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    Process for the manufacture of mercaptocarboxylic acids from unsaturated carboxylic acids
    1.
    发明授权
    Process for the manufacture of mercaptocarboxylic acids from unsaturated carboxylic acids 失效
    从不饱和羧酸制备巯基羧酸的方法

    公开(公告)号：US06689907B1

    公开(公告)日：2004-02-10

    申请号：US09713189

    申请日：2000-11-16

    申请人： Yves Labat

    发明人： Yves Labat

    IPC分类号： C07C5300

    CPC分类号： C07C319/04 ,  C07C323/52

    摘要： A mercaptocarboxylic acid of formula (I) is prepared by reacting an unsaturated carboxylic acid of formula (II) with a hydrosulphide of formula ASH, A being an alkali metal cation or a cation NR3R4R5R6+, R3 to R6 each representing H or a hydrocarbon radical, or of formula Q(SH)2, Q being an alkaline-earth metal cation, by acidifying the resulting reaction medium in order to obtain the desired compound (I). According to the present invention, the reaction is carried out with a supply of H2S other than that supplied by the neutralization of the acid (II). In particular, H2S is introduced into the medium by a direct external supply. H2S can also be produced in situ by reacting the hydrosulphide with at least one acid introduced into the medium. The compound (I) is obtained with a very good selectivity.

    摘要翻译： 式（I）的巯基羧酸通过使式（II）的不饱和羧酸与式ASH的硫化氢反应制备，A为碱金属阳离子或阳离子NR 3 R 4 R 5 R 通过酸化所得到的反应介质，得到的反应介质酸化，得到反应介质，得到 所需化合物（I）。 根据本发明，除了通过酸（II）的中和提供的H2S供应之外，反应是进行的。 特别地，H2S通过直接外部电源引入介质中。 H2S也可以通过使硫化氢与引入到介质中的至少一种酸反应而原位制备。以非常好的选择性获得化合物（I）。

    Processes for preparing 3.3-dimethylbutyric acid
    3.
    发明授权
    Processes for preparing 3.3-dimethylbutyric acid 有权
    制备3.3-二甲基丁酸的方法

    公开(公告)号：US06686501B2

    公开(公告)日：2004-02-03

    申请号：US10068631

    申请日：2002-02-05

    申请人： Dennis E. Jackman

    发明人： Dennis E. Jackman

    IPC分类号： C07C5300

    CPC分类号： C07C51/353 ,  C07C53/126

    摘要： A process for preparing 3,3-dimethylbutyric acid includes the steps of reacting trimethylpyruvic acid with a first portion of hydrazine to obtain a ketazine, and treating the ketazine with base and a second portion of hydrazine.

    摘要翻译： 制备3,3-二甲基丁酸的方法包括使三甲基丙酮酸与肼的第一部分反应以获得酮连氮，并用肼和第二部分肼处理酮连氮的步骤。

    Acid oil-in-water emulsified composition
    4.
    发明授权
    Acid oil-in-water emulsified composition 有权
    酸性油包水乳化组合物

    公开(公告)号：US06635777B1

    公开(公告)日：2003-10-21

    申请号：US09926741

    申请日：2001-12-11

    申请人： Shigeru Kawai ,  Yoshihiro Konishi

    发明人： Shigeru Kawai ,  Yoshihiro Konishi

    IPC分类号： C07C5300

    CPC分类号： A23D7/011 ,  A23D7/0053 ,  A23L27/60 ,  A23L33/11

    摘要： Described is an acid oil-in-water emulsified composition comprising an oil phase having a diglycerides content of 30 wt. % or greater and a yolk, wherein a ratio of lysophospholipids to the whole phospholipids is at least 15% in terms of a phosphorus amount. The composition has excellent storage stability appearance, taste and physical properties even if it contains diglycerides in a high concentration without decreasing the amount of the yolk.

