公开(公告)号：US06743835B2

公开(公告)日：2004-06-01

申请号：US10006962

申请日：2001-12-05

申请人： Werner Schäfer ,  Manfred Scheiba ,  Stefan Stadtmüller ,  Markus Weimann ,  Karlheinz Rümpler ,  Ulrich Walter

发明人： Werner Schäfer ,  Manfred Scheiba ,  Stefan Stadtmüller ,  Markus Weimann ,  Karlheinz Rümpler ,  Ulrich Walter

IPC分类号： C08L302

CPC分类号： C09B67/0095 ,  C08J3/226 ,  C09B67/0003 ,  C09B67/0094

摘要： The invention relates to a process for preparing nondusting free-flowing pigment concentrates with removal of the water from pigment suspensions comprising polymers and dispersants in a fluidized bed drier. The resulting bead-form pigment concentrates are nondusting and readily free-flowing. The invention further embraces the use of pigment concentrates prepared in this way for coloring plastics and polymers.

摘要翻译： 本发明涉及一种在流化床干燥器中从包含聚合物和分散剂的颜料悬浮液中除去水的非阻燃自由流动颜料浓缩物的方法。 所得到的珠粒状颜料浓缩物是无污染的并且容易自由流动。 本发明还包括以这种方式制备的颜料浓缩物用于着色塑料和聚合物的用途。

公开(公告)号：US20110228628A1

公开(公告)日：2011-09-22

申请号：US13063575

申请日：2009-06-20

申请人： Michael Jacob ,  Karlheinz Rümpler ,  Frank Ohlendorf ,  Tilo Klöppel

发明人： Michael Jacob ,  Karlheinz Rümpler ,  Frank Ohlendorf ,  Tilo Klöppel

IPC分类号： B01J2/16 ,  B01F13/02

CPC分类号： B01J2/16

摘要： A method and an associated apparatus for treating fine-grained material in a spouted bed. Here, the method and design for an associated apparatus for treating fine-grained material in a spouted bed eliminate the drawbacks of the prior art, allow different process conditions in the process chamber to be adjusted in a regulated manner, and has a simple and inexpensive structure. The method is provides that a nearly circular gas flow of the fluidizer is generated in the process chamber (5) by an external annular gap (7) lying on the y-z plane, the diameter of the nearly circular gas flow expands outward in the direction of the x axis inside the process chamber (5), and a nearly circular gas flow of the fluidizer is generated by an internal annular gap (8) lying on the y-z plane, the diameter of the nearly circular gas flow expands inward within the process chamber (5). A displacement member (2) and an annular central contour (9) are centrally disposed in the lower region of the process chamber (5) in such a way that an internal annular gap (7) is formed between the displacement member (2) and the inner contour of the annular central contour (9), while an external annular gap (8) is formed between the outer contour of the annular central contour (9) and the lower outer edge of the process chamber (5) in order to feed the fluidizer.

摘要翻译： 一种用于在喷射床中处理细粒材料的方法和相关设备。 这里，用于处理喷射床中的细粒材料的相关设备的方法和设计消除了现有技术的缺点，允许处理室中的不同工艺条件以调节的方式调节，并且具有简单且便宜 结构体。 该方法规定，通过位于yz平面上的外部环形间隙（7）在处理室（5）中产生流化器的几乎圆形的气体流，几乎圆形的气体流的直径沿着 处理室（5）内的x轴，并且通过位于yz平面上的内部环形间隙（8）产生流化器的近似圆形的气体流，几乎圆形的气体流的直径在处理室内向内膨胀 （5）。 位移构件（2）和环形中心轮廓（9）以处理室（5）的下部区域中心地设置，使得内部环形间隙（7）形成在位移构件（2）和 环形中心轮廓（9）的内部轮廓，而在环形中心轮廓（9）的外部轮廓和处理室（5）的下部外边缘之间形成外部环形间隙（8），以便进给 流化器。

