公开(公告)号：US08828158B2

公开(公告)日：2014-09-09

申请号：US12664816

申请日：2008-06-09

申请人： Ryuichi Inoue ,  Nozomu Kawabe ,  Nobuyuki Mori ,  Masatada Numano ,  Junichi Matsumoto ,  Motonori Nakamura ,  Masayuki Nishizawa ,  Atsushi Kimura ,  Yukihiro Oishi

发明人： Ryuichi Inoue ,  Nozomu Kawabe ,  Nobuyuki Mori ,  Masatada Numano ,  Junichi Matsumoto ,  Motonori Nakamura ,  Masayuki Nishizawa ,  Atsushi Kimura ,  Yukihiro Oishi

IPC分类号： C22C23/02 ,  C22F1/06

CPC分类号： C22C23/04 ,  C22C23/00 ,  C22C23/02 ,  C22F1/06

摘要： The invention offers a magnesium alloy sheet having excellent warm plastic formability, a production method thereof, and a formed body produced by performing warm plastic forming on this sheet. The magnesium alloy sheet is produced by giving a predetermined strain to a rolled sheet RS that is not subjected to a heat treatment aiming at recrystallization. The sheet is not subjected to the foregoing heat treatment even after the giving of a strain. The strain is given through the process described below. A rolled sheet RS is heated in a heating furnace 10. The heated rolled sheet RS is passed between rollers 21 to give bending to the rolled sheet RS. The giving of a strain is performed such that the strain-given sheet has a half peak width of 0.20 deg or more and 0.59 deg or less in a (0004) diffraction peak in monochromatic X-ray diffraction. The alloy sheet exhibits high plastic deformability by forming continuous recrystallization during warm plastic forming through the use of the remaining strain.

摘要翻译： 本发明提供一种具有优异的耐热塑性成形性的镁合金板及其制造方法，以及通过在该片上进行热塑性成形而制成的成形体。 通过对未进行再结晶的热处理的轧制板RS给予规定的应变来制造镁合金板。 即使施加了应变，片材也不进行上述的热处理。 通过下述方法给出菌株。 轧制板RS在加热炉10中被加热。加热的轧制板RS在辊21之间通过，以使轧制板RS弯曲。 进行应变的施加使得在单色X射线衍射中的（0004）衍射峰中，应变给定片的半峰宽度为0.20度以上且0.59度以下。 通过使用剩余的应变，通过在热塑性成型期间形成连续的再结晶，合金板表现出高的塑性变形性。

公开(公告)号：US20130337282A1

公开(公告)日：2013-12-19

申请号：US14001646

申请日：2012-02-23

申请人： Yukihiro Oishi ,  Nobuyuki Mori ,  Ryuichi Inoue ,  Nozomu Kawabe

发明人： Yukihiro Oishi ,  Nobuyuki Mori ,  Ryuichi Inoue ,  Nozomu Kawabe

IPC分类号： C22C23/02 ,  C22C23/00

CPC分类号： C22C23/02 ,  B22D11/001 ,  B22D11/0622 ,  C21D2201/05 ,  C22C1/02 ,  C22C23/00 ,  C22F1/06 ,  Y10T428/12

摘要： There are provided a magnesium alloy material and a method for producing the magnesium alloy material. In a magnesium (Mg) alloy material having a sheet-shaped portion with a thickness of 1.5 mm or more, when a region having ¼ the thickness of the sheet-shaped portion in a thickness direction from a surface of the sheet-shaped portion is defined as a surface region and a remaining region is defined as an internal region, the ratio OF/OC of the basal plane peak ratio OF in the surface region to the basal plane peak ratio OC (degree of orientation of (002) planes) in the internal region satisfies 0.95≦OF/OC≦1.05. A sheet-shaped Mg alloy material is obtained by performing at least one pass of the rolling at a reduction ratio of 25% or more and the remaining passes of the rolling at a reduction ratio of 10% or more.

