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    Organic dye compound having both pyridiniotriazinyl and vinylsulfone type fiber-reactive groups
    1.
    发明授权
    Organic dye compound having both pyridiniotriazinyl and vinylsulfone type fiber-reactive groups 失效
    具有吡啶并三嗪基和乙烯基砜型纤维反应性基团的有机染料化合物

    公开(公告)号：US4626589A

    公开(公告)日：1986-12-02

    申请号：US699182

    申请日：1985-02-07

    申请人： Takashi Omura ,  Yutaka Kayane ,  Mikoto Takahashi ,  Tetsuya Miyamoto ,  Akira Takeshita ,  Naoki Harada ,  Katsumasa Otake

    发明人： Takashi Omura ,  Yutaka Kayane ,  Mikoto Takahashi ,  Tetsuya Miyamoto ,  Akira Takeshita ,  Naoki Harada ,  Katsumasa Otake

    IPC分类号： C09B62/002 ,  C09B62/04 ,  C09B62/44 ,  C09B62/503 ,  D06P1/38 ,  C09B44/02 ,  C09B44/08 ,  C09B62/523 ,  C09B62/527

    CPC分类号： C09B62/4403 ,  D06P1/38

    摘要： A compound of the formula, ##STR1## wherein D is an organic dye moiety, R.sub.1 and R.sub.2 are independently hydrogen or a substituted or unsubstituted lower alkyl group, R.sub.3 is hydrogen or a substituted or unsubstituted lower alkyl, phenyl or naphthyl group, X.sub.1 and X.sub.2 are independently hydrogen, halogen or a lower alkyl, cyano, carbamoyl, vinyl, .beta.-hydroxyethyl, .beta.-sulfoethyl, .beta.-sulfatoethyl, carboxyl, carboxylic acid ester or sulfonic acid group, and Z is appended to the above-defined D or R.sub.3 and stands for --SO.sub.2 CH.dbd.CH.sub.2 or --SO.sub.2 CH.sub.2 CH.sub.2 Y, in which Y is a group capable of being split by the action of an alkali, which is useful for dyeing hydroxyl or amido group-containing fiber materials with excellent build-up properties, thereby giving dyed products having excellent various fastness properties.

    摘要翻译： 下式的化合物，其中D是有机染料部分，R1和R2独立地是氢或取代或未取代的低级烷基，R3是氢或取代或未取代的低级烷基，苯基或萘基，X1和 X 2独立地是氢，卤素或低级烷基，氰基，氨基甲酰基，乙烯基，β-羟基乙基，β-磺基乙基，β-磺基乙基，羧基，羧酸酯或磺酸基，并且Z附加到上述定义的D或 R3代表-SO2CH = CH2或-SO2CH2CH2Y，其中Y是能够通过碱的作用分裂的基团，其可用于染色具有优异累积性质的含羟基或含酰胺基的纤维材料，因此 给出具有优异的各种牢度特性的染色产品。

    Water-soluble pyridone monoazo compounds suitable as fiber reactive dyestuffs
    2.
    发明授权
    Water-soluble pyridone monoazo compounds suitable as fiber reactive dyestuffs 失效

