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公开(公告)号：US5886230A
公开(公告)日：1999-03-23
申请号：US885044
申请日：1997-06-30
申请人： Willi Hofen , Wolfgang Boeck , Stephan Rautenberg , Joerg Sauer , Dietrich Arntz , Ralf Goedecke , Wolfgang Taugner , Raymund Sonnenschein
发明人： Willi Hofen , Wolfgang Boeck , Stephan Rautenberg , Joerg Sauer , Dietrich Arntz , Ralf Goedecke , Wolfgang Taugner , Raymund Sonnenschein
IPC分类号： B01J21/04 , B01J23/30 , C07B61/00 , C07C319/08 , C07C321/04 , C07C319/00
CPC分类号： C07C319/08
摘要： A process for continuous production of methyl mercaptan by catalytic reaction of methanol and hydrogen sulfide. Significant improvements in the pretreatment of the feed gas mixture and in utilization of the heat of reaction and the heat content of the product gas mixture. The energy required to vaporize the methanol is derived partly from utilization of the heat of compression of the hydrogen sulfide gas and from the heat content of the product gas leaving the reactor. The heat of reaction is utilized to heat the feed gas mixture to the reaction temperature, with the help of an external gas heater.
摘要翻译： 通过甲醇和硫化氢的催化反应连续生产甲硫醇的方法。 进料气体混合物的预处理以及反应热和产物气体混合物的热含量的显着改进。 蒸发甲醇所需的能量部分来自利用硫化氢气体的压缩热和离开反应器的产物气体的热含量。 借助于外部气体加热器，利用反应热将原料气体混合物加热至反应温度。
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2.发明授权Process for separating the product gas mixture from the catalytic synthesis of methyl mercaptan 失效从甲硫醇的催化合成中分离产物气体混合物的方法
公开(公告)号：US5866721A
公开(公告)日：1999-02-02
申请号：US885043
申请日：1997-06-30
申请人： Willi Hofen , Wolfgang Boeck , Stephan Rautenberg , Joerg Sauer , Dietrich Arntz , Ralf Goedecke , Wolfgang Taugner , Raymund Sonnenschein
发明人： Willi Hofen , Wolfgang Boeck , Stephan Rautenberg , Joerg Sauer , Dietrich Arntz , Ralf Goedecke , Wolfgang Taugner , Raymund Sonnenschein
IPC分类号： C07C319/02 , C07C319/28 , C07C321/04 , C07C319/06
CPC分类号： C07C319/28 , Y02P20/582
摘要： A process for separating the product gas mixture from the catalytic synthesis of methyl mercaptan. Because of improved separation of the product gas mixture into its components, less hydrogen sulfide and methyl mercaptan are lost in discharging the inert gases than in the known process. The inert gases can be burned without after-treatment of the exhaust gas. Likewise, the process water that is discharged is less contaminated with polysulfides.
摘要翻译： 从甲硫醇的催化合成中分离产物气体混合物的方法。 由于改进了产物气体混合物与其组分的分离，在排放惰性气体方面比在已知方法中更少的硫化氢和甲基硫醇就会减少。 惰性气体可以在没有废气的后处理的情况下燃烧。 同样，排出的工艺水较少被多硫化物污染。
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公开(公告)号：US07326393B2
公开(公告)日：2008-02-05
申请号：US10529148
申请日：2003-08-26
IPC分类号： C01B12/20
CPC分类号： C01B17/167 , C01B17/168
摘要： The invention provides a process for the removal of polysulfanes from gas streams formed during H2S synthesis.
摘要翻译： 本发明提供了一种从H 2 S合成期间形成的气流中除去多硫烷的方法。
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4.发明申请公开(公告)号：US20050137426A1
公开(公告)日：2005-06-23
申请号：US11016130
申请日：2004-12-17
申请人： Alexander Moller , Wolfgang Bock , Stephan Rautenberg , Hans-Joachim Hasselbach , Wolfgang Taugner , Harald Heinzel , Theo Zarfl
发明人： Alexander Moller , Wolfgang Bock , Stephan Rautenberg , Hans-Joachim Hasselbach , Wolfgang Taugner , Harald Heinzel , Theo Zarfl
IPC分类号： C07C319/18 , C07C319/28 , C07C321/04 , C07C323/22 , C07C319/08
CPC分类号： C07C319/08 , C07C319/18 , C07C319/28 , C07C321/04 , C07C323/22
摘要： The invention relates to a method for the separation of methyl mercaptan from reaction gas mixtures obtained by means of the catalytic conversion of H2S with methanol, by means of converting the methyl mercaptan into MMP in the presence of the byproducts with acrolein, and separating the same.
