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公开(公告)号：US20180155208A1
公开(公告)日：2018-06-07
申请号：US15806183
申请日：2017-11-07
CPC分类号： C01G51/06 , C01B17/64 , C01D5/00 , C01D5/18 , C01D15/08 , C01G51/04 , C01G51/42 , C01G53/006 , C02F2103/34 , H01M10/052 , H01M10/0525 , H01M2004/028
摘要： A process for water removal and/or recycling of sodium sulfate and/or sodium dithionate containing liquors derived from processing cobalt resource material essentially free of lithium comprising the steps of precipitation of cobalt as cobaltous carbonate or cobaltous hydroxide followed by removal thereof from the liquor, crystallization of sodium sulfate and sodium dithionate and removal of the crystals, followed by heating of the crystals to anhydrous sodium sulfate, sulphur dioxide and water and then separating the anhydrous sodium sulfate.
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2.发明公开公开(公告)号：US20230160036A1
公开(公告)日：2023-05-25
申请号：US17922644
申请日：2021-05-21
发明人： Suk Joon PARK , Myung Gyu LEE , Jeong Sik HONG , So Yeong BYUN , Gwang Seok LEE , Jong Sun PARK , Beom Seok SEO , Min Woo LEE , Da Mo A KIM , Hui Sang KIM , A Ram PARK
CPC分类号： C22B23/043 , C22B7/007 , C22B26/12 , C22B3/08 , C22B1/005 , C22B23/0453 , H01M10/54 , C01G53/06 , C01G51/06
摘要： A method according to an embodiment is for recovering a valuable metal from a waste electrode material of a lithium secondary battery by using lithium carbonate. An anode-cathode mixed electrode material that has been separated by draining, crushing, screening, and sorting a waste lithium secondary battery is preprocessed. A precipitation operation performed by adding lithium carbonate (Li2CO3) to a metal melt acquired by performing sulfuric acid dissolution using sulfuric acid. A valuable metal such as nickel, cobalt, manganese, aluminum, and copper is recovered as a residue in the form of a carbonate composite, and a lithium sulfate (Li2SO4) aqueous solution including lithium is recovered as a filtrate.
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3.发明授权Method for producing fine spherical particles of carbonate or hydroxide of nickel, cobalt or copper 有权用于生产镍，钴或铜的碳酸盐或氢氧化物的细球形颗粒的方法公开(公告)号：US06197273B1
公开(公告)日：2001-03-06
申请号：US09463021
申请日：2000-03-22
申请人： Kazuhiko Nagano , Kazunobu Abe , Shigefumi Kamisaka , Kiyoshi Fukai , Tsutomu Hatanaka , Shinji Ohgama , Hiroshi Nakao , Minoru Yoneda , Hideto Mizutani
发明人： Kazuhiko Nagano , Kazunobu Abe , Shigefumi Kamisaka , Kiyoshi Fukai , Tsutomu Hatanaka , Shinji Ohgama , Hiroshi Nakao , Minoru Yoneda , Hideto Mizutani
IPC分类号： C01B3124
CPC分类号： C01G53/06 , B01J23/70 , B01J37/00 , B22F9/026 , C01B13/328 , C01G3/00 , C01G3/02 , C01G51/04 , C01G51/06 , C01G53/04 , C01P2002/02 , C01P2002/72 , C01P2004/03 , C01P2004/32 , C01P2004/51 , C01P2004/61 , C01P2004/62
摘要： The invention provides a process for production of fine spherical particles of a carbonate or a hydroxide of nickel, cobalt or copper which comprises: dissolving a carbonate or a hydroxide of nickel, cobalt or copper having the general formula (I) M(CO3)x/2.(OH)y wherein M represents Ni, Co or Cu, and x and y are numerals satisfying the followings: 0≦x≦2, 0≦y≦2 and x+y=2, in aqueous ammonia, converting the resulting solution to a W/O emulsion containing droplets of the solution in a non-aqueous medium, and then removing volatile components including ammonia from within the droplets, thereby precipitating a basic carbonate or a hydroxide of a metal selected from nickel, cobalt and copperin the droplets. The fine spherical particles of a carbonate or a hydroxide of nickel, cobalt or copper obtained according to the process of the invention are especially useful as a precursor for the manufacture of uniform, fine spherical particles of nickel, copper or cobalt metal, as well as useful as themselves as a catalyst for use in organic synthesis, a carrier, a pigment, a filler or a glaze.
摘要翻译： 本发明提供一种生产镍，钴或铜的碳酸盐或氢氧化物的细球形颗粒的方法，其包括：将通式（I）的其中M表示Ni的镍，钴或铜的碳酸盐或氢氧化物溶解， Co或Cu，x和y是在氨水中将满足以下条件的数字：0 <= x <= 2,0 <= y <= 2和x + y = 2，将所得溶液转化成W / O乳液 在非水介质中含有溶液的液滴，然后从液滴内除去包括氨的挥发性组分，从而沉淀出液滴中选自镍，钴和铜的金属的碱性碳酸盐或氢氧化物。微球形颗粒 根据本发明的方法获得的镍，钴或铜的碳酸盐或氢氧化物特别可用作制造镍，铜或钴金属的均匀的细小球形颗粒的前体，并且作为其自身可用作 用于有机合成的催化剂，载体，颜料，填料或釉料。
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5.发明授权
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公开(公告)号：US20230382760A1
公开(公告)日：2023-11-30
申请号：US18231805
申请日：2023-08-09
申请人： GUANGDONG BRUNP RECYCLING TECHNOLOGY CO., LTD. , HUNAN BRUNP RECYCLING TECHNOLOGY CO., LTD. , HUNAN BRUNP EV RECYCLING CO., LTD.
