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    Method of making natural oil-based polyols and polyurethanes therefrom
    1.
    发明授权
    Method of making natural oil-based polyols and polyurethanes therefrom 有权
    从其制备天然油基多元醇和聚氨酯的方法

    公开(公告)号：US06433121B1

    公开(公告)日：2002-08-13

    申请号：US09612716

    申请日：2000-07-10

    申请人： Zoran Petrovic ,  Ivan Javni ,  Andrew Guo ,  Wei Zhang

    发明人： Zoran Petrovic ,  Ivan Javni ,  Andrew Guo ,  Wei Zhang

    IPC分类号： C08J300

    CPC分类号： C07D303/42 ,  C08G18/36 ,  C08G2190/00

    摘要： A method for making natural oil-based polyols directly from vegetable or animal oil using a consecutive two-step process involving epoxidation and hydroxylation is provided. Specifically, this process comprises adding a peroxyacid to a natural oil wherein said natural oil and said peroxyacid react to form an epoxidized natural oil and adding said epoxidized natural oil to a mixture of an alcohol, water, and a fluoboric acid catalyst. The catalytic amount of fluoboric acid is less than about 0.5% by weight of the entire reaction mixture, and the amount of water is about 10 to 30% by weight of the entire mixture. The epoxidized natural oil undergoes hydroxylation and forms a natural oil-based polyol. The present invention further includes a method for making natural oil-based polyols from epoxidized oil by hydroylating the epoxidized oil in the presence of fluoboric acid, alcohol and water in the amounts discussed above. The natural oil-based polyols created by this method may be reacted with isocyanates so as to form polyurethanes, which is another embodiment of the present invention. Alternatively, fillers such as silica may be combined with these natural oil-based polyols before they are reacted with isocyanates to form polyurethanes. In still another embodiment of the present invention, polyurethanes made from natural oil-based polyols may be used to form electroinsulating casting resins for use in electrical applications.

    摘要翻译： 提供了一种使用直接由植物油或动物油直接制备天然油基多元醇的方法，该方法使用涉及环氧化和羟基化的连续两步法。 具体地，该方法包括向天然油中加入过氧酸，其中所述天然油和所述过氧酸反应形成环氧化天然油，并将所述环氧化天然油加入到醇，水和氟硼酸催化剂的混合物中。 氟硼酸的催化量小于整个反应混合物的约0.5重量％，水的量为整个混合物的约10至30重量％。 环氧化天然油经历羟基化，形成天然油基多元醇。 本发明还包括通过在上述量的氟硼酸，醇和水的存在下对环氧化油进行水解来制备环氧化油的天然油基多元醇的方法。通过该方法制备的天然油基多元醇可以是 与异氰酸酯反应以形成聚氨酯，这是本发明的另一个实施方案。 或者，诸如二氧化硅的填料可以在与异氰酸酯反应形成聚氨酯之前与这些天然油基多元醇组合。 在本发明的另一个实施方案中，由天然油基多元醇制成的聚氨酯可用于形成用于电气应用的电绝缘铸塑树脂。

    Method of making natural oil-based polyols and polyurethanes therefrom
    3.
    发明授权
    Method of making natural oil-based polyols and polyurethanes therefrom 有权
    从其制备天然油基多元醇和聚氨酯的方法

