Quartz glass crucible
    1.
    发明授权

    公开(公告)号:US11821103B2

    公开(公告)日:2023-11-21

    申请号:US17267283

    申请日:2019-06-04

    发明人: Yuji Baba

    IPC分类号: C30B15/10 C30B35/00

    CPC分类号: C30B15/10 C30B35/002

    摘要: A quartz glass crucible including a bottom portion, a curved portion, and a straight body portion, where the quartz glass crucible includes an outer layer including opaque quartz glass containing bubbles therein, and an inner layer including transparent quartz glass, the outer layer includes a plurality of layers in a part of the straight body portion, out of the plurality of layers, one layer having a devitrification spot number of 50/cm3 or more and 70/cm3 or less when the quartz glass crucible is heated at 1600° C. for 24 hours, and a layer positioned inwards of the devitrifiable layer in a thickness direction of the quartz glass crucible is a low devitrification layer having a spot number of 2/cm3 or less when the quartz glass crucible is heated at 1600° C. for 24 hours. This provides a quartz glass crucible suppressed from deformation due to heating and excessive progression of devitrification.

    SILICA GLASS DISC HAVING DIMPLES FORMED THEREON

    公开(公告)号:US20220402812A1

    公开(公告)日:2022-12-22

    申请号:US17836704

    申请日:2022-06-09

    IPC分类号: C03C15/00 C23C16/455

    摘要: Provided is a silica glass disc in which the deformation amount thereof in heat treatment is minimized, and the surface area of a silica glass surface can be increased. There is provided a silica glass disc, including a dimple forming area in which a large number of dimples are formed on at least one of a front surface or a back surface of a silica glass body, and the dimples in the dimple forming area are regularly formed. It is preferred that the dimples be formed by a laser.

    SILICA GLASS MEMBER FOR HERMETIC SEALING OF ULTRAVIOLET SMD LED ELEMENT AND METHOD FOR MANUFACTURING QUARTZ GLASS MEMBER FOR ULTRAVIOLET LED

    公开(公告)号:US20210226105A1

    公开(公告)日:2021-07-22

    申请号:US16306185

    申请日:2017-05-19

    摘要: Provided is a silica glass member for hermetic sealing of an ultraviolet SMD LED element to be suitably used for hermetic sealing of, and as a transmission window material for, a surface mount-type package (SMD) having an ultraviolet LED mounted thereon and configured to emit ultraviolet light in a wavelength range of from 200 nm to 350 nm. The silica glass member for hermetic sealing includes a silica glass substrate, which is homogeneously and integrally formed without an internal boundary, wherein the silica glass substrate has: a first surface on an inside opposed to an SMD LED element; and a second surface on an outside corresponding to the first surface, wherein an outer peripheral portion of the first surface has formed therein a substrate joining plain surface for joining to the container outer periphery joining plain surface, and wherein the second surface on the outside corresponding to the first surface has formed therein a lens-like convex portion configured to process emitted light from the ultraviolet SMD LED element.

    Method for producing a quartz glass crucible having a roughened inner surface region for pulling single crystal silicon

    公开(公告)号:US10323334B2

    公开(公告)日:2019-06-18

    申请号:US15327206

    申请日:2015-06-01

    发明人: Yuji Baba

    摘要: The present invention is a method for producing a quartz glass crucible for pulling a single crystal silicon from a silicon melt held therein, including the steps of: producing a quartz glass crucible having an outer layer including an opaque quartz glass containing bubbles therein and an inner layer including a transparent quartz glass containing substantially no bubbles; roughening a region of an inner surface of the produced quartz glass crucible, the region being in contact with the silicon melt when holding the silicon melt; and heating the quartz glass crucible having the roughened inner surface to crystallize a surface of the roughened region. This can produce a quartz glass crucible for pulling a single crystal silicon which can suppress generation of a brown ring on the inner surface of the crucible during pulling the single crystal silicon and can suppress crystallinity disorder of the single crystal silicon.

