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    Process for selective liquid-liquid extraction of germanium
    3.
    发明授权
    Process for selective liquid-liquid extraction of germanium 失效
    选择性液 - 液萃取锗的工艺

    公开(公告)号：US4568526A

    公开(公告)日：1986-02-04

    申请号：US336608

    申请日：1982-01-04

    申请人： Denise Rouillard nee Bauer ,  Gerard Cote ,  Paolo Fossi ,  Bruno Marchon

    发明人： Denise Rouillard nee Bauer ,  Gerard Cote ,  Paolo Fossi ,  Bruno Marchon

    IPC分类号： C01G17/00 ,  C22B3/36

    CPC分类号： C01G17/003 ,  C22B3/0036 ,  Y02P10/234

    摘要： A process for selective liquid-liquid extraction of germanium from an aqueous acidic liquor containing, besides germanium, at least one other metal selected from the group which comprises cadmium, zinc, cobalt, iron, arsenic and nickel. This process includes extracting germanium from said aqueous liquor by contacting said liquor with an organic medium containing a diluent and an extractant, said diluent being immiscible with said aqueous liquor. The major part of germanium passes from said aqueous liquor to an organic phase which is subsequently submitted to a stripping step by contacting with an alkaline medium, with formation of an aqueous phase containing the major part of germanium from said aqueous liquor.

    摘要翻译： 从含有除了锗之外的至少一种选自包含镉，锌，钴，铁，砷和镍的组的其它金属的含水酸性液体中选择性液体 - 液体提取锗的方法。 该方法包括通过使所述液体与含有稀释剂和萃取剂的有机介质接触从所述含水液体中提取锗，所述稀释剂与所述含水液体不混溶。 锗的主要部分从所述含水液体经过有机相，随后通过与碱性介质接触进行剥离步骤，形成含有来自所述含水液体的主要部分锗的水相。

    Shingle-machine
    6.
    发明授权
    Shingle-machine 失效

    公开(公告)号：US12105A

    公开(公告)日：1854-12-19

    申请号：US12105D

    CPC分类号： C01G17/003

    METHOD FOR PRODUCING HIGH PURITY GERMANE BY A CONTINUOUS OR SEMI-CONTINUOUS PROCESS
    7.
    发明申请
    METHOD FOR PRODUCING HIGH PURITY GERMANE BY A CONTINUOUS OR SEMI-CONTINUOUS PROCESS 有权
    通过连续或半连续生产高纯度德国的方法

    公开(公告)号：US20150158738A1

    公开(公告)日：2015-06-11

    申请号：US14540466

    申请日：2014-11-13

    申请人： Gelest Technologies, Inc.

    发明人： Barry C. ARKLES ,  George A. TIMBERLAKE, JR.

    IPC分类号： C01G17/00 ,  B01D53/04 ,  F25J3/08 ,  B01D53/047

    CPC分类号： C01G17/003 ,  B01D53/0462 ,  B01D53/047 ,  B01D2253/108 ,  B01D2256/16 ,  B01D2257/55 ,  C01B3/56 ,  C01B6/06 ,  C01G17/00 ,  F25J3/08

    摘要： A continuous or semi-continuous process for producing a high purity germane includes (a) preparing a reaction mixture containing hydrogen and crude germane and (b) separating the hydrogen from the crude germane by a pressure swing adsorption process. The pressure swing adsorption process results in a hydrogen-rich product stream and a germane-rich product stream.The method further includes (c) purifying the germane-rich product stream by continuous distillation thereof to remove impurities therefrom and to produce a high purity germane containing less than 0.1 volume percent of impurities.

    摘要翻译： 用于生产高纯度锗烷的连续或半连续方法包括（a）制备含有氢和粗锗烷的反应混合物，和（b）通过变压吸附法从粗锗烷中分离出氢。 变压吸附过程产生富氢产物流和富含锗的产物流。 该方法还包括（c）通过连续蒸馏来纯化富含锗烷的产物流，以从其中除去杂质，并产生含有小于0.1体积％杂质的高纯度锗烷。

    Process for recovering germanium
    8.
    发明授权
    Process for recovering germanium 失效
    回收锗的工艺

    公开(公告)号：US5277882A

    公开(公告)日：1994-01-11

    申请号：US752542

    申请日：1991-09-25

    申请人： Jean H. Vliegen ,  Guy G. Haesebroek ,  Achille J. De Schepper

    发明人： Jean H. Vliegen ,  Guy G. Haesebroek ,  Achille J. De Schepper

    IPC分类号： C01G17/00 ,  C22B3/40

    CPC分类号： C22B3/0095 ,  C01G17/003 ,  Y02P10/234

    摘要： A germanium bearing sulphate solution containing indium and/or gallium is brought at pH 1-2.5 into contact with an organic phase, containing a substituted 8-hydroxyquinoline and an acid organophosphorus compound. So, in addition to germanium, indium and gallium are also extracted from the sulphate solution.

