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公开(公告)号：US20240279821A1
公开(公告)日：2024-08-22
申请号：US18563570
申请日：2022-03-16
申请人： DE NORA PERMELEC LTD
发明人： Hiroki DOMON , Shigeki SUDO , Hideo OTSU
CPC分类号： C25B1/26 , C01B11/062 , C25B9/19 , C25B9/70 , C25B13/08 , C25B15/02 , C25B15/087
摘要： To provide a production method and a production apparatus of a sodium hypochlorite solution that can produce a sodium hypochlorite solution with a high available chlorine concentration at a low cost using an on-site facility. In production of a sodium hypochlorite solution by feeding secondary salt water as an aqueous sodium chloride solution, in an electrolyzer 10 comparted into an anode chamber 2 and a cathode chamber 3 by an ion-exchange membrane 1, to the anode chamber and, after electrolysis, introducing an anolyte and a generated chlorine gas in the anode chamber and an aqueous sodium hydroxide solution generated in the cathode chamber into a reaction tank 20 to allow the anolyte, the chlorine gas, and the generated aqueous sodium hydroxide solution as a catholyte to react in the reaction tank, a primary salt water generation step of dissolving raw salt G containing sodium chloride as a main component in purified water B to generate primary salt water, and a chelating step of chelating the primary salt water to generate secondary salt water A are included, in which a decomposition rate of salt ranges from 80 to 95%.
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公开(公告)号：US20240218542A1
公开(公告)日：2024-07-04
申请号：US18288757
申请日：2022-03-16
申请人： DE NORA PERMELEC LTD
发明人： Hiroki DOMON , Masahiro OHARA , Masaaki KATO
CPC分类号： C25B15/081 , C01B11/062 , C02F1/42 , C02F1/683 , C25B1/46 , C25B9/19 , C25B15/085 , C02F2001/425
摘要： To provide a method and an apparatus for producing a sodium hypochlorite solution on-site at a high efficiency and at the initial cost and suppressing operating cost without any problems about impurities derived from raw material water and raw salt. A method of producing a sodium hypochlorite solution on-site in the vicinity of a physical plant where a sodium hypochlorite solution is used. In production of a sodium hypochlorite solution by feeding secondary salt water, in an electrolyzer comparted into an anode chamber and a cathode chamber with an ion-exchange membrane, to the anode chamber and allowing components in the anode chamber and the cathode chamber after electrolysis to react in a reaction tank, there are included respective steps of treating raw material water A with a cation-exchange resin B to generate purified water 5, dissolving raw salt D in the purified water to generate primary salt water E, performing an examination for confirming the presence or absence of a precipitate or suspended solid in the primary salt water, and directly performing chelating in the case of no precipitate or suspended solid contained in the primary salt water, or performing chelating after addition of an acid component for dissolution of the precipitate or suspended solid in the case of the precipitate or suspended solid contained therein, to generate secondary salt water 4.
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公开(公告)号：US20230354817A1
公开(公告)日：2023-11-09
申请号：US18223205
申请日：2023-07-18
申请人： Pur Products LLC
发明人： Harold D. Grant
摘要： An anti-microbial formulation for seed and crop application is a formulation including only between about 1 ppm and about 100 ppm hypochlorous acid; between about 1 ppm and about 300 ppm alkyl polyglycoside, wherein sufficient amount of alkyl polyglycoside is present such that the formulation has a pH between about 5.2 and about 7.8; and a remainder water. A method of manipulating the pH of the formulation and a method of treating seeds and crops with the formulation to restrict or eliminate microbial growth and proliferation is also described herein.
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公开(公告)号：US20220240515A1
公开(公告)日：2022-08-04
申请号：US17207812
申请日：2021-03-22
申请人： Pur Products LLC
发明人： Lance Shepherdson , Harold D. Grant
摘要： An anti-microbial formulation for seed and crop application includes about 170 ppm hypochlorous acid; about 25 ppm hypochlorite ion; about 2.5 ppm ozone; about 2.5 ppm chlorine dioxide; between about 10 ppm and about 100,000 ppm alkyl polyglycoside; and a remainder of water. A method of manipulating the pH of the formulation and a method of treating seeds and crops with the formulation to restrict or eliminate microbial growth and proliferation is also described herein.
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公开(公告)号：US11377349B2
公开(公告)日：2022-07-05
申请号：US16490315
申请日：2018-02-06
发明人： Tomohide Okada , Hideo Shimazu , Hiromichi Ito , Yukihiro Sugiyama , Takashi Toyama , Kaoru Shimada , Hiroshi Fujihisa , Satoshi Takeya , Takehiro Matsunaga , Yoshito Gotoh
IPC分类号： C01B11/06
摘要： Provided are sodium hypochlorite pentahydrate crystals capable of long-term storage that have improved stability of sodium hypochlorite pentahydrate, which is effective as an oxidizing 5 agent or bactericide, in the vicinity of normal temperatures, and a method for producing the same. The sodium hypochlorite pentahydrate crystals are such that peaks appear at the locations of the angles of diffraction described in Table 1 of claim 1 over a range of 10°≤2θ (angle of diffraction)≤65° as measured by powder X-ray diffraction using a Cukα radiation source.
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6.发明申请公开(公告)号：US20210206636A1
公开(公告)日：2021-07-08
申请号：US17044863
申请日：2019-04-02
发明人： Hisataka GODA
摘要： The purpose of the present invention is to provide a