    公开(公告)号：US06686435B1

    公开(公告)日：2004-02-03

    申请号：US10176214

    申请日：2002-06-20

    申请人： Zoran Petrovic ,  Ivan Javni ,  Andrew Guo ,  Wei Zhang

    发明人： Zoran Petrovic ,  Ivan Javni ,  Andrew Guo ,  Wei Zhang

    IPC分类号： C08J300

    CPC分类号： C07D303/42 ,  C08G18/36 ,  C08G2190/00

    摘要： A method for making natural oil-based polyols directly from vegetable or animal oil using a consecutive two-step process involving epoxidation and hydroxylation is provided. Specifically, this process comprises adding a peroxyacid to a natural oil wherein said natural oil and said peroxyacid react to form an epoxidized natural oil and adding said epoxidized natural oil to a mixture of an alcohol, water, and a fluoboric acid catalyst. The catalytic amount of fluoboric acid is less than about 0.5% by weight of the entire reaction mixture, and the amount of water is about 10 to 30% by weight of the entire mixture. The epoxidized natural oil undergoes hydroxylation and forms a natural oil-based polyol. The present invention further includes a method for making natural oil-based polyols from epoxidized oil by hydroylating the epoxidized oil in the presence of fluoboric acid, alcohol and water in the amounts discussed above. The natural oil-based polyols created by this method may be reacted with isocyanates so as to form polyurethanes, which is another embodiment of the present invention. Alternatively, fillers such as silica may be combined with these natural oil-based polyols before they are reacted with isocyanates to form polyurethanes. In still another embodiment of the present invention, polyurethanes made from natural oil-based polyols may be used to form electroinsulating casting resins for use in electrical applications.

    摘要翻译： 提供了一种使用直接由植物油或动物油直接制备天然油基多元醇的方法，该方法使用涉及环氧化和羟基化的连续两步法。 具体地，该方法包括向天然油中加入过氧酸，其中所述天然油和所述过氧酸反应形成环氧化天然油，并将所述环氧化天然油加入到醇，水和氟硼酸催化剂的混合物中。 氟硼酸的催化量小于整个反应混合物的约0.5重量％，水的量为整个混合物的约10至30重量％。 环氧化天然油经历羟基化，形成天然油基多元醇。 本发明还包括通过在上述量的氟硼酸，醇和水的存在下对环氧化油进行水解来制备环氧化油的天然油基多元醇的方法。通过该方法制备的天然油基多元醇可以是 与异氰酸酯反应以形成聚氨酯，这是本发明的另一个实施方案。 或者，诸如二氧化硅的填料可以在与异氰酸酯反应形成聚氨酯之前与这些天然油基多元醇组合。 在本发明的另一个实施方案中，由天然油基多元醇制成的聚氨酯可用于形成用于电气应用的电绝缘铸塑树脂。

    Process for the preparation of vegetable oil-based polyols and electroinsulating casting compounds created from vegetable oil-based polyols
    4.
    发明授权
    Process for the preparation of vegetable oil-based polyols and electroinsulating casting compounds created from vegetable oil-based polyols 有权
    植物油基多元醇的制备方法和由植物油基多元醇制成的电铸电铸化合物的方法

    公开(公告)号：US06573354B1

    公开(公告)日：2003-06-03

    申请号：US09567997

    申请日：2000-05-10

    申请人： Zoran Petrovic ,  Andrew Guo ,  Ivan Javni

    发明人： Zoran Petrovic ,  Andrew Guo ,  Ivan Javni

    IPC分类号： C08J300

    CPC分类号： C08G18/36 ,  C07D303/42 ,  C08G2190/00

    摘要： A vegetable oil-based polyol is made by adding a peroxyacid to vegetable oil wherein said peroxyacid reacts with said vegetable oil to form epoxidized vegetable oil and adding said epoxidized vegetable oil to a mixture of an alcohol, water, and a catalytic amount of fluoboric acid so as to form a vegetable oil-based polyol. A further embodiment of the present invention involves making a vegetable oil-based polyol using an epoxidized vegetable oil as the starting material. The epoxidized vegetable oil undergoes hydroxylation by the same process as outlined above. According to another aspect of the present invention, the vegetable oil-based polyol formed by the novel methods of this invention may be reacted with an isocyanate to form a polyurethane. Alternatively, a filler such as silica may be combined with the vegetable oil-based polyol before it is reacted with the isocyanate. These polyurethanes made from vegetable oil-based polyols may be used to form electroinsulating casting resins.