    摘要翻译： PCT No.PCT / BE90 / 00016 Sec。 371日期1991年9月25日 102（e）1991年9月25日PCT提交1990年4月11日PCT公布。 第WO90 / 13677号公报 日期为1990年11月15日。含有铟和/或镓的含锗硫酸盐溶液的pH为1-2.5，与含有取代的8-羟基喹啉和酸有机磷化合物的有机相接触。 因此，除了锗之外，还从硫酸盐溶液中提取铟和镓。

    Emulsion-forming composition
    9.
    发明授权
    Emulsion-forming composition 失效
    乳液形成组合物

    公开(公告)号：US4904412A

    公开(公告)日：1990-02-27

    申请号：US204378

    申请日：1988-06-09

    申请人： Karl Schugerl ,  Wilfried Gutknecht

    发明人： Karl Schugerl ,  Wilfried Gutknecht

    IPC分类号： B01D17/06 ,  B01D61/40 ,  B01F17/52 ,  C01G17/00 ,  C01G28/00

    CPC分类号： C01G28/001 ,  B01D61/40 ,  C01G17/003 ,  Y10S423/14 ,  Y10S516/915

    摘要： An emulsion-forming composition for forming an emulsion for use in a process for selectively recovering germanium or arsenic from an aqueous solution thereof by liquid membrane technology is disclosed, said composition consisting essentially of: a solvent mixture consisting essentially of specified amounts of a hydrocarbon which is a predominantly straight-chain saturated C.sub.16 -C.sub.20 hydrocarbon or kerosine, a mononuclear aromatic hydrocarbon (pref. xylene), and a halogenated C.sub.1 -C.sub.5 hydrocarbon (pref. CCl.sub.4); and more than 0.1% by weight of an oil-soluble polyisobutylene-succinic anhydride/polyamine condensation product.

    Process for selective liquid-liquid extraction of germanium
    10.
    发明授权
    Process for selective liquid-liquid extraction of germanium 失效
    选择性液 - 液萃取锗的工艺

    公开(公告)号：US4389379A

    公开(公告)日：1983-06-21

    申请号：US178583

    申请日：1980-08-15

    申请人： Denise Rouillard epouse Bauer ,  Gerard Cote ,  Paolo Fossi ,  Bruno Marchon

    发明人： Denise Rouillard epouse Bauer ,  Gerard Cote ,  Paolo Fossi ,  Bruno Marchon

    IPC分类号： C01G17/00 ,  C22B3/36 ,  C22B19/00 ,  C22B19/20 ,  C22B41/00

    CPC分类号： C22B3/0037 ,  C01G17/003 ,  Y02P10/234

    摘要： A process for selective liquid-liquid extraction of germanium from an aqueous acidic liquor containing, besides germanium, at least another metal selected from the group which comprises cadmium, zinc, cobalt and nickel. This process includes extracting germanium from said aqueous liquor by contacting said liquor with an organic medium containing a diluent and an extractant, said diluent being immiscible with said aqueous liquor. The major part of germanium passes from said aqueous liquor to an organic phase which is subsequently submitted to a stripping step by contacting with an alkaline medium, with formation of an aqueous phase containing the major part of germanium from said aqueous liquor.

    摘要翻译： 从含有除锗之外的至少另一种选自包含镉，锌，钴和镍的金属的含水酸性液体中选择性液体 - 液体提取锗的方法。 该方法包括通过使所述液体与含有稀释剂和萃取剂的有机介质接触从所述含水液体中提取锗，所述稀释剂与所述含水液体不混溶。 锗的主要部分从所述含水液体经过有机相，随后通过与碱性介质接触进行剥离步骤，形成含有来自所述含水液体的主要部分锗的水相。