公开(公告)号：US09079147B2

公开(公告)日：2015-07-14

申请号：US13063575

申请日：2009-06-20

申请人： Michael Jacob ,  Karlheinz Rümpler ,  Frank Ohlendorf ,  Tilo Klöppel

发明人： Michael Jacob ,  Karlheinz Rümpler ,  Frank Ohlendorf ,  Tilo Klöppel

IPC分类号： B01F13/02 ,  B01J2/16

CPC分类号： B01J2/16

摘要： A method and an associated apparatus for treating fine-grained material in a spouted bed. Here, the method and design for an associated apparatus for treating fine-grained material in a spouted bed eliminate the drawbacks of the prior art, allow different process conditions in the process chamber to be adjusted in a regulated manner, and has a simple and inexpensive structure. The method is provides that a nearly circular gas flow of the fluidizer is generated in the process chamber (5) by an external annular gap (7) lying on the y-z plane, the diameter of the nearly circular gas flow expands outward in the direction of the x axis inside the process chamber (5), and a nearly circular gas flow of the fluidizer is generated by an internal annular gap (8) lying on the y-z plane, the diameter of the nearly circular gas flow expands inward within the process chamber (5). A displacement member (2) and an annular central contour (9) are centrally disposed in the lower region of the process chamber (5) in such a way that an internal annular gap (7) is formed between the displacement member (2) and the inner contour of the annular central contour (9), while an external annular gap (8) is formed between the outer contour of the annular central contour (9) and the lower outer edge of the process chamber (5) in order to feed the fluidizer.

摘要翻译： 一种用于在喷射床中处理细粒材料的方法和相关设备。 这里，用于处理喷射床中的细粒材料的相关设备的方法和设计消除了现有技术的缺点，允许处理室中的不同工艺条件以调节的方式调节，并且具有简单且便宜 结构体。 该方法规定，通过位于yz平面上的外部环形间隙（7）在处理室（5）中产生流化器的几乎圆形的气体流，几乎圆形的气体流的直径沿着 处理室（5）内的x轴，并且通过位于yz平面上的内部环形间隙（8）产生流化器的近似圆形的气体流，几乎圆形的气体流的直径在处理室内向内膨胀 （5）。 位移构件（2）和环形中心轮廓（9）以处理室（5）的下部区域中心地设置，使得内部环形间隙（7）形成在位移构件（2）和 环形中心轮廓（9）的内部轮廓，而在环形中心轮廓（9）的外部轮廓和处理室（5）的下部外边缘之间形成外部环形间隙（8），以便进给 流化器。

公开(公告)号：US08231938B2

公开(公告)日：2012-07-31

申请号：US10560372

申请日：2004-05-26

申请人： Karlheinz Rümpler ,  Michael Jacob ,  Mike Waskow

发明人： Karlheinz Rümpler ,  Michael Jacob ,  Mike Waskow

IPC分类号： B05D7/00

CPC分类号： C12N9/98 ,  A23K20/189 ,  A23K40/10 ,  A23L29/06 ,  A23P10/22 ,  A61K9/1688 ,  B01J2/16 ,  C12N9/16

摘要： A method of producing enzyme granulates, enzyme granulates produced By the method, and the use thereof in formulations is provided, for example, for animal feed, foodstuffs, washing agents, rinsing agents or for pharmaceutical uses. The enzyme granulates have a high relative proportion of active enzyme, particular particle size, good shelf life, particularly small rounding factors and/or low residual moisture proportion, and further specific properties. The production of the enzyme granulates is achieved by linking of the thermal conditions in the injection zone and temperature conditions in the remainder of the apparatus. This is achieved by introduction of heated process gasses for drying exclusively in the injection zone. The secure introduction of articles into the injection zone is achieved by the specific geometric arrangement of the apparatus using gravity. The absolute value for enzyme activity of the enzyme granulates can be controlled by the addition of particles as seed material for the granules.

摘要翻译： 提供了制备酶颗粒的方法，通过该方法制备的酶颗粒及其在制剂中的用途，例如用于动物饲料，食品，洗涤剂，漂洗剂或药物用途。 酶颗粒具有高的相对比例的活性酶，特定的粒度，良好的保存期限，特别是小的圆化因子和/或低残留水分比例，以及进一步的具体特性。 酶颗粒的生产通过在注射区中的热条件和装置的其余部分中的温度条件的连接来实现。 这是通过引入用于在注射区域中专门干燥的加热过程气体来实现的。 通过使用重力的装置的特定几何布置来实现将物品牢固地引入注射区域。 酶颗粒的酶活性的绝对值可以通过加入颗粒作为颗粒的种子材料来控制。

公开(公告)号：US07709036B2

公开(公告)日：2010-05-04

申请号：US11151629

申请日：2005-06-13

申请人： Karlheinz Rümpler ,  Mike Waskow ,  Bernhard Wand

发明人： Karlheinz Rümpler ,  Mike Waskow ,  Bernhard Wand

IPC分类号： A23L3/46

CPC分类号： A23P10/20

摘要： A method for producing granules made from malt extract is provided. The method provides for producing granules continuously or in batches under the prevention as much as possible of non-uniform temperature distributions in the production process. Simultaneously, the controllability of the granulation in the production is improved. This is realized by linking thermal conditions in the spraying zone and the temperature conditions in other region of the apparatus. This is achieved such that the supply of the heated process gas for drying is realized exclusively in the spraying region. The reliable supply of particles into the spraying region is performed through the special geometric configuration of the apparatus under the use of gravity.