    摘要翻译： 描述了酸性水包油乳化组合物，其包含具有30重量％甘油二酯含量的油相。 ％以上的蛋黄质，其中溶血磷脂与全磷脂的比例以磷量计至少为15％。 该组合物即使在不降低蛋黄量的情况下高浓度地含有甘油二酯，也具有优异的保存稳定性外观，味道和物理性质。

    Utilization of ethoxylated fatty acid esters as self-emulsifiable compounds
    5.
    发明授权
    Utilization of ethoxylated fatty acid esters as self-emulsifiable compounds 失效
    乙氧基化脂肪酸酯作为自乳化的化合物的利用

    公开(公告)号：US06221919B1

    公开(公告)日：2001-04-24

    申请号：US09361225

    申请日：1999-07-27

    申请人： Gërard Trouve

    发明人： Gërard Trouve

    IPC分类号： C07C5300

    CPC分类号： C07C69/52 ,  A01N25/02 ,  A01N25/30 ,  A61K9/0019 ,  A61K9/1075 ,  A61K47/14 ,  A61K47/44 ,  Y10S514/937

    摘要： The present invention relates to the use of ethoxylated fatty acid esters as self-emulsifiable compounds particularly useful for the preparation of phytosanitary treatment products or as drugs for veterinary or human use. According to the invention, said fatty acid esters comprise a total number of ethylene oxide molecules such that the HLB value (hydrophilic-lipophilic balance) of said compounds is comprised between about 4 and about 10, preferably between about 5 and about 9. Said ethoxylated fatty acid esters form in an original way self-emulsifiable components without requiring any other surfactant, and they are biodegradable and capable of dissolving active principles which are little or non water-soluble.

    摘要翻译： 本发明涉及乙氧基化脂肪酸酯作为特别可用于制备植物检疫处理产品或作为兽医或人类使用的药物的自乳化化合物的用途。 根据本发明，所述脂肪酸酯包括总数的环氧乙烷分子，使得所述化合物的HLB值（亲水 - 亲油平衡）为约4至约10，优选约5至约9.所述乙氧基化 脂肪酸酯以原始方式形成自乳化成分，而不需要任何其它表面活性剂，并且它们是可生物降解的并且能够溶解少量或非水溶性的活性成分。

    Sunflower seeds and oil having a high stearic acid content
    6.
    发明授权
    Sunflower seeds and oil having a high stearic acid content 有权
    向日葵种子和具有高硬脂酸含量的油

    公开(公告)号：US06486336B1

    公开(公告)日：2002-11-26

    申请号：US09649288

    申请日：2000-08-26

    申请人： Jorge Osorio ,  Jose Maria Fernandez ,  Manuel Mancha ,  Rafael Garcés

    发明人： Jorge Osorio ,  Jose Maria Fernandez ,  Manuel Mancha ,  Rafael Garcés

    IPC分类号： C07C5300

    CPC分类号： A23D9/00 ,  A01H1/06 ,  A01H5/10

    摘要： The invention relates to a sunflower seed, comprising a sunflower oil having an increased stearic acid content as compared to wild type seeds, obtainable by treating parent seeds with a mutagenic agent during a period of time and in a conceatration sufficient to induce one or more mutations in the genetic trait involved in stearic acid biosynthesis resulting in an incresed production of stearic acid, germinating the treated seeds and culturing progeny plants therefrom, collecting and analyzing progeny seeds, selecting seeds that have acquired the desirable genetic trait and optionally repeating the cycle of germination, culturing and collection of seeds. Preferably the seeds comprise an oil having a stearic acid content of between 19.1 and 35% by weight related to the total amount of fatty acids in the oil, and are obtainable by treating the parent seeds with an alkylating agent, such as ethyl methane sulfonate in water, or with sodium azide in water. The invention further relates to sunflower oil obtainable by extracting the sunflower seeds, to a method for preparing sunflower seeds having an incresed stearic acid content as compared to wild type seeds, a method for preparing a sunflower oil having an increased stearic acid content sunflower plants produced from the seeds and the use of the sunflower oil in various products.

    摘要翻译： 本发明涉及向日葵种子，其包含与野生型种子相比具有增加的硬脂酸含量的向日葵油，其可通过在一段时间内用诱变剂处理亲本种子并且足以诱导一种或多种突变 在涉及硬脂酸生物合成的遗传性状中，导致硬脂酸的生产不足，发芽处理的种子并从中培养后代植物，收集和分析后代种子，选择获得所需遗传特征并任选重复发芽循环的种子 ，栽培和种子收集。 优选地，种子包含与油中脂肪酸总量相关的硬脂酸含量为19.1至35重量％的油，并且可通过用烷基化剂如甲磺酸乙酯处理母体种子获得 水或叠氮化钠在水中。 本发明还涉及通过提取向日葵种子获得的向日葵油，与野生型种子相比，制备具有增加的硬脂酸含量的向日葵种子的方法，制备具有增加的硬脂酸含量向日葵植物产生的向日葵油的方法 从种子和使用向日葵油的各种产品。