    摘要翻译： 通过向植物油中加入过氧酸而制备植物油性多元醇，其中所述过氧酸与所述植物油反应形成环氧化植物油，并将所述环氧化植物油加入到醇，水和催化量的氟硼酸的混合物中 以形成植物油基多元醇。 本发明的另一个实施方案涉及使用环氧化植物油作为原料制备植物油基多元醇。 环氧化植物油通过与上述相同的方法进行羟基化。 根据本发明的另一方面，通过本发明的新方法形成的植物油基多元醇可以与异氰酸酯反应形成聚氨酯。 或者，诸如二氧化硅的填料可以在与异氰酸酯反应之前与植物油基多元醇组合。 这些由植物油基多元醇制成的聚氨酯可用于形成电绝缘铸塑树脂。

    Modified vegetable oil-based polyols
    5.
    发明申请
    Modified vegetable oil-based polyols 有权
    改性植物油基多元醇

    公开(公告)号：US20060041157A1

    公开(公告)日：2006-02-23

    申请号：US11165962

    申请日：2005-06-24

    申请人： Zoran Petrovic ,  Ivan Javni ,  Alisa Zlatanic ,  Andrew Guo

    发明人： Zoran Petrovic ,  Ivan Javni ,  Alisa Zlatanic ,  Andrew Guo

    IPC分类号： C07C67/31

    CPC分类号： C08G18/36 ,  C07D303/42

    摘要： Methods of making unsaturated modified vegetable oil-based polyols are described. Also described are methods of making oligomeric modified vegetable oil-based polyols. An oligomeric composition having a modified fatty acid triglyceride structure is also described. Also, methods of making a polyol including hydroformylation and hydrogenation of oils in the presence of a catalyst and support are described.

    摘要翻译： 描述了制备不饱和改性植物油基多元醇的方法。 还描述了制备低聚改性植物油基多元醇的方法。 还描述了具有改性脂肪酸甘油三酯结构的低聚组合物。 另外，描述了在催化剂和载体的存在下制备包括加氢甲酰基化和油化氢化的多元醇的方法。

    Process for the preparation of vegetable oil-based polyols and electroninsulating casting compounds created from vegetable oil-based polyols
    6.
    发明授权
    Process for the preparation of vegetable oil-based polyols and electroninsulating casting compounds created from vegetable oil-based polyols 有权
    由植物油基多元醇制备的植物油基多元醇和电子注射铸造化合物的制备方法

    公开(公告)号：US6107433A

    公开(公告)日：2000-08-22

    申请号：US187992

    申请日：1998-11-06

    申请人： Zoran Petrovic ,  Andrew Guo ,  Ivan Javni

    发明人： Zoran Petrovic ,  Andrew Guo ,  Ivan Javni

    IPC分类号： C07D303/42 ,  C08G18/36 ,  C08G83/00 ,  C07D301/00 ,  C07D301/14 ,  C07D301/19 ,  C07D303/00

    CPC分类号： C08G18/36 ,  C07D303/42 ,  C08G2190/00

    摘要： A vegetable oil-based polyol is made by adding a peroxyacid to vegetable oil wherein said peroxyacid reacts with said vegetable oil to form epoxidized vegetable oil and adding said epoxidized vegetable oil to a mixture of an alcohol, water, and a catalytic amount of fluoboric acid so as to form a vegetable oil-based polyol. A further embodiment of the present invention involves making a vegetable oil-based polyol using an epoxidized vegetable oil as the starting material. The epoxidized vegetable oil undergoes hydroxylation by the same process as outlined above. According to another aspect of the present invention, the vegetable oil-based polyol formed by the novel methods of this invention may be reacted with an isocyanate to form a polyurethane. Alternatively, a filler such as silica may be combined with the vegetable oil-based polyol before it is reacted with the isocyanate. These polyurethanes made from vegetable oil-based polyols may be used to form electroinsulating casting resins.

    摘要翻译： 通过向植物油中加入过氧酸而制备植物油性多元醇，其中所述过氧酸与所述植物油反应形成环氧化植物油，并将所述环氧化植物油加入到醇，水和催化量的氟硼酸的混合物中 以形成植物油基多元醇。 本发明的另一个实施方案涉及使用环氧化植物油作为原料制备植物油基多元醇。 环氧化植物油通过与上述相同的方法进行羟基化。 根据本发明的另一方面，通过本发明的新方法形成的植物油基多元醇可以与异氰酸酯反应形成聚氨酯。 或者，诸如二氧化硅的填料可以在与异氰酸酯反应之前与植物油基多元醇组合。 这些由植物油基多元醇制成的聚氨酯可用于形成电绝缘铸塑树脂。