摘要翻译： 提供了由麦芽提取物制造颗粒的方法。 该方法提供了在生产过程中尽可能多地预防不均匀的温度分布来连续或分批地生产颗粒。 同时，生产中造粒的可控性提高。 这是通过将喷涂区中的热条件和装置的其他区域中的温度条件相关联来实现的。 实现这一点，使得仅在喷射区域中实现用于干燥的加热过程气体的供应。 通过重力使用设备的特殊几何结构，可以将可靠的颗粒供应到喷涂区域。

公开(公告)号：US07767161B2

公开(公告)日：2010-08-03

申请号：US11448406

申请日：2006-06-07

申请人： Michael Jacob ,  Karlheinz Rümpler ,  Mike Waskow

发明人： Michael Jacob ,  Karlheinz Rümpler ,  Mike Waskow

IPC分类号： B01J8/18 ,  F27B15/00

CPC分类号： B01J8/1854 ,  B01J8/1818 ,  B01J8/26 ,  B01J8/34 ,  B01J8/36 ,  B01J8/386 ,  B01J2208/00884

摘要： A fluidized bed apparatus for batch-by-batch or continuous process control is provided that allows the processes in the fluidization region to be influenced as desired, especially in terms of material movement and dwell time. The fluidized bed apparatus is formed from at least two processing regions and the processing regions are connected to each other by overflow channels. The first processing region is provided with a solids inlet and the last processing region is provided with a solids outlet. For influencing the dwell time, the material to be treated is supplied to at least two processing regions one after the other and flows through these regions, wherein the material transport direction is a cross flow relative to the flow of the fluidization means.

摘要翻译： 提供了一种用于分批或连续过程控制的流化床设备，其允许流化区域中的过程受到影响，特别是在材料运动和停留时间方面。 流化床装置由至少两个处理区域形成，并且处理区域通过溢流通道相互连接。 第一处理区域设置有固体入口，最后一个处理区域设置有固体出口。 为了影响停留时间，将待处理的材料一个接一个地供给至少两个处理区域，并且流过这些区域，其中材料输送方向是相对于流化装置的流动的横流。

公开(公告)号：US07691438B2

公开(公告)日：2010-04-06

申请号：US10862238

申请日：2004-06-07

申请人： Michael Jacob ,  Karlheinz Rümpler ,  Mike Waskow

发明人： Michael Jacob ,  Karlheinz Rümpler ,  Mike Waskow

IPC分类号： B05D7/00

CPC分类号： C12N9/98 ,  A23K20/189 ,  A23K40/10 ,  A23L29/06 ,  A23P10/22 ,  A61K9/1688 ,  B01J2/16 ,  C12N9/16

摘要： A method for producing enzyme granulates, the resulting enzyme granulates, and their use in formulations, e.g., for animal feed, food, washing means, rinsing means, and/or for pharmaceutical purposes and the like. The enzyme granulates show, in particular, a high relative percentage of active enzymes, certain grain sizes, good storage stability, especially small roundness factor, and/or low residual moisture percentage as well as preferably additional specific properties. According to the invention, the enzyme granulates are produced by linking the thermal conditions in the spray zone and the temperature conditions in the remaining region of the fluidized bed. In the process according to the invention, this is achieved in that the supply of heated processing gas is realized for drying exclusively in the injection region. The reliable supply of particles in the injection region is realized through the special geometrical shape of the apparatus under the use of gravity. Through the addition of inert particles as nuclei material for cores, the absolute content of enzyme activity of the enzyme granulate can be controlled.

