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    Combined supported liquid membrane/strip dispersion process for the removal and recovery of radionuclides
    3.
    发明授权
    Combined supported liquid membrane/strip dispersion process for the removal and recovery of radionuclides 失效
    用于去除和回收放射性核素的组合支撑液膜/带分散方法

    公开(公告)号：US06696589B2

    公开(公告)日：2004-02-24

    申请号：US09789787

    申请日：2001-02-20

    申请人： W. S. Winston Ho

    发明人： W. S. Winston Ho

    IPC分类号： C07F940

    CPC分类号： B01D61/246 ,  B01D61/38 ,  C02F1/20 ,  C02F1/26 ,  C02F1/44 ,  C02F2101/006 ,  C07F9/4006 ,  C22B3/0067 ,  G21F9/12 ,  G21F9/125 ,  Y02P10/234

    摘要： The present invention provides a novel process for the removal and recovery of radionuclides from waste waters and process streams. The process of the present invention utilizes a combination of a supported liquid membrane (SLM) and a strip dispersion to improve extraction of the target species while increasing membrane stability and reducing processing costs. Additionally, the invention provides a family of new extractants, alkyl phenylphosphonic acids, for the removal and recovery of radionuclides and/or metals, including the use of the new extractants in the process. The new extractant selectively removes radionuclides and metals from the feed stream to provide a concentrated strip solution of the target species.

    摘要翻译： 本发明提供了从废水和工艺流中去除和回收放射性核素的新方法。 本发明的方法利用支撑液膜（SLM）和带状分散体的组合来改善目标物质的提取，同时提高膜稳定性并降低加工成本。 另外，本发明提供了用于去除和回收放射性核素和/或金属的一系列新的萃取剂，烷基苯基膦酸，包括在该方法中使用新的萃取剂。 新的萃取剂从进料流中选择性地除去放射性核素和金属，以提供目标物质的浓缩条带溶液。

    Optical material
    4.
    发明授权
    Optical material 失效
    光学材料

    公开(公告)号：US06562992B2

    公开(公告)日：2003-05-13

    申请号：US09939123

    申请日：2001-08-24

    申请人： Naoki Hayashi ,  Shigeru Mizusawa ,  Tomoyoshi Koizumi ,  Katsuichi Machida

    发明人： Naoki Hayashi ,  Shigeru Mizusawa ,  Tomoyoshi Koizumi ,  Katsuichi Machida

    IPC分类号： C07F940

    CPC分类号： G02B1/04 ,  C07F9/4006 ,  C08K5/5317 ,  C08L33/06

    摘要： The optical material in accordance with the present invention contains a specific phosphonate monoester compound such as monoethyl 3-methoxy butyl phosphonate, and a metal ion such as a copper ion or rare-earth metal ion. They may be contained in a solvent or resin. The use of such a specific phosphonate monoester compound improves the compatibility with a resin, whereby the metal ion can favorably be dispersed into the resin. Consequently, spectral characteristics can be improved when the optical member is formed into a resin-made optical member.

    摘要翻译： 根据本发明的光学材料含有特定的膦酸酯单酯化合物，例如3-甲氧基丁基膦酸单乙酯和金属离子如铜离子或稀土金属离子。 它们可以包含在溶剂或树脂中。 使用这种特定的膦酸酯单酯化合物改善了与树脂的相容性，由此金属离子可以有利地分散在树脂中。 因此，当光学构件形成为树脂制的光学构件时，可以提高光谱特性。

    Preparation of fluorinated compounds
    5.
    发明授权
    Preparation of fluorinated compounds 失效
    氟化合物的制备

    公开(公告)号：US06255518B1

    公开(公告)日：2001-07-03

    申请号：US09463268

    申请日：2000-03-20

    申请人： Richard Dickinson Chambers ,  John Hutchinson

    发明人： Richard Dickinson Chambers ,  John Hutchinson

    IPC分类号： C07F940

    CPC分类号： C07F9/4037 ,  C07F9/4006

    摘要： A method for the preparation of a fluorinated Phosphonate having the formula (RO)2PO CFR′R″ comprises treating a phosphonate of the formula (RO)2PO CHR′R″, or a metal salt thereof, with fluorine. R is an alkyl group R′ is hydrogen or alkyl and R″ is hydrogen, alkyl or another group.