摘要翻译： 提供镁合金材料和镁合金材料的制造方法。 在具有厚度为1.5mm以上的片状部分的镁（Mg）合金材料中，当从片状部分的表面沿厚度方向的片状部分的厚度为1/4时， 定义为表面区域，剩余区域被定义为内部区域，表面区域中的基底平面峰值比OF与基底面峰值比率OC（（002）面取向度）的比值OF / OC） 内部区域满足0.95 @ OF / OC @ 1.05。 通过以25％以上的压下率和10％以上的压下率进行轧制的至少一次轧制，得到片状的Mg合金材料。

公开(公告)号：US20130333809A1

公开(公告)日：2013-12-19

申请号：US14001661

申请日：2012-02-23

申请人： Yukihiro Oishi ,  Nobuyuki Mori ,  Ryuichi Inoue ,  Nozomu Kawabe

发明人： Yukihiro Oishi ,  Nobuyuki Mori ,  Ryuichi Inoue ,  Nozomu Kawabe

IPC分类号： C22C23/02 ,  C22C23/00

CPC分类号： C22C23/02 ,  B22D11/001 ,  B22D11/0622 ,  C22C23/00 ,  C22F1/06

摘要： There are provided a magnesium alloy material and a method for producing the magnesium alloy material. In a magnesium (Mg) alloy material (e.g., Mg alloy sheet) having a sheet-shaped portion with a thickness of 1.5 mm or more, when a region having ¼ the thickness of the sheet-shaped portion in a thickness direction from a surface of the sheet-shaped portion is defined as a surface region and a remaining region is defined as an internal region, the ratio OF/OC of the basal plane peak ratio OF in the surface region to the basal plane peak ratio OC (degree of orientation of (002) planes) in the internal region satisfies 1.05

摘要翻译： 提供镁合金材料和镁合金材料的制造方法。 在具有厚度为1.5mm以上的片状部分的镁（Mg）合金材料（例如Mg合金板）中，当厚度方向上的片状部分的厚度为1/4时， 被定义为表面区域，将剩余区域定义为内部区域，表面区域中的基底峰值比率OF与基准面峰值比率OC（取向度）的比值OF / OC 的（002）面）满足1.05

公开(公告)号：US20130220496A1

公开(公告)日：2013-08-29

申请号：US13882785

申请日：2011-11-08

申请人： Ryuichi Inoue ,  Kohji Inokuchi ,  Yukihiro Oishi ,  Nozomu Kawabe

发明人： Ryuichi Inoue ,  Kohji Inokuchi ,  Yukihiro Oishi ,  Nozomu Kawabe

IPC分类号： C22F1/06 ,  C22C23/02

CPC分类号： C22F1/06 ,  B22D11/001 ,  C22C23/00 ,  C22C23/02 ,  C22C23/04 ,  C22C23/06

摘要： Provided are a magnesium alloy sheet having excellent corrosion resistance and a method for producing the same.The magnesium alloy sheet has dispersed therein particles of an intermetallic compound containing an additive element (e.g., Al) and Mg (a typical example of which is Mg17Al12), and the ratio obtained by dividing the diffraction intensity of the main diffraction plane (4,1,1) of the intermetallic compound by the diffraction intensity of the c plane (0,0,2) of the Mg alloy phase in an XRD analysis of the surface of the sheet is 0.040 or more. The method for producing a magnesium alloy sheet includes the following steps: a casting step of producing a cast material composed of a magnesium alloy containing an additive element by continuous casting; a heat treatment step of holding the cast material at 400° C. or higher and then cooling the cast material at a cooling rate of 30° C./min or less to produce a heat-treated material; and a rolling step of subjecting the heat-treated material to warm rolling to produce a rolled sheet.

摘要翻译： 本发明提供耐腐蚀性优异的镁合金板及其制造方法。 镁合金薄片中分散有含有添加元素（例如Al）和Mg（典型实例为Mg17Al12）的金属间化合物的颗粒，并且通过将主衍射平面（4， 在该表面的XRD分析中，通过Mg合金相的c面（0,0,2）的衍射强度，金属间化合物的重量比为0.01以上。 镁合金板的制造方法包括以下步骤：通过连续铸造制造由含有添加元素的镁合金构成的铸造材料的铸造工序; 将铸造材料保持在400℃以上，然后以30℃/分钟以下的冷却速度冷却铸造材料的热处理工序，制造热处理材料; 以及对热处理材料进行加热轧制以生产轧制板的轧制步骤。