    公开(公告)号：US4659807A

    公开(公告)日：1987-04-21

    申请号：US757687

    申请日：1985-07-22

    申请人： Marcos Segal

    发明人： Marcos Segal

    IPC分类号： C09B62/51 ,  D06P1/384 ,  D06P3/10 ,  D06P3/66 ,  C09B62/527 ,  C09B62/53

    CPC分类号： D06P1/384 ,  C09B62/51

    摘要： Monoazo compounds which are suitable as fiber-reactive dyestuffs have the general formula (1) ##STR1## in which: D is a benzene or naphthalene ring or a radical of the formula (2) or (3) ##STR2## R.sup.1 is hydrogen, alkyl of 1 to 4 carbon atoms, alkoxy of 1 to 4 carbon atoms, hydroxy, nitro or halogen, if D stands for a benzene ring, andR.sup.2 is hydrogen, alkyl of 1 to 4 carbon atoms, alkoxy of 1 to 4 carbon atoms, halogen, carboxy or sulfo, if D stands for a benzene ring, orR.sup.1 is hydrogen, alkyl of 1 to 4 carbon atoms, alkoxy of 1 to 4 carbon atoms, carboxy, halogen, sulfo or a group of the formula --SO.sub.2 --Y (where Y has the meaning mentioned hereinafter), if D stands for a naphthalene ring, andR.sup.2 is hydrogen or sulfo, if D is a naphthalene ring, orR.sup.1 is, if D is a radical of the formula (2), hydrogen, nitro, chlorine or alkoxy of 1 to 4 carbon atoms, R.sup.1 being bonded to the benzene nucleus V, andR.sup.2 is, if D is a radical of the formula (2), chlorine, sulfo, nitro or hydrogen, R.sup.2 being bonded to the benzene nucleus W, orR.sup.1 is, if D is a radical of the formula (3), hydrogen, nitro or sulfo, R.sup.1 being bonded to the benzene nucleus V, andR.sup.2 is, if D is a radical of the formula (3), chlorine, sulfo or hydrogen, R.sup.2 being bonded to the benzene nucleus W;the group --SO.sub.2 --Y in the formulae (2) and (3) is bonded to V or W, preferably to V;Y is vinyl or ethyl which contains bonded in the .beta.-position a substituent which is eliminatable as an anion under alkaline conditions;R is hydrogen or carbamoyl,B is alkyl of 1 to 4 carbon atoms which is substituted by sulfato, phosphato, carboxy or sulfo;M is hydrogen or one equivalent of a monovalent, divalent or trivalent metal;the moieties B, R.sup.1, R.sup.2 and R can have meanings which are identical to or different from one another.The new monoazo compounds produce on hydroxy- and/or carboxamido-containing materials, in particular fiber materials, such as cellulose fibers and wool, useful dyeings and prints having good end-use and manufacturing fastness properties.

    Reactive monazo-dyestuffs
    3.
    发明授权
    Reactive monazo-dyestuffs 失效
    反应性MONAZO-DYESTUFFS

    公开(公告)号：US3637648A

    公开(公告)日：1972-01-25

    申请号：US3637648D

    申请日：1968-07-09

    申请人： HOECHST AG

    发明人： KUHNE RUDOLF ,  MEININGER FRITZ ,  FROLICH HEINRICH

    IPC分类号： C09B62/527 ,  C09B62/53

    CPC分类号： C09B62/527 ,  C09B62/53 ,  Y10S8/918

    摘要： REACTIVE MONOAZO DYESTUFFS CONTAINING AS REACTIVE GROUPINGS ONE OR TWO GROUPS OF THE FORMULA

    -N(-R'')-SO2-Y

    WHEREIN Y REPRESENTS ONE OF THE MOIETIES

    PHENYL-O-CH2-CH2-CH2-COO-CH2-CH2-

    PHENYL-N(+)-CH2-CH2- CL(-),

    -CH2-CH2-N(+)(-LOWER ALKYL)3 CL(-)

    AND -CH=CH2, AND R'' IS LOWER ALKYL OR BENZYL, WHICH ARE SUITABLE FOR THE DYEING OR PRINTING OF LEATHER, WOOL, SILK, TEXTILE MATERIALS OF POLYAMIDES, POLYACTYLONITRILE, POLYURETHANES OR CELLULOSE.

    Water-soluble, fiber-reactive organic dyestuffs containing a .beta.-chloro-ethylsulfonyl-methyl-benzoic acid amide group
    5.
    发明授权
    Water-soluble, fiber-reactive organic dyestuffs containing a .beta.-chloro-ethylsulfonyl-methyl-benzoic acid amide group 失效
    含有β-氯乙基磺酰基 - 甲基 - 苯甲酸酰胺基团的水溶性纤维反应性有机染料

    公开(公告)号：US4473498A

    公开(公告)日：1984-09-25

    申请号：US288386

    申请日：1981-07-30

    申请人： Ludwig Schlafer ,  Reinhard Hahnle

    发明人： Ludwig Schlafer ,  Reinhard Hahnle

    IPC分类号： C07C67/00 ,  C07C313/00 ,  C07C317/44 ,  C09B62/503 ,  C09B62/505 ,  C09B62/51 ,  C09B62/513 ,  C09B62/515 ,  C09B62/517 ,  D06M13/02 ,  D06M13/244 ,  D06M13/248 ,  D06M13/268 ,  D06M13/278 ,  D06M13/322 ,  D06M13/402 ,  D06M13/415 ,  D06M13/438 ,  D06M101/00 ,  D06M101/02 ,  D06M101/06 ,  D06M101/08 ,  D06M101/10 ,  D06M101/16 ,  D06M101/18 ,  D06M101/30 ,  D06M101/34 ,  D06P5/00 ,  C09B62/523 ,  C09B62/525 ,  C09B62/527 ,  C09B62/53 ,  C09B62/535 ,  C09B62/537