    摘要翻译： 制备具有式（RO）2 PO CFR'R“的氟化膦酸酯的方法包括用氟处理式（RO）2 POCHR'R”的膦酸酯或其金属盐。 R是烷基，R'是氢或烷基，R“是氢，烷基或另一个基团。

    Method for manufacturing phosphonate esters
    6.
    发明授权
    Method for manufacturing phosphonate esters 失效
    膦酸酯的制备方法

    公开(公告)号：US06765107B2

    公开(公告)日：2004-07-20

    申请号：US09979077

    申请日：2002-07-30

    申请人： Li-Biao Han ,  Farzad Mirzaei ,  Masato Tanaka

    发明人： Li-Biao Han ,  Farzad Mirzaei ,  Masato Tanaka

    IPC分类号： C07F940

    CPC分类号： C07F9/657181 ,  C07F9/4015

    摘要： The present invention relates to a new manufacturing method for phosphonate esters, which have utility as a carbon-carbon binding formation agent, as well as a synthesis intermediate for biologically active substances such as medical drugs and agri-chemicals. Specifically the present invention relates to a new industrially advantageous manufacturing method for phosphonate esters in which the phosphonate esters of the subject can be efficiently obtained with a high yield rate through a simple operation while having barely any side reaction or sub-product. More specifically, the present invention pertains to a manufacturing method for phosphonate esters in which secondary phosphonate esters and alkene compounds are reacted in a transition metal catalyst. In addition the present invention relates to a new manufacturing method for allylphosphonate esters in which secondary cyclic phosphonate esters and 1,3-diene compounds are reacted in a palladium catalyst.

    摘要翻译： 本发明涉及一种可用作碳 - 碳结合形成剂的膦酸酯的新制备方法，以及用于生物活性物质如医药和农药的合成中间体。 具体而言，本发明涉及一种新的工业上有利的膦酸酯的制造方法，其中通过简单的操作，几乎没有任何副反应或副产物，可以以高产率有效地获得受试者的膦酸酯。 更具体地说，本发明涉及膦酸酯的制备方法，其中次膦酸酯和烯烃化合物在过渡金属催化剂中反应。 此外，本发明涉及烯丙基膦酸酯的新制备方法，其中二次环状膦酸酯和1,3-二烯化合物在钯催化剂中反应。

    Production process of diphosphine oxide and diphosphonate
    8.
    发明授权
    Production process of diphosphine oxide and diphosphonate 有权
    二氧化膦和二膦酸盐的生产工艺

    公开(公告)号：US06472539B1

    公开(公告)日：2002-10-29

    申请号：US09899207

    申请日：2001-07-06

    申请人： Tohru Yokozawa ,  Takao Saito ,  Noboru Sayo ,  Takero Ishizaki

    发明人： Tohru Yokozawa ,  Takao Saito ,  Noboru Sayo ,  Takero Ishizaki

    IPC分类号： C07F940

    CPC分类号： C07F9/65517

    摘要： A process for producing a diphosphine oxide or diphosphonate represented by formula (1) as defined, which comprises treating, with a base, a phosphine compound represented by formula (2) as defined and adding the thus-treated phosphine compound to a nonpolar solvent having an oxidative metal compound suspended therein so as to effect dimerization. The present invention makes it possible to produce, conveniently, in a high yield and safely, a diphosphine oxide or diphosphonate which is an intermediate for producing a diphosphine compound useful as a ligand of a metal complex serving as a catalyst for asymmetric synthesis reaction.