公开(公告)号：US20110003139A1

公开(公告)日：2011-01-06

申请号：US12864419

申请日：2009-01-14

申请人： Masatada Numano ,  Nozomu Kawabe ,  Yukihiro Oishi ,  Nobuyuki Mori ,  Nobuyuki Okuda ,  Ryuichi Inoue

发明人： Masatada Numano ,  Nozomu Kawabe ,  Yukihiro Oishi ,  Nobuyuki Mori ,  Nobuyuki Okuda ,  Ryuichi Inoue

IPC分类号： B32B15/02 ,  B32B5/16

CPC分类号： C22F1/06 ,  B22D11/007 ,  B22D19/04 ,  B22D21/007 ,  C22C23/02 ,  C22C32/0063 ,  Y10T428/25

摘要： The invention offers a magnesium alloy sheet material having excellent plastic processibility and rigidity and a magnesium alloy formed body having excellent rigidity. The sheet material has magnesium alloy that forms the matrix containing hard particles. The region from the surface of the sheet material to a position away from the surface by 40% of the thickness of the sheet material is defined as the surface region, and the remaining region as the center region. Hard particles existing in the center region have a maximum diameter of more than 20 μm and less than 50 μm, and hard particles existing in the surface region have a maximum diameter of 20 μm or less. Because the hard particles existing at the surface side are fine particles, they are less likely to become the starting point of cracking or another defect at the time of plastic processing. Because the hard particles existing in the center region are coarse, they can increase the rigidity of the sheet material.

摘要翻译： 本发明提供具有优异的塑性加工性和刚性的镁合金板材和具有优异刚性的镁合金成形体。 片材具有形成含有硬质粒子的基体的镁合金。 从片材的表面到离开表面的位置的片材的厚度的40％的区域被定义为表面区域，其余区域被定义为中心区域。 存在于中心区域的硬质粒子的最大直径大于20μm且小于50μm，存在于表面区域的硬质粒子的最大直径为20μm以下。 由于存在于表面侧的硬质粒子是微细的粒子，因此在塑性加工时不太可能成为开裂的起点或其他缺陷。 由于存在于中心区域的硬质粒子较粗糙，因此能够提高片材的刚性。

公开(公告)号：US20050208324A1

公开(公告)日：2005-09-22

申请号：US10506509

申请日：2003-03-04

申请人： Yukihiro Oishi ,  Nozomu Kawabe ,  Hitoshi Takahashi ,  Katsumi Wakamatsu

发明人： Yukihiro Oishi ,  Nozomu Kawabe ,  Hitoshi Takahashi ,  Katsumi Wakamatsu

IPC分类号： B21C1/00 ,  B21C1/24 ,  B21C5/00 ,  B21C9/00 ,  C22C23/02 ,  C22C23/04 ,  C22F1/00 ,  C22F1/06 ,  B32B15/10

CPC分类号： C22F1/06 ,  B21C1/003 ,  B21C1/24 ,  B21C5/00 ,  B21C5/003 ,  B21C9/00 ,  C22C23/02 ,  C22C23/04 ,  Y10T428/12292 ,  Y10T428/12764 ,  Y10T428/12792

摘要： A magnesium base alloy pipe having high strength and toughness is provided along with a method of manufacturing such pipes. A magnesium base alloy pipe, wherein the pipe is produced by drawing a pipe blank of a magnesium base alloy comprising containing either of the following ingredients (1) or (2): (1) about 0.1-12.0 mass % of Al; or (2) about 1.0-10.0 mass % of Zn and about 0.1-2.0 mass % of Zr. The novel alloy pipe is manufactured by a method comprising steps of providing the above-described pipe blank, pointing the pipe blank, and drawing the pointed pipe blank. The drawing step is executed at a drawing temperature above approx. 50 ° C.

