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14 条记录 (耗时 0.009 秒)

    Process for the manufacture of dialkyltin diiodide from tin and alkyl iodide
    1.
    发明授权
    Process for the manufacture of dialkyltin diiodide from tin and alkyl iodide 失效
    二丁基二锡的制备方法

    公开(公告)号：US3661958A

    公开(公告)日：1972-05-09

    申请号：US3661958D

    申请日：1969-06-10

    申请人： KUREHA CHEMICAL IND CO LTD

    发明人： ONOZUKA MITSUO ,  IIDA KINJI

    IPC分类号： C07F7/22

    CPC分类号： C07F7/2236 ,  C07F7/2216

    摘要： A PROCESS FOR THE MANUFACTURE OF DIALKYLTIN DIIODIDES WHICH COMPRISES REACTING METALLIC TIN AND AN ALKYL IODIDE HAVING FROM 8 TO 24 CARBON ATOMS IN THE ALKYL MOIETY, SAID ALKYYL IODIDE BEING PRESENT IN A RATIO OF FROM 2.2 TO 4.0 MOLS OF ALKYYL IODIDE TO 1.0 GR.-ATOM OF SAID METALLIC TIN, AND FURTHER, SAID REACTION BEING CARRIED OUT IN THE PRESENCE OF FROM 0.0001-0.5 MOLS OF A CATALYST CONSISTING ESSENTIALLY OF NITROGEN-CONTAINING ORGANIC CATALYTIC COMPOUND SELECTED FROM THE GROUP CONSISTING OF A PRIMARY, SECONDARY, AND TERITARY AMINE, A HETEROCYCLIC AMINE, AND A LACTAM.

    Anti-fouling paints
    2.
    发明授权
    Anti-fouling paints 失效
    防滑涂料

    公开(公告)号：US3854960A

    公开(公告)日：1974-12-17

    申请号：US38758973

    申请日：1973-08-13

    申请人： SCHERING AG

    发明人： PLUM H ,  RUNGGAS F ,  VON HAAREN M ,  KRASE H

    IPC分类号： C09D5/08 ,  C07F7/22 ,  C09D5/16

    CPC分类号： C07F7/2236 ,  C09D5/1631

    摘要： Anti-fouling paints containing tributyl tin oxide as the antifouling agent wherein said tributyl tin oxide is present in the paint with colloidal silicic acid produced by the flame hydrolysis of silicon tetrachloride and/or montmorillonite modified with a quaternary ammonium salt.

    摘要翻译： 含有三丁基锡氧化物作为防污剂的防污涂料，其中所述三丁基锡氧化物通过用季铵盐改性的四氯化硅和/或蒙脱石的火焰水解产生的胶态硅酸存在于涂料中。

    Process of the manufacture of dialkyltin oxide
    5.
    发明授权
    Process of the manufacture of dialkyltin oxide 失效
    氧化铝氧化物的制备方法

    公开(公告)号：US3813424A

    公开(公告)日：1974-05-28

    申请号：US25924672

    申请日：1972-06-02

    申请人： KUREHA CHEMICAL IND CO LTD

    发明人： HAYASHI Y ,  ADACHI Y

    IPC分类号： C07F7/22

    CPC分类号： C07F7/2236 ,  C07F7/2216

    摘要： THE INVENTION RELATES TO THE PROCESS FOR THE DIRECT MANUFACTURE OF DIALKYTIN OXIDE THROUGH SUCH REACTION STEPS THAT ALKYL IODINE IS REACTED DIRECTLY WITH METALLIC TIN TO DIALKYTIN IODINE WHICH IS THEN HYDROLYZED TO THE DESIRED PRODUCT. THE MAIN OBJECT OF THE INVENTION IS TO PROVIDE A PROCESS FOR THE MANUFACTURE OF DIALKYLTIN OXIDE WITH LEAST POSSIBLE LOSS OF IODINE AND AT A MAXIUM POSSIBLE PURITY OF THE FINAL PRODUCT. FOR THIS PURPOSE, AN AQUEOUS ALKALINE SOLUTION APPEARED FROM A CERTAIN PROCESSING STAGE AND CONTAINING UNRECOVERED ALKALI METAL IODINE AFTER EXCUTION OF THE RECOVERY STEP THEREOF IS RETURNED TO SAID FIRST STEP FOR RECICULATION.

    Process for preparing dialkyltin compounds
    6.
    发明授权
    Process for preparing dialkyltin compounds 失效
    制备二烯丙基化合物的方法

    公开(公告)号：US3711524A

    公开(公告)日：1973-01-16

    申请号：US3711524D

    申请日：1971-07-28

    申请人： COON L

    发明人： LEEBRICK J

    IPC分类号： C07F7/22

    CPC分类号： C07F7/2236

    摘要： DIALKYTIN COMPOUNDS ARE PREPARED BY THE REACTION OF LOWER DIALKYL SULFATES AND METALLIC TIN. THE PRODUCT CAN BE HYDROLYZED TO GIVE THE CORRESPONDING DIALKYLTIN OXIDE.

    Divinyltin oxide and method of preparation
    10.
    发明授权
    Divinyltin oxide and method of preparation 失效
    氧化二乙烯基锡及其制备方法

    公开(公告)号：US2867642A

    公开(公告)日：1959-01-06

    申请号：US61066556

    申请日：1956-09-18

    申请人： METAL & THERMIT CORP

    发明人： RAMSDEN HUGH E ,  ROSENBERG SANDERS D

    IPC分类号： C07F7/22

    CPC分类号： C07F7/2236

    摘要： Divinyl tin oxide, a polymeric material composed of units of structure is made by the hydrolysis of divinyl tin chloride or bromide. It will copolymerize with vinyl chloride, styrene, vinyl silanes, methyl methacrylate or acrylates. It may also be used as a stabilizer in polyvinyl chloride compositions, as may epoxyethyl tin oxide, obtained by epoxidizing the unsaturated linkages. The preparation of the polymeric divinyl tin oxides takes place in a basic aqueous solution containing sufficient hydroxyl ions to replace all the halogen atoms with oxygen. Specified bases are Na and K hydroxides, carbonates and bicarbonates, Ca, Ba, NH4 and tetra-alkyl ammonium hydroxides, CaO, aniline, pyridine and morpholine. The divinyl tin halides may be added to the basic aqueous solution as such, or in the form of an organic solution (e.g. in benzine, toluene, xylene, pentane, hexane, heptane, cyclohexane, or an alcohol or ether). Uses.-P.V.C. stabilizers, as above. Anthelmintics for chicken feeds or medicines.ALSO:The invention comprises divinyltin oxide which is prepared by reacting divinyltin chloride or bromide with a basic compound in aqueous solution containing sufficient hydroxyl ions to replace all the halogen atoms by oxygen. Specified bases include sodium and potassium hydroxides, carbonates and bicarbonates, ammonium hydroxide, aniline, pyridine, morpholine, tetra-alkyl-ammonium hydroxides, calcium oxide and hydroxide and barium hydroxide. The divinyltin chloride or bromide may react with the aqueous solution in the pure state, or it may react in solution in an inert hydrocarbon or organic solvent (e.g. benzene, toluene, pentane, hexane, cyclohexane, an alcohol or ether). An inert atmosphere such as nitrogen may be maintained during the reaction if desired. Epoxy ethyl tin oxide may be obtained by epoxidizing the unsaturated linkages in divinyl tin oxide.