    摘要翻译： 一种制备由式（1）表示的二膦氧化物或二膦酸盐的方法，该方法包括用碱处理如上定义的式（2）表示的膦化合物，并将如此处理的膦化合物加入到具有 悬浮在其中以实现二聚化的氧化金属化合物。 本发明使得可以以高产率和安全地生产作为用作不对称合成反应催化剂的金属络合物的配位体的二膦化合物的中间体的二氧化膦或二膦酸盐的方法。

    Phosphonic acid diester derivatives
    9.
    发明授权
    Phosphonic acid diester derivatives 失效
    膦酸二酯衍生物

    公开(公告)号：US06468992B1

    公开(公告)日：2002-10-22

    申请号：US09674145

    申请日：2000-12-13

    申请人： Yasuhiro Sakai ,  Kazuyoshi Miyata ,  Kenichi Kawamura ,  Yoshihiko Tsuda ,  Yasuhide Inoue

    发明人： Yasuhiro Sakai ,  Kazuyoshi Miyata ,  Kenichi Kawamura ,  Yoshihiko Tsuda ,  Yasuhide Inoue

    IPC分类号： C07F940

    CPC分类号： C07F9/4065 ,  C07F9/4006 ,  C07F9/58 ,  C07F9/650952

    摘要： The present invention provides novel phosphonic acid diester derivatives useful as medicines. The phosphonic acid diester derivatives are represented by the general formula: wherein R1 represents amino group, N-lower alkylamino group, N-lower alkenylamino group, or the like; R2 and R3 represent hydrogen atom, lower alkyl group, halogen atom, lower alkoxy group, or the like; R4 represents hydrogen atom, lower alkyl group or phenyl(lower)alkyl group; R5 and R6 represent lower alkyl group; X, Y and Z represent that all of them are carbon atoms or one of them is nitrogen atom and the other two are carbon atoms; Q represents a single bond or alkylene group; or the pharmacologically acceptable salts thereof.

    摘要翻译： 本发明提供了可用作药物的新型膦酸二酯衍生物。 膦酸二酯衍生物由以下通式表示：其中R1表示氨基，N-低级烷基氨基，N-低级链烯基氨基等; R2和R3表示氢原子，低级烷基，卤素原子，低级烷氧基 等; R4表示氢原子，低级烷基或苯基（低级）烷基; R5和R6表示低级烷基; X，Y和Z表示全部为碳原子或其中一个为氮原子， 另外两个是碳原子; Q表示单键或亚烷基;或其药理学上可接受的盐。

    Thioalkenylphosphonic acid ester and process for the preparation thereof
    10.
    发明授权
    Thioalkenylphosphonic acid ester and process for the preparation thereof 失效
    硫代烯基膦酸酯及其制备方法

    公开(公告)号：US06191298B1

    公开(公告)日：2001-02-20

    申请号：US09521844

    申请日：2000-03-09

    申请人： Li-Biao Han ,  Masato Tanaka

    发明人： Li-Biao Han ,  Masato Tanaka

    IPC分类号： C07F940

    CPC分类号： C07F9/4018 ,  C07F9/4015

    摘要： A phosphonic acid ester compound of the formula: R1C(SR3)═CHP(═O)(OR2)2 or [P(═O)(OR2)2]CH═C(SR3)—R4—C(SR3)═CH[P(═O)(OR2)2] wherein R1 represents a monovalent group selected from hydrogen, alkyl, cycloalkyl, cycloalkenyl, aryl, aralkyl, alkenyl and silyl, R2 and R3 each represent aryl and R4 represents alkylene or cycloalkylene. The ester compound is produced by reaction of an acetylene compound, R1C≡CH or HC≡C—R4—C≡CH, with with a phosphorothioate, (R2O)2P(═O)SR3, in the presence of a palladium complex catalyst.

    摘要翻译： 下式的膦酸酯化合物：其中R 1表示选自氢，烷基，环烷基，环烯基，芳基，芳烷基，烯基和甲硅烷基的一价基团，R 2和R 3各自表示芳基，R 4表示亚烷基或亚环烷基。 通过乙炔化合物R1C = CH或HC = C-R4-C = CH与硫代磷酸酯（R2O）2P（= O）SR3在钯络合物催化剂存在下反应制备酯化合物。