摘要翻译： 提供具有高强度和韧性的镁基合金管以及这种管的制造方法。 一种镁基合金管，其特征在于，所述管是通过拉制含有以下成分（1）或（2）中的任一种的镁基合金的管坯制造的：（1）约0.1-12.0质量％的Al; 或（2）约1.0-10.0质量％的Zn和约0.1-2.0质量％的Zr。 该新型合金管通过以下步骤制造，该方法包括以下步骤：提供上述管坯，指向管坯，以及拉出尖的管坯。 绘图步骤在高于约的绘图温度下执行。 50°C

公开(公告)号：US09598749B2

公开(公告)日：2017-03-21

申请号：US13985430

申请日：2012-02-13

申请人： Yukihiro Oishi ,  Nobuyuki Mori ,  Ryuichi Inoue ,  Masaaki Fujii ,  Masahiko Ito ,  Nozomu Kawabe

发明人： Yukihiro Oishi ,  Nobuyuki Mori ,  Ryuichi Inoue ,  Masaaki Fujii ,  Masahiko Ito ,  Nozomu Kawabe

IPC分类号： C22F1/06 ,  C22C23/00 ,  C22C23/02 ,  C22C23/04 ,  C22C23/06 ,  B21B1/00 ,  B21B3/00

CPC分类号： C22C23/00 ,  B21B1/00 ,  B21B3/00 ,  C22C23/02 ,  C22C23/04 ,  C22C23/06 ,  C22F1/06

摘要： Provided are a rolled Mg alloy material whose mechanical properties are locally different in a width direction, a Mg alloy structural member produced by plastically working the rolled Mg alloy material, and a method for producing the rolled Mg alloy material. The method for producing a rolled Mg alloy material includes rolling a Mg alloy material with a reduction roll. The reduction roll has three or more regions in the width direction. The temperature is controlled in each of the regions so that a difference between a maximum temperature and a minimum temperature exceeds 10° C. in the width direction of a surface of the reduction roll. The rolled state in the width direction is varied by varying a difference in temperature over the width direction of the reduction roll. As a result, it is possible to produce a rolled Mg alloy material whose mechanical properties are locally different in the width direction.

公开(公告)号：US20110268986A1

公开(公告)日：2011-11-03

申请号：US13142360

申请日：2009-11-17

申请人： Masatada Numano ,  Ryuichi Inoue ,  Nobuyuki Okuda ,  Nozomu Kawabe ,  Koji Mori ,  Nobuyuki Mori ,  Yukihiro Oishi ,  Takahiko Kitamura

发明人： Masatada Numano ,  Ryuichi Inoue ,  Nobuyuki Okuda ,  Nozomu Kawabe ,  Koji Mori ,  Nobuyuki Mori ,  Yukihiro Oishi ,  Takahiko Kitamura

IPC分类号： B21D39/00 ,  B23P11/00

CPC分类号： H05K5/04 ,  Y10T29/49908 ,  Y10T156/10 ,  Y10T156/1002 ,  Y10T428/12611

摘要： The method of producing a magnesium alloy joined part has the following steps: a joining step of joining a reinforcing material made of metal to a plate material made of magnesium alloy without allowing an organic material to remain at the joined portion and a plastic-working step of performing plastic working on the plate material to which the reinforcing material is joined. A desirable means of joining the reinforcing material to the plate material can be to use an inorganic adhesive. Because the magnesium alloy joined part is formed by a structure in which the reinforcing material is joined to the plate material, in comparison with the case where the reinforcing material is formed by machining or the like, the magnesium alloy structural member can be obtained with high production efficiency.

摘要翻译： 镁合金接合部的制造方法具有以下步骤：将由金属制成的增强材料与镁合金制的板材接合而不使有机材料残留在接合部的接合工序和塑性加工工序 对加强材料接合的板材进行塑性加工。 将增强材料接合到板材的期望的方法可以是使用无机粘合剂。 由于镁合金接合部分是通过加强材料与板材接合的结构形成的，与通过机加工等形成增强材料的情况相比，可以获得高的镁合金结构件 生产效率。

公开(公告)号：US20110217514A1

公开(公告)日：2011-09-08

申请号：US12377916

申请日：2007-07-10

申请人： Nobuyuki Okuda ,  Masatoshi Majima ,  Shoichiro Sakai ,  Shinji Inazawa ,  Nobuyuki Mori ,  Ryuichi Inoue ,  Yukihiro Oishi ,  Nozomu Kawabe ,  Masatada Numano