发明人： Xinghua Lu , Changdong Li , Dingshan Ruan , Genghao Liu , Yong Cai , Bin Li
IPC分类号： C01G51/06
CPC分类号： C01G51/06 , C01P2006/80 , C01P2004/51 , C01P2004/61 , C01P2006/40
摘要： The present disclosure discloses a preparation method of platy aluminum-doped cobalt carbonate and use thereof. The preparation method includes the following steps: S1: mixing a cobalt salt, an aluminum salt, and a polyhydroxy compound to prepare a mixed solution; S2: mixing the mixed solution with an ammonium bicarbonate solution, adjusting a pH, and heating and stirring to allow a reaction to obtain a seed crystal solution; and S3: adding the mixed solution and an ammonium bicarbonate solution to the seed crystal solution, adjusting a pH, and heating and stirring to allow a reaction, during which a solid content in a slurry is controlled at 20% to 40% until a particle size in the slurry grows to a target value; and separating out, washing, and drying a solid phase to obtain the platy aluminum-doped cobalt carbonate.
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7.发明授权Spheroidally agglomerated basic cobalt(II) carbonate and spheroidally agglomerated cobalt(II) hydroxide, process for their production and their use 失效碳酸球形碳酸碱式钴（II）和球形聚集的氢氧化钴（II），其生产和使用过程公开(公告)号：US06699453B1
公开(公告)日：2004-03-02
申请号：US08952913
申请日：1997-11-24
IPC分类号： C01G5106
CPC分类号： C01G51/06 , C01G51/04 , C01P2004/03 , C01P2004/10 , C01P2004/20 , C01P2004/32 , C01P2004/50 , C01P2004/61 , C01P2004/62 , C01P2006/10 , C01P2006/11 , C01P2006/12 , C01P2006/80 , H01M4/52
摘要： The present invention relates to basic cobalt(II) carbonate, agglomerated from fine primary particles and of general composition Co[(OH)2]a[CO3]1−a, where 0.1≦a≦0.9, and to spheroidal cobalt(II) hydroxide, to a process for producing them and to their use.
摘要翻译： 本发明涉及碳酸碱式钴（II），其由细一级颗粒凝聚，并且具有通常组成的Co [（OH）2] a [CO 3] 1-a，其中0.1 <= a <= 0.9，和球形钴（ II）氢氧化物，用于生产它们和使用它们的方法。
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公开(公告)号：US06183621B2
公开(公告)日：2001-02-06
申请号：US08981079
申请日：1997-11-25
IPC分类号： C25B312
CPC分类号： C01G51/06 , C01G51/04 , C01P2006/60 , C01P2006/80 , C07C55/07 , C25B1/00
摘要： The present invention relates to processes for the production of cobalt(II) carbonates corresponding to the general formula Co[(OH)2]a[CO3]1−a, cobalt(II) carbonates and cobalt(II) oxalate carbonates obtainable by the process and the use thereof.
摘要翻译： 本发明涉及生产相应于通式Co [（OH）2] a [CO 3] 1-a，碳酸钴（II）和碳酸钴（II））的碳酸钴（II）的方法， 过程及其用途。
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公开(公告)号：US4002719A
公开(公告)日：1977-01-11
申请号：US615801
申请日：1975-09-22
申请人： Utah Tsao
发明人： Utah Tsao
CPC分类号： C22B23/0453 , C01G51/06 , C01G53/06 , C22B23/0492
摘要： An ammonium carbonate leach solution containing dissolved nickel and/or cobalt values is sprayed into a flash chamber to flash a portion of the ammonia therefrom, resulting in the production of a fine precipitate of nickel and/or cobalt carbonate. The solution is introduced into a stripping tower wherein remaining ammonia is stripped therefrom to precipitate further nickel and/or cobalt carbonate on the previously precipitated carbonate, which function as nuclei to reduce deposition in the column.
摘要翻译： 将含有溶解的镍和/或钴值的碳酸铵浸出溶液喷射到闪蒸室中以从其中闪蒸一部分氨，导致产生镍和/或碳酸钴的细沉淀物。 将溶液引入汽提塔，其中从其中除去剩余的氨，以沉淀在先前沉淀的碳酸盐上的进一步的镍和/或碳酸钴，其作为核以减少柱中的沉积。
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10.发明授权The separation of nickel from a mixture containing soluble compounds of nickel and cobalt 失效从含有可溶性镍和钴的化合物的混合物中分离镍
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