（I）化合物。