摘要翻译： 生产酶颗粒的方法，所得的酶颗粒及其在制剂中的用途，例如用于动物饲料，食品，洗涤方法，漂洗装置和/或用于药物目的等。 酶颗粒特别表现出活性酶的高相对百分比，某些晶粒尺寸，良好的储存稳定性，特别是小圆度因子和/或低残留水分百分比以及优选额外的特定性质。 根据本发明，通过将喷雾区中的热条件和流化床的剩余区域中的温度条件相关联来生产酶颗粒。 在根据本发明的方法中，实现了加热处理气体的供应被实现用于仅在喷射区域中进行干燥。 通过重力使用设备的特殊几何形状，可以实现注射区域中可靠的颗粒供应。 通过添加惰性颗粒作为芯的核材料，可以控制酶颗粒的酶活性的绝对含量。

公开(公告)号：US07241425B2

公开(公告)日：2007-07-10

申请号：US10756093

申请日：2004-01-13

申请人： Michael Jacob ,  Karlheinz Rümpler ,  Mike Waskow

发明人： Michael Jacob ,  Karlheinz Rümpler ,  Mike Waskow

IPC分类号： B32B5/02

CPC分类号： B01J8/1854 ,  B01J8/1818 ,  B01J8/26 ,  B01J8/34 ,  B01J8/36 ,  B01J8/386 ,  B01J2208/00884

摘要： A fluidized bed apparatus for batch-by-batch or continuous process control is provided that allows the processes in the fluidization region to be influenced as desired, especially in terms of material movement and dwell time. The fluidized bed apparatus is formed from at least two processing regions and the processing regions are connected to each other by overflow channels. The first processing region is provided with a solids inlet and the last processing region is provided with a solids outlet. For influencing the dwell time, the material to be treated is supplied to at least two processing regions one after the other and flows through these regions, wherein the material transport direction is a cross flow relative to the flow of the fluidization means.

摘要翻译： 提供了一种用于分批或连续过程控制的流化床设备，其允许流化区域中的过程受到影响，特别是在材料运动和停留时间方面。 流化床装置由至少两个处理区域形成，并且处理区域通过溢流通道相互连接。 第一处理区域设置有固体入口，最后一个处理区域设置有固体出口。 为了影响停留时间，将待处理的材料一个接一个地供给至少两个处理区域，并且流过这些区域，其中材料输送方向是相对于流化装置的流动的横流。

公开(公告)号：US06740632B1

公开(公告)日：2004-05-25

申请号：US09609110

申请日：2000-06-30

申请人： Michael Jacob ,  Karlheinz Rümpler

发明人： Michael Jacob ,  Karlheinz Rümpler

IPC分类号： C11D1100

CPC分类号： C11D11/0082 ,  C11D11/0088 ,  C11D11/02

摘要： A process is provided for manufacturing industrial detergents and industrial detergent components in granular or agglomerate form on a dry basis in an essentially horizontally oriented fluidized bed. The finished detergent granulates or agglomerates are distinguished by a homogenous composition of the individual raw material components, including the binder and the moisture content, have a high resistance to mechanical stress, are readily dispersible in water, and are low in dust or almost dust-free. In the process a binder and/or components in the form of solutions, suspensions, or melts are added to the solid material in the fluidized bed via a spray or injection system. Through the energy introduced via the process air, drying and compacting of the agglomerate granulate forming in the injection area of the fluidized bed occur. The supply temperature of the process air is in a range of about 20° C. up to the decomposition temperature of the individual materials. By adjusting the drying parameters, the product moisture can be varied. The particles entrained by the process air from the fluidized bed are separated from the air in an expansion zone provided with cross-sectional widenings integrated into the fluidized bed apparatus and in a filter system connected to it, and are conveyed back into the fluidized bed and agglomerated there. A low-dust or dust-free product results that having a granularity range of about 0.2 to 2.0 mm.

摘要翻译： 提供了一种在基本上水平取向的流化床中以干基方式制造颗粒或团块形式的工业洗涤剂和工业洗涤剂组分的方法。 成品洗涤剂颗粒或附聚物的特征在于各种原料组分的均匀组成，包括粘合剂和水分含量，具有高的机械应力抵抗性，易于分散在水中，并且灰尘少或几乎具有粉尘 - 自由。 在该方法中，将粘合剂和/或溶液，悬浮液或熔体形式的组分通过喷雾或注射系统加入到流化床中的固体物质中。 通过经由工艺空气引入的能量，发生在流化床的喷射区域中形成的附聚颗粒的干燥和压实。 工艺空气的供应温度在约20℃到单独材料的分解温度的范围内。 通过调整干燥参数，可以改变产品的湿度。 通过流化床处理空气夹带的颗粒在设置有流体床装置的横截面宽度的膨胀区和与其连接的过滤系统中的空气中分离，并被输送回流化床 聚集在那里 低灰尘或无尘产品的粒度范围约为0.2至2.0毫米。