摘要:
An ion mobility spectrometer is provided including at least one ionization chamber (1), which can be passed through by analyte-containing gas and at least one radiation source (2), from which ionizing radiation which is suitable for at least partially ionizing the analyte-containing gas enters the ionization chamber (1). At least one transition area (3) is provided, into which the at least partially ionized gas as ion carrier gas (4) and an almost ion-free gas as drift gas (5) can be charged in a way that, at least at the end of the transition area (3), a flow is established, in which cross-sectional areas (6) are mainly passed through by ion carrier gas (4) and other cross-sectional areas (7, 7′) are mainly passed through by drift gas (5). At least one separation area (8) is provided lying in the direction of flow behind the transition area (3), in which, likewise, cross-sectional areas are mainly passed through by ion carrier gas (4) and other cross-sectional areas are mainly passed through by drift gas (5). The drift gas (5) and ion carrier gas (4) flow unidirectionally, and the cross-sectional areas (6) that are mainly passed through by ion carrier gas (4) are smaller at least in one dimension than the cross-sectional areas (7, 7′) that are mainly passed through by drift gas (5).
摘要:
A novel, compact non-radioactive electron emitter is provided with a cylindrical shape and with an interior space (6), which forms a vacuum chamber. A substrate (7) forms the bottom of the arrangement with a plurality of field emitter tips (5) formed of carbon nanotubes in the interior space (6). The tips are fastened to the substrate. A layer structure forms the cover of the arrangement, having, from the outside towards the interior space (6), an electrode layer (13), which acts as a counterelectrode and is applied to a gas-impermeable and electron-permeable membrane (10). A substrate (11), which is left open in the form of a window (12) in the area above the field emitter tips (6), acts as a carrier substrate for the membrane (10) and the electrode layer (13). A circumferential wall (14) of the arrangement is formed by an electrically insulating material. The field emitter tips (5) and the electrode layer (13) are connected to a d.c. power source, so that the electrons exiting from the field emitter tips (5) are accelerated through the vacuum chamber, window (12) and the membrane (10) towards the electrode layer (13), pass through the electrode layer (13) and enter the ionization area (3) outside the electron emitter (1, 1′).
摘要:
An ion mobility spectrometer is provided with at least one ionization chamber (1) through which analyte-containing gas can flow. A radiation source (2) is provided from which ionizing radiation is suitable for ionizing the analyte-containing gas at least partially, enters the ionization space (1). A separation area is located behind the ionization space (1) in the direction of flow, into which the partially ionized gas is admitted as an ion carrier gas (4) and a nearly ion-free gas is admitted as a drift gas (5) in such a way that a flow in which predominantly ion carrier gas (4) flows through cross-sectional areas (6) and predominantly drift gas (5) flows through other cross-sectional areas (7, 7′), becomes established at least in the inlet area of the separation area (8). The drift gas (5) and ion carrier gas (4) flow unidirectionally and the cross-sectional areas (6), through which predominantly ion carrier gas (4) flows, are smaller in at least one dimension than the cross-sectional areas (7, 7′), through which predominantly drift gas (5) flows.
摘要:
A colorimetric detector such as a gas dosimeter, contains a strip-like carrier with a detection reagent in a transparent housing that can be opened at least at one end thereof. The detector is expanded in terms of its use to such reagent systems in which the pigment formed diffuses beyond the reaction zone. For this purpose, the detection reagent is provided such that it is contained in impregnated tabs arranged in a row on the carrier.
摘要:
A device for displaying the exhaustion of a gas filter filled with an adsorbent (3). A toxic gas detector (14) determines the toxic gas content at a sampling site (8) within the adsorbent (3). A reference sampling site (12) is located in the area of a gas inlet point (6) of the gas filter (2). The toxic gas detector is designed such that it determines the toxic gas content alternately at the sampling sites (8, 12), and the exhaustion of the filter is determined by a comparison of the toxic gas content at the sampling site (8) with the toxic gas content at the reference sampling site (12).
摘要:
The subject of the invention is a method for identification of analytes with an ion mobility spectrometer by performing a series of measurements while varying the residence time of the analytes in the reaction space and identifying of monomer and nascent dimer analytes in the spectra so obtained.
摘要:
The invention relates to a colorimetric gas measuring device having a porous substrate accessible to the air sample to be investigated. The substrate includes a conversion zone which converts a component to be detected into a substance which leads to a coloration of an indicator in a detection zone. The gas measuring device makes possible a simple and inexpensive quantitative detection of chlorosilanes. For this purpose, the conversion zone includes silica gel and the detection zone includes a carrier impregnated with an acid indicator.
摘要:
The subject of the invention is a method for identification of analytes with an ion mobility spectrometer by performing a series of measurements while varying the residence time of the analytes in the reaction space and identifying of monomer and nascent dimer analytes in the spectra so obtained.
摘要:
One or more reaction zones, formed as channels into a carrier, are each lined with a color indicator. This carrier is improved so that the reaction zones can be coated with the required indicators with uniform coating thickness. The coating can be individually changed and can be easily provided. The above is achieved with a carrier which is subdivided into an upper part and a lower part and a sandwich-like composite foil is held between these parts. A reagent carrier foil of the composite foil is provided with the reaction zones and is covered with a channel foil which delimits the reaction zones to have a channel-like shape. An especially advantageous configuration for the reaction zones is provided by an aperture matrix in which carrier spherules are accommodated. The carrier spherules are impregnated with the indicator.
摘要:
A respirator with an eye space (16), through which the air to be inhaled flows, and with an indicator located on a support for indicating the efficiency of the protective device on the respiration connection, which is to retain the pollutant from the environment. The pollutant indication takes place both in the case of leakages at the sealing zones of the mask or the respiration gas-carrying lines (compressed air respirator) and in the case of insufficient filter effect. To achieve this, the support (10) is arranged on an inner half mask (3) of the respirator, and an access surface, which is exposed to the pollutant and contains the indicator (18, 118), is in flow contact with the air being inhaled, which flows through the passage openings (12, 112) between the eye space (16) of the full mask (1) and the inner half mask space (4).