Dental zirconia blank having high relative density

    公开(公告)号:US12115032B2

    公开(公告)日:2024-10-15

    申请号:US18136575

    申请日:2023-04-19

    申请人: SHOFU INC.

    IPC分类号: A61C13/00 A61C13/08

    摘要: The present disclosure relates to a dental cutting zirconia blank having high relative density for preparing a dental restoration. More specifically, the present disclosure relates to a dental cutting zirconia blank which consists of a zirconia ceramics used for the cutting with the CAD/CAM system in the dental field, a semi-sinter zirconia blank (pre-sintered body) of which has high relative density, and which can provide a prosthesis device having high aesthetics after sintering. There is provided a dental cutting zirconia blank wherein the dental cutting zirconia blank has at least one layer consisting of zirconia powder containing 4 to 15 mol % of yttria or erbium oxide as a stabilizer, a relationship among pre-sintering density, final-sintering density and relative density satisfies the following relation:

    54≤Relative density (%)={(Pre-sintering density)/(Perfect-sintering density)}×100≤70.

    DENTAL PORCELAIN PASTE CONTAINING INORGANIC SALT

    公开(公告)号:US20240307273A1

    公开(公告)日:2024-09-19

    申请号:US18396126

    申请日:2023-12-26

    申请人: SHOFU INC.

    摘要: [Problem]
    To provide a dental porcelain paste that can maintain a constant paste property even during long-term storage, and that hardly generates carbonization and bubbles during firing even in the case of containing organic components.
    [Solution]
    To provide a dental porcelain paste for preparing a dental prosthesis device, comprising (a) base material glass having an average particle diameter D50 of 1 to 20 μm, (b) hydrophobized fine particle silica having an average primary particle diameter of 1 to 50 nm, (c) organic solvent having a boiling point of 100 to 300° C., and (d) inorganic salt.

    DENTAL RESIN-REINFORCED GLASS IONOMER CEMENT KIT

    公开(公告)号:US20240173211A1

    公开(公告)日:2024-05-30

    申请号:US18222577

    申请日:2023-07-17

    申请人: SHOFU INC.

    摘要: [Problem]
    To provide a dental resin-reinforced glass ionomer cement kit which can exhibit high adhesive property to tooth substance by a simple procedure without complicated operations and contains a dental tooth surface treatment material composition and a dental resin-reinforced glass ionomer cement composition.
    [Solution]
    To provide a dental resin-reinforced glass ionomer cement kit comprising a dental tooth surface treatment material composition (i) and a dental resin-reinforced glass ionomer cement composition (ii), wherein



    the dental tooth surface treatment material composition (i) contains

    (A) water-soluble organic solvent: 20% by mass or more and 79% by mass or less.
    (B) water: 20% by mass or more and 79% by mass or less, and
    (C) polymerizable monomer having acid anhydride structure: 1% by mass or more and 30% by mass or less, and


    the dental resin-reinforced glass ionomer cement composition (ii) contains

    (D) acid-reactive glass powder,
    (B) water,
    (E′) polymer of acidic group-containing polymerizable monomer,
    (F) tri or more functional (meth)acrylamide-based polymerizable monomer,
    (G) hydroxyl group-containing (meth)acrylate-based polymerizable monomer, and
    (H) polymerization initiator.

    DENTAL ZIRCONIA BLANK HAVING HIGH RELATIVE DENSITY

    公开(公告)号:US20230255734A1

    公开(公告)日:2023-08-17

    申请号:US18136575

    申请日:2023-04-19

    申请人: SHOFU INC.