    CPC分类号： D06M13/278 ,  C09B62/503

    摘要： Novel organic, water-soluble compounds having fiber-reactive and fiber-finishing properties and containing, as a fiber-reactive group, one or two .beta.-chloroethylsulfonylmethyl-benzoic acid amide groups. These compounds can be prepared (1) by reacting novel .beta.-chloroethylsulfonylmethyl-benzoic acid halide compounds with an organic, water-soluble compound having fiber-finishing properties and containing one or two amino groups, or (2) analogously to known and usual procedures, from precursors containing the .beta.-chloroethylsulfonylmethyl-benzoic acid amide grouping. The novel fiber-finishing compounds are applied to and fixed on suitable fiber materials, especially cellulose fiber material and natural or synthetic polyamide fiber materials, by methods corresponding to those which are conventional for application and fixation of fiber-reactive compounds. The above-mentioned .beta.-chloroethylsulfonylmethyl-benzoic acid halides are synthesized by monochlorinating the methyl grouping of a toluenecarboxylic acid or an alkyl ester thereof or an acid halide thereof, converting this monochlorinated compound by reaction with 2-mercaptoethanol in aqueous solution, optionally with simultaneous hydrolysis of the carboxylic acid chloride group, to form the thioether compound, hydrolyzing the carbalkoxy grouping optionally present in this thioether compound, and then oxidizing said thioether compound by means of an oxidizing agent to form the corresponding sulfonyl compound; the .beta.-hydroxyethylsulfonylmethyl grouping is subsequently reacted with a chlorinating agent.

    摘要翻译： 具有纤维反应性和纤维整理性能的新型有机水溶性化合物，作为纤维反应性基团含有一个或两个β-氯乙基磺酰基甲基 - 苯甲酸酰胺基团。 这些化合物可以通过使新的β-氯乙基磺酰基甲基 - 苯甲酸卤化物与具有纤维整理性质并含有一个或两个氨基的有机水溶性化合物反应来制备（1），或（2）类似于已知和常规方法 ，来自含有β-氯乙基磺酰基甲基 - 苯甲酸酰胺基团的前体。 通过与常规用于纤维反应性化合物的施用和固定的方法相对应的方法，将新型纤维整理剂施用并固定在合适的纤维材料，特别是纤维素纤维材料和天然或合成聚酰胺纤维材料上。 上述β-氯乙基磺酰基甲基 - 苯甲酸卤化物是通过一甲基甲苯甲酸或其烷基酯或其酰卤单氯化合成的，通过与2-巯基乙醇在水溶液中的反应转化该一氯化合物，任选地同时 水解羰基氯化物基团，形成硫醚化合物，水解任选存在于该硫醚化合物中的烷氧基，然后用氧化剂氧化所述硫醚化合物，形成相应的磺酰化合物; 然后将β-羟乙基磺酰基甲基与氯化剂反应。

    s-Triazines
    6.
    发明授权
    s-Triazines 失效

    公开(公告)号：US4467088A

    公开(公告)日：1984-08-21

    申请号：US425592

    申请日：1982-09-28

    申请人： Hansrudolf Schwander

    发明人： Hansrudolf Schwander

    IPC分类号： C09B29/08 ,  C09B62/085 ,  C09B62/44 ,  C09B62/527 ,  C07D251/46 ,  C07D251/52 ,  C07D251/70

    CPC分类号： C09B62/085 ,  C09B29/0803 ,  C09B62/4413 ,  C09B62/527

    摘要： s-Triazine compounds of the formula: ##STR1## in which R.sub.1 and R.sub.2 independently of one another are C.sub.1-4 alkyl, R.sub.3 and R.sub.4 independently of one another are one of the following radicals; C.sub.1-10 alkoxy which is unsubstituted or substituted by alkoxy; N-C.sub.1-10 alkylamino which is unsubstituted or substituted by phenyl; phenylamino which is unsubstituted or substituted by halogen, C.sub.1-4 alkyl or C.sub.1-4 alkoxy; naphthylamino which is unsubstituted or substituted by halogen, C.sub.1-4 alkyl or C.sub.1-4 alkoxy; halogen; N-phenyl-N-alkylamino; dialkylamino; alkylmercapto; cyclohexyloxy; N-alkyl-N-cyclohexylamino and cyclohexylamino; M is hydrogen or one equivalent of a cation and n is 1 or 2. These compounds may be used in the preparation of dyes.