    Oil from seeds with a modified fatty acid composition
    7.
    发明授权
    Oil from seeds with a modified fatty acid composition 有权
    来自具有改性脂肪酸组成的种子的油

    公开(公告)号：US06348610B1

    公开(公告)日：2002-02-19

    申请号：US09326500

    申请日：1999-06-04

    申请人： Enrique Martinez Force ,  Begona Perez Vich ,  Jose Fernandez Martinez ,  Rafael Garces

    发明人： Enrique Martinez Force ,  Begona Perez Vich ,  Jose Fernandez Martinez ,  Rafael Garces

    IPC分类号： C07C5300

    CPC分类号： A01H5/10 ,  A23D9/00

    摘要： The invention relates to plant seeds that contain an oil having an oleic acid content of more than 5% and less than 65% by weight based upon the total fatty acid content, a linoleic acid content of more than 1% and less than 65% by weight based upon the total fatty acid content, a palmitic acid content of more than 20% and less than 40% by weight based upon the total fatty acid content, a stearic acid content of more than 3% and less than 15% based upon the total fatty acid content, and wherein the palmitoleic acid content is less than 4% based upon the total fatty acid content, and the asclepic acid content is less than 4% based upon the total fatty acid content. The invention further relates to the oil that can be obtained from the seeds, the use of that oil and to plants grown from the seeds or producing the seeds.

    摘要翻译： 本发明涉及植物种子，其含有基于总脂肪酸含量，油酸含量大于5％且小于65％（重量）的油，亚油酸含量大于1％且小于65％ 基于总脂肪酸含量的重量，基于总脂肪酸含量，棕榈酸含量大于20重量％且小于40重量％，硬脂酸含量大于3重量％且小于15重量％，基于 总脂肪酸含量，并且其中所述棕榈油酸含量基于总脂肪酸含量小于4％，并且所述百里香酸含量基于总脂肪酸含量小于4％。本发明还涉及所述油， 可以从种子获得，使用该油和从种子生长的植物或产生种子。

    Process for the preparation of alkanoyloxy-benzenesulfonic acids and salts thereof
    8.
    发明授权
    Process for the preparation of alkanoyloxy-benzenesulfonic acids and salts thereof 有权
    烷酰氧基 - 苯磺酸及其盐的制备方法

    公开(公告)号：US06218555B1

    公开(公告)日：2001-04-17

    申请号：US09543950

    申请日：2000-04-06

    申请人： Robert Thomas Hembre ,  Edwin Franklin Holcombe, III ,  Robert Lin ,  Mark Robert Shelton

    发明人： Robert Thomas Hembre ,  Edwin Franklin Holcombe, III ,  Robert Lin ,  Mark Robert Shelton

    IPC分类号： C07C5300

    CPC分类号： C07C303/06 ,  C07C67/08 ,  C07C69/017 ,  C07C309/42 ,  C07C69/24

    摘要： Disclosed is a process for the preparation of alkanoate esters of hydroxybenzenesulfonic acids and salts thereof by the steps of (1) contacting or reacting phenol with an alkanoic acid in the presence of trifluoroacetic acid (TFA) and trifluoroacetic anhydride (TFAA) to produce a aryl alkanoate ester and (2) contacting the reaction mixture of step (1) with a sulfonating agent to convert the aryl alkanoate ester to an alkanoate ester of hydroxybenzenesulfonic acid. The process provides the economic advantage inherent in using the product of esterification of step (1) without Disolation in the sulfonation of step (2).

    摘要翻译： 公开了通过以下步骤制备羟基苯磺酸的链烷酸酯及其盐的方法：（1）在三氟乙酸（TFA）和三氟乙酸酐（TFAA）存在下使苯酚与烷酸接触或反应，生成芳基 链烷酸酯和（2）使步骤（1）的反应混合物与磺化剂接触以将芳基链烷酸酯转化为羟基苯磺酸的链烷酸酯。 该方法提供了在步骤（2）的磺化中使用步骤（1）的酯化产物而没有分离的固有的经济优点。