    Conforming shoe construction and gel compositions therefor
    9.
    发明授权
    Conforming shoe construction and gel compositions therefor 失效
    符合鞋结构及其凝胶成分

    公开(公告)号：US5766704A

    公开(公告)日：1998-06-16

    申请号：US614758

    申请日：1996-03-13

    申请人： Bernie Allen ,  Zoran Petrovic ,  Ivan Javni

    发明人： Bernie Allen ,  Zoran Petrovic ,  Ivan Javni

    IPC分类号： A43B7/02 ,  A43B7/14 ,  A43B7/16 ,  A43B7/18 ,  A43B17/16 ,  B29D35/12 ,  B29D35/14 ,  C08L71/02 ,  C08L33/24

    CPC分类号： B29D35/126 ,  A43B17/16 ,  A43B7/02 ,  A43B7/142 ,  A43B7/144 ,  A43B7/1495 ,  A43B7/16 ,  A43B7/18 ,  B29D35/146 ,  C08L71/02 ,  Y10T428/13

    摘要： The invention provides a conforming medium containing gels for customized fitting components, such as those used in a shoe. The invention further includes environmentally-responsive gels that are temperature-responsive so that they will react to body heat to transition from a liquid to a gel state or a gel state to a liquid state. The invention optionally includes thermally-sensitive dyes and other colorants in the environmentally-responsive gels. Furthermore, the invention is directed to an article for conforming to the contours of an object having isolation means, such as a bladder of a flexible member, to contain the environmentally-responsive gel therein.

    摘要翻译： 本发明提供了一种含有用于定制装配部件的凝胶的合适介质，例如在鞋中使用的那些。 本发明还包括温度敏感的环境响应性凝胶，使得它们将与体热反应从液体转变为凝胶状态或凝胶状态至液体状态。 本发明任选地包括在环境敏感性凝胶中的热敏染料和其它着色剂。 此外，本发明涉及一种用于符合具有隔离装置（例如柔性构件的囊）的物体的轮廓以在其中容纳环境响应性凝胶的物品。

    Golf shoe having spike socket spine system
    10.
    发明授权
    Golf shoe having spike socket spine system 失效
    高尔夫鞋具有尖钉套筒脊柱系统

    公开(公告)号：US5987783A

    公开(公告)日：1999-11-23

    申请号：US462310

    申请日：1995-06-05

    申请人： Bernie Allen ,  Zoran Petrovic

    发明人： Bernie Allen ,  Zoran Petrovic

    IPC分类号： A43B5/00 ,  A43B13/12 ,  A43B13/18 ,  A43C15/02 ,  A43C15/16

    CPC分类号： A43B13/223 ,  A43B13/026 ,  A43B13/12 ,  A43B13/189 ,  A43B5/001 ,  A43C15/02 ,  A43C15/161 ,  Y10T428/24331 ,  Y10T428/249921 ,  Y10T428/249958 ,  Y10T428/249972 ,  Y10T428/249978 ,  Y10T428/31551 ,  Y10T428/31554

    摘要： The present invention is an improved golf shoe which incorporates a spike socket spine frame system that extends throughout the shoe sole for receiving all of the spike receptacles and is embedded in the outsole. The spine frame provides improved shoe performance and spike location and is made of a material that is stiffer than the outsole material. More particularly, the shoe sole is comprised of a spike socket spine having seventeen spike socket locations: three spike sockets in the toe section, six spike sockets in the metatarsal section, four spike sockets in the shank section and four spike sockets in the heel section, for receiving the posts of the golf spikes.

    摘要翻译： 本发明是一种改进的高尔夫球鞋，它包括一个贯穿整个鞋底延伸的钉钉套筒脊框架系统，用于容纳所有的钉销容器并且嵌入在外底中。 脊柱框架提供改进的鞋子性能和尖钉位置，并且由比外底材料更硬的材料制成。 更具体地，鞋底由具有十七个尖钉插座位置的尖钉插座脊部组成：脚趾部分中的三个尖钉插座，跖部部分中的六个尖钉插座，柄部分中的四个尖钉插座和脚跟部分中的四个尖钉插座 ，用于接收高尔夫球杆的位置。