    摘要翻译： 其中R 1和R 2彼此独立地是C 1-4烷基，R 3和R 4彼此独立地是下式的其中之一： 未取代或被烷氧基取代的C 1-10烷氧基; 未取代或被苯基取代的N-C 1-10烷基氨基; 苯基氨基，其未被取代或被卤素，C 1-4烷基或C 1-4烷氧基取代; 未被取代或被卤素，C 1-4烷基或C 1-4烷氧基取代的萘基氨基; 卤素; N-苯基-N-烷基氨基; 二烷基氨基; 烷基巯基 环己氧基; N-烷基-N-环己基氨基和环己基氨基; M为氢或1当量阳离子，n为1或2.这些化合物可用于制备染料。

    Reactive dyestuff composition and their use
    9.
    发明授权
    Reactive dyestuff composition and their use 失效
    活性染料组合物及其用途

    公开(公告)号：US07704286B2

    公开(公告)日：2010-04-27

    申请号：US11300461

    申请日：2005-12-15

    申请人： Huei-Chin Huang ,  Ya-Chi Tseng

    发明人： Huei-Chin Huang ,  Ya-Chi Tseng

    IPC分类号： C09B29/036 ,  C09B62/527

    CPC分类号： C09B67/0047 ,  C09B67/0052

    摘要： A dye composition, which comprising: (a) a mono azo dye of the formula (I) wherein R, R1, K, Y and m are defined the same as the specification; and (b)at least one azo dye selected from the group consisting of the following formula (II), (III) and (IV), wherein R, R2, R3, Y, (W)0˜3, (W′)0˜3, D, D1 and D2 are defined the same as the specification. These kinds of dye composition with good stability and build-up. The dye composition are suitable for dyeing and printing of materials containing either cellulose fibers, such as cotton, artificial cotton, linen, and artificial linen, or synthetic polyamide, such as wool, silk, and nylon etc. Dyed materials with excellent properties can be obtained, showing especially outstanding performance in of wash-off, built-up, level-dyeing, photochromism, wet-fastnes, ghosting fastness and light fastness.

    摘要翻译： 一种染料组合物，其包含：（a）式（I）的单偶氮染料，其中R，R 1，K，Y和m定义与说明书相同; 和（b）至少一种选自下式（II），（III）和（IV）的偶氮染料，其中R，R2，R3，Y，（W）0-3，（W' 0〜3，D，D1，D2的定义与说明书相同。 这些染料组合物具有良好的稳定性和积聚性。 染料组合物适用于染色和印刷含有纤维素纤维如棉，人造棉，亚麻布和人造亚麻的材料，或合成聚酰胺如羊毛，丝绸和尼龙等。具有优异性能的染色材料可以是 获得，在洗涤，建成，水平染色，光致变色，湿牢牢，重影牢度和耐光性方面表现出特别出色的表现。

    Process for the dyeing of synthetic polyamide fibre materials
    10.
    发明授权
    Process for the dyeing of synthetic polyamide fibre materials 失效
    合成聚酰胺纤维材料染色工艺

    公开(公告)号：US5356440A

    公开(公告)日：1994-10-18

    申请号：US96143

    申请日：1993-07-22

    申请人： Pierre Galafassi ,  Jean-Marie Adam

    发明人： Pierre Galafassi ,  Jean-Marie Adam

    IPC分类号： C09B62/503 ,  D06P3/24 ,  D06P1/384 ,  C09B62/527 ,  C09B62/53

    CPC分类号： C09B62/503 ,  D06P3/248

    摘要： The invention relates to a process for the dyeing of synthetic polyamide fibre materials, which comprises dyeing these fibre materials with a reactive dye of the formulaHO.sub.3 S--Fa--X--SO.sub.2 CH.sub.2 CH.sub.2 OSO.sub.3 H).sub.m(1),in which Fa is a dye radical, X is a direct bond or a radical of the formula --CONHCH.sub.2 CH.sub.2 -- and m is the number 1 or 2, the dye of the formula (1) containing only one sulfo group, from an aqueous liquor at a pH of 5 to 9 and, to set the dyeing temperature, raising the temperature from 80.degree. C. to at least 95.degree. C. over a period of at least 20 minutes. The process according to the invention produces level dyeings on synthetic polyamide fibre materials.

    摘要翻译： 本发明涉及一种染色合成聚酰胺纤维材料的方法，其中包括使用式HO3S-Fa-X-SO2CH2CH2OSO3H）m（1）的活性染料染色这些纤维材料，其中Fa是染料基团，X 是式-CONHCH 2 CH 2 - 的直接键或基团，m为1或2，式（1）的染料仅含有一个磺基，pH为5至9的含水液体，以及 设定染色温度，在至少20分钟的时间内将温度从80℃提高至至少95℃。 根据本发明的方法在合成聚酰胺纤维材料上产生高级染色。