摘要翻译： 本发明涉及通过在丙烯醛的副产物存在下将甲硫醇转化为MMP，将甲硫醇与通过H 2 S与甲醇的催化转化得到的反应气体混合物分离的方法， 。
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公开(公告)号：US20080175778A1
公开(公告)日：2008-07-24
申请号：US11976717
申请日：2007-10-26
CPC分类号： C01B17/168
摘要： The invention provides a process for the removal of polysulfanes from gas streams formed during H2S synthesis.
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6.发明授权公开(公告)号：US07199270B2
公开(公告)日：2007-04-03
申请号：US11016130
申请日：2004-12-17
申请人： Alexander Möller , Wolfgang Böck , Stephan Rautenberg , Hans-Joachim Hasselbach , Wolfgang Taugner , Harald Heinzel , Theo Zarfl
发明人： Alexander Möller , Wolfgang Böck , Stephan Rautenberg , Hans-Joachim Hasselbach , Wolfgang Taugner , Harald Heinzel , Theo Zarfl
IPC分类号： C07C319/00
CPC分类号： C07C319/08 , C07C319/18 , C07C319/28 , C07C321/04 , C07C323/22
摘要： The invention relates to a method for the separation of methyl mercaptan from reaction gas mixtures obtained by means of the catalytic conversion of H2S with methanol, by means of converting the methyl mercaptan into MMP in the presence of the byproducts with acrolein, and separating the same.
摘要翻译： 本发明涉及通过在丙烯醛的副产物存在下将甲硫醇转化为MMP，将甲硫醇与通过H 2 S与甲醇的催化转化得到的反应气体混合物分离的方法， 。
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公开(公告)号：US07604788B2
公开(公告)日：2009-10-20
申请号：US11976717
申请日：2007-10-26
CPC分类号： C01B17/168
摘要： The invention provides a process for the removal of polysulfanes from gas streams formed during H2S synthesis.
摘要翻译： 本发明提供从H2S合成过程中形成的气流中除去多硫烷的方法。
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公开(公告)号：US20050265913A1
公开(公告)日：2005-12-01
申请号：US10529148
申请日：2003-08-26
CPC分类号： C01B17/167 , C01B17/168
摘要： The invention provides a process for the removal of polysulfanes from gas streams formed during H2S synthesis.
摘要翻译： 本发明提供了一种从H 2 S合成期间形成的气流中除去多硫烷的方法。
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9.发明授权Method for removing acrolein from the process gas of a heterogeneously catalysed oxidation of propene 有权从异丙烯催化丙烯氧化的工艺气体中除去丙烯醛的方法公开(公告)号：US09334215B2
公开(公告)日：2016-05-10
申请号：US14762124
申请日：2014-01-28
申请人： Wolfgang Boeck , Wolfgang Taugner , Udo Gruber
发明人： Wolfgang Boeck , Wolfgang Taugner , Udo Gruber
CPC分类号： C07C45/35 , C07C45/78 , C07C45/783 , C07C45/82 , C07C47/22
摘要： The invention relates to a process for separating acrolein from the process gas of a heterogeneously catalyzed oxidation of propene by means of atmospheric oxygen, wherein high boilers (including acrylic acid) are firstly separated off from the process gas by means of quenching and technical-grade acrolein having small proportions of low boilers is then obtained by means of absorption and subsequent distillation. Small amounts of a solvent by means of which, in particular, oligomers formed are separated off and the tendency for foam to be formed in the apparatuses or columns is reduced is added in the columns and heat exchangers in the work-up process. The solvent is, according to the invention, separated off and recycled in the form of an organic phase in-situ within the existing process.
摘要翻译： 本发明涉及一种通过大气氧从异丙烯催化丙烯氧化的工艺气体中分离丙烯醛的方法，其中高沸点（包括丙烯酸）首先通过淬火和技术级分离工艺气体 然后通过吸收和随后的蒸馏获得具有小比例的低锅炉的丙烯醛。 在后处理过程中，在柱和热交换器中加入少量的溶剂，特别是所形成的低聚物被除去，并且在装置或塔中形成泡沫的趋势被减少。 根据本发明，溶剂在现有方法中分离并以有机相的形式在原位再循环。
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