    IPC分类号: A61C13/00 A61C13/08

    摘要: The present disclosure relates to a dental cutting zirconia blank having high relative density for preparing a dental restoration. More specifically, the present disclosure relates to a dental cutting zirconia blank which consists of a zirconia ceramics used for the cutting with the CAD/CAM system in the dental field, a semi-sinter zirconia blank (pre-sintered body) of which has high relative density, and which can provide a prosthesis device having high aesthetics after sintering. There is provided a dental cutting zirconia blank wherein the dental cutting zirconia blank has at least one layer consisting of zirconia powder containing 4 to 15 mol % of yttria or erbium oxide as a stabilizer, a relationship among pre-sintering density, final-sintering density and relative density satisfies the following relation:


    54≤Relative density (%)={(Pre-sintering density)/(Perfect-sintering density)}×100≤70

    Dental zirconia blank having high relative density

    公开(公告)号:US11660172B2

    公开(公告)日:2023-05-30

    申请号:US15805396

    申请日:2017-11-07

    申请人: SHOFU INC.

    IPC分类号: A61C13/00 A61C13/08

    摘要: The present disclosure relates to a dental cutting zirconia blank having high relative density for preparing a dental restoration. More specifically, the present disclosure relates to a dental cutting zirconia blank which consists of a zirconia ceramics used for the cutting with the CAD/CAM system in the dental field, a semi-sinter zirconia blank (pre-sintered body) of which has high relative density, and which can provide a prosthesis device having high aesthetics after sintering. There is provided a dental cutting zirconia blank wherein the dental cutting zirconia blank has at least one layer consisting of zirconia powder containing 4 to 15 mol % of yttria or erbium oxide as a stabilizer, a relationship among pre-sintering density, final-sintering density and relative density satisfies the following relation:

    54≤Relative density(%)={(Pre-sintering density)/(Perfect-sintering density)}×100≤70.

    SINTERING METHOD FOR DENTAL ZIRCONIA CALCINED BODY

    公开(公告)号:US20230082975A1

    公开(公告)日:2023-03-16

    申请号:US17828656

    申请日:2022-05-31

    申请人: SHOFU INC.

    IPC分类号: C04B35/48 C04B35/64

    摘要: [Problem]
    A technique for improving translucency in order to prepare a zirconia sintered body having high translucency without using special equipment, has been required.
    [Solution]
    To provide A sintering method for a dental zirconia calcined body containing 5.5 mol % to 7.0 mol % of a stabilizer, wherein the method satisfies the following (a) to (c). (a) an average rate of temperature increase in the section from room temperature to 1300° C. is 9° C./min or more. (b) an average rate of temperature increase in the section from 1300° C. to 1400° C. is 0.6° C./min or more and 3° C./min or less. (c) an average rate of temperature increase in the section from 1400° C. to the maximum temperature of the sintering process is 0.5° C./min or more and 2.5° C./min or less.

    Dental glass ionomer cement composition

    公开(公告)号:US11504306B2

    公开(公告)日:2022-11-22

    申请号:US17032212

    申请日:2020-09-25

    申请人: SHOFU INC.

    IPC分类号: A61K6/889 A61K6/77 A61C5/00

    摘要: A dental glass ionomer cement composition that exhibits high mechanical properties. In particular, the dental glass ionomer cement composition of the present disclosure comprising (a) non-crosslinked polyalkenoic acid, (b) water, (c) crosslinked polyalkenoic acid: 0.01 to 10 wt. %, and (d) acid-reactive glass powder, exhibits extremely high compressive strength by including the crosslinked polyalkenoic acid in the specified content range.

    DENTAL PHOTOCURABLE COMPOSITION CONTAINING HIGH SOLUBLE PHOTOACID GENERATOR

    公开(公告)号:US20220287920A1

    公开(公告)日:2022-09-15

    申请号:US17201165

    申请日:2021-03-15

    申请人: SHOFU INC.

    IPC分类号: A61K6/62 A61K6/887

    摘要: To provide a dental photocurable composition which can exhibit excellent mechanical characteristics even after returning from a low temperature to room temperature.
    To provide a dental photocurable composition, comprising (A) polymerizable monomer, (B) photosensitizer, (C) photoacid generator and (D) photopolymerization accelerator and the (C) photoacid generator may include only (C-1) iodonium salt-based compound of an anion having log S of −4 or less.