发明人： Nobuyuki Okuda ,  Masatoshi Majima ,  Shoichiro Sakai ,  Shinji Inazawa ,  Nobuyuki Mori ,  Ryuichi Inoue ,  Yukihiro Oishi ,  Nozomu Kawabe ,  Masatada Numano

IPC分类号： B32B3/00 ,  B05D3/12 ,  B22D25/00 ,  B05D1/36 ,  C25D7/00

CPC分类号： C23C22/83 ,  C22C23/02 ,  C22F1/06 ,  C23C22/18 ,  C23C22/364 ,  C23C22/37 ,  C25D11/30 ,  Y10T428/24364

摘要： There is provided a magnesium alloy member having mechanical properties and corrosion resistance and a method of manufacturing the magnesium alloy member.A magnesium alloy member has a base material made of a magnesium alloy, and an anticorrosive film formed on the base material. The base material is a rolled magnesium alloy including 5 to 11% by mass of Al. By using a base material including a large amount of Al, a magnesium alloy member having excellent mechanical properties and high corrosion resistance can be produced. In addition, by using a rolled material, the number of surface defects at the time of casting is small, and the frequency of compensation processes such as undercoating and puttying can be reduced.

摘要翻译： 提供了具有机械性能和耐腐蚀性的镁合金构件以及镁合金构件的制造方法。 镁合金构件具有由镁合金制成的基材和形成在基材上的防腐蚀膜。 基材是含有5〜11质量％的Al的轧制镁合金。 通过使用含有大量Al的基材，可以制造具有优异的机械性能和高耐腐蚀性的镁合金构件。 此外，通过使用轧制材料，铸造时的表面缺陷的数量少，可以降低底涂和腻子等补偿处理的频率。

公开(公告)号：US20110203706A1

公开(公告)日：2011-08-25

申请号：US13125023

申请日：2009-09-29

申请人： Yukihiro Oishi ,  Nozomu Kawabe ,  Nobuyuki Okuda ,  Nobuyuki Mori ,  Masatada Numano ,  Koji Mori ,  Takahiko Kitamura ,  Ryuichi Inoue

发明人： Yukihiro Oishi ,  Nozomu Kawabe ,  Nobuyuki Okuda ,  Nobuyuki Mori ,  Masatada Numano ,  Koji Mori ,  Takahiko Kitamura ,  Ryuichi Inoue

IPC分类号： C22C23/02

CPC分类号： C22C23/02 ,  C22F1/06

摘要： A formed product of a magnesium alloy having excellent impact resistance and a magnesium alloy sheet suitable as a material for the formed product are provided. The formed product is produced by press-forming a magnesium alloy sheet having an Al content of 7% by mass to 12% by mass and has a flat portion that is not subjected to drawing deformation. In a metal texture in a cross section of the flat portion in the thickness direction, the number of coarse intermetallic compound (Mg17Al12) particles having a particle size of 5 μm or more present in a surface area region extending from a surface of the flat portion to a position one-third of the thickness from the surface in the thickness direction is five or less. The formed product has a texture in which the number of coarse precipitations d1 is small and in which fine precipitations d0 are dispersed. The formed product is less likely to be dented even when impacted because of dispersion strengthening owing to the fine precipitations and solid-solution strengthening owing to Al that sufficiently forms a solid solution.

摘要翻译： 提供了具有优异抗冲击性的镁合金的成型产品和适合成型产品的材料的镁合金板。 形成的产品通过压制形成Al含量为7质量％至12质量％的镁合金板而制成，并具有不受拉伸变形的平坦部分。 在平坦部分的厚度方向的横截面中的金属结构中，存在于从平坦部分的表面延伸的表面区域中具有5μm以上的粒子的粗大的金属间化合物（Mg17Al12）颗粒的数量 到厚度方向上的表面厚度的三分之一的位置为五分之一以下。 形成的产品具有其中粗沉淀物d1的数量少并且其中分散有细小沉淀物d0的织构。 即使由于由于充分形成固溶体的Al的细小沉淀和固溶强化而引起的分散强化，即使被冲击也难以形成凹陷。