    Single-crystal silicon pulling silica container and method for producing the same
    6.
    发明授权
    Single-crystal silicon pulling silica container and method for producing the same 有权
    单晶硅拉硅胶容器及其制造方法

    公开(公告)号:US09376761B2

    公开(公告)日:2016-06-28

    申请号:US14006169

    申请日:2012-11-08

    发明人: Shigeru Yamagata

    摘要: The present invention is directed to a single-crystal silicon pulling silica container, the silica container including a straight body portion, a curved portion, and a bottom portion, wherein the OH group concentration in the straight body portion is 30 to 300 ppm by mass, the OH group concentration in the bottom portion is 30 ppm by mass or less, and the difference in the OH group concentration between the straight body portion and the bottom portion is 30 ppm by mass or more. As a result, a low-cost single-crystal silicon pulling silica container, the silica container that can reduce cavity defects called voids and pinholes in pulled single crystal silicon, is provided.

    摘要翻译: 本发明涉及一种单晶硅拉硅石容器,该二氧化硅容器包括直体部分,弯曲部分和底部,其中直体部分中的OH基浓度为30〜300质量ppm ,底部的OH基浓度为30质量ppm以下,直体部与底部之间的OH基浓度的差为30质量ppm以上。 结果,提供了一种低成本的单晶硅拉硅石容器,可以减少被称为空穴的凹陷的二氧化硅容器和拉制的单晶硅中的针孔。

    Black synthetic quartz glass with transparent layer and method for producing the same
    7.
    发明授权
    Black synthetic quartz glass with transparent layer and method for producing the same 有权
    具有透明层的黑色合成石英玻璃及其制造方法

    公开(公告)号:US09051203B2

    公开(公告)日:2015-06-09

    申请号:US13614398

    申请日:2012-09-13

    摘要: Provided in a facile manner are a black synthetic quartz glass with a transparent layer, which meets demands for various shapes, has a black portion satisfying required light shield property and emissivity in an infrared region, keeps a purity equivalent to that of a synthetic quartz glass in terms of metal impurities, has a high-temperature viscosity characteristic comparable to that of a natural quartz glass, can be subjected to high-temperature processing such as welding, does not release carbon from its surface, and is free of bubbles and foreign matter in the transparent layer and the black quartz glass, and at an interface between the transparent layer and the black quartz glass, and a production method therefor.

    摘要翻译: 以简单的方式提供了具有透明层的黑色合成石英玻璃,其满足各种形状的要求,具有满足所需遮光性的黑色部分和红外区域中的发射率,保持与合成石英玻璃相当的纯度 在金属杂质方面,具有与天然石英玻璃相当的高温粘度特性,可以进行诸如焊接的高温加工,不会从其表面释放碳,并且没有气泡和异物 在透明层和黑色石英玻璃中,以及在透明层和黑色石英玻璃之间的界面处,及其制造方法。

    Silica container and method for producing the same
    8.
    发明授权
    Silica container and method for producing the same 有权
    二氧化硅容器及其制造方法

    公开(公告)号:US08915097B2

    公开(公告)日:2014-12-23

    申请号:US13797028

    申请日:2013-03-12

    摘要: Producing a silica container includes forming a powder mixture by adding an Al compound or a crystal nucleating agent into a first powdered raw material; preliminarily molding to an intended shape by feeding the powder mixture to an inner wall of an outer frame while rotating the outer frame having aspiration holes; forming a silica substrate; and forming a transparent silica glass layer on an inner surface of the silica substrate, wherein the preliminarily molded article is degassed by aspiration from a peripheral side and heated from inside the preliminarily molded article at high temperature making a peripheral part of the preliminarily molded article to a sintered body while an inner part to a fused glass body, and a second powdered raw material having a higher silica purity than the first powdered raw material is spread from inside the silica substrate and heated from the inside at high temperature.

    摘要翻译: 生产二氧化硅容器包括通过向第一粉末原料中加入Al化合物或晶体成核剂来形成粉末混合物; 通过在将具有抽吸孔的外框架旋转的同时将粉末混合物进料到外框的内壁,预先成型为预期的形状; 形成二氧化硅基板; 在二氧化硅基板的内表面上形成透明的二氧化硅玻璃层,其中预成型品通过从外周侧抽吸脱气并在高温下从预成型品内部加热,使预成型品的周边部分被加热至 将熔融玻璃体的内部部分的烧结体和比第一粉末状原料高的二氧化硅纯度的第二粉末原料从二氧化硅基板的内部扩散并在高温下从内部加热。

    SINGLE-CRYSTAL SILICON PULLING SILICA CONTAINER AND PRODUCING METHOD THEREOF
    9.
    发明申请
    SINGLE-CRYSTAL SILICON PULLING SILICA CONTAINER AND PRODUCING METHOD THEREOF 审中-公开
    单晶硅拉丝二氧化硅容器及其制造方法

    公开(公告)号:US20140150715A1

    公开(公告)日:2014-06-05

    申请号:US14234588

    申请日:2013-03-18

    发明人: Shigeru Yamagata

    IPC分类号: C30B15/10 C03B11/10 C03B11/02

    摘要: A single-crystal silicon pulling silica container includes: a transparent layer made of transparent silica glass in an inner side of the silica container, and an opaque layer made of opaque silica glass containing gaseous bubbles in an outer side of the silica container, wherein the transparent layer is constituted of a high-OH group layer that is placed in an inner surface side of the silica container and contains the OH group at a concentration of 200 to 2000 ppm by mass and a low-OH group layer that has the OH group concentration lower than that of the high-OH group layer, and Ba is applied to the inner surface of the high-OH group layer at a concentration of 25 to 1000 μg/cm2.

    摘要翻译: 单晶硅拉硅石容器包括:在二氧化硅容器的内侧由透明石英玻璃制成的透明层和在二氧化硅容器的外侧含有气泡的不透明石英玻璃制成的不透明层,其中, 透明层由置于二氧化硅容器的内表面侧且含有浓度为200〜2000质量ppm的OH基和具有OH基的低-OH基层构成的高OH基层构成 浓度低于高-OH基团的浓度,Ba以25〜1000μg/ cm 2的浓度施加到高-OH基层的内表面。

    SINGLE-CRYSTAL SILICON PULLING SILICA CONTAINER AND MANUFACTURING METHOD THEREOF
    10.
    发明申请
    SINGLE-CRYSTAL SILICON PULLING SILICA CONTAINER AND MANUFACTURING METHOD THEREOF 有权
    单晶硅拉丝二氧化硅容器及其制造方法

    公开(公告)号:US20140053772A1

    公开(公告)日:2014-02-27

    申请号:US14004085

    申请日:2012-10-02

    发明人: Shigeru Yamagata

    IPC分类号: C30B15/10

    摘要: The present invention provides a single-crystal silicon pulling silica container including an outer layer made of opaque silica glass containing gaseous bubbles and an inner layer made of transparent silica glass that does not substantially contain the gaseous bubbles; the container also including: a bottom portion, a curved portion, and a straight body portion, wherein continuous grooves are formed on a surface of the inner layer from at least part of the bottom portion to at least part of the straight body portion through the curved portion. As a result, there are provided the single-crystal silicon pulling silica container that can reduce defects called voids or pinholes in the pulled single-crystal silicon and a method for manufacturing such a silica container.

    摘要翻译: 本发明提供一种单晶硅拉硅石容器,其包括由含有气泡的不透明石英玻璃制成的外层和由实质上不含有气泡的透明石英玻璃制成的内层; 所述容器还包括:底部,弯曲部分和直体部分,其中在所述内层的表面上从所述底部的至少一部分到所述直体部分的至少一部分通过所述内部部分形成连续的凹槽 弯曲部分。 结果,提供了可以减少拉制的单晶硅中的称为空隙或针孔的缺陷的单晶硅拉硅
    石容器以及这种二氧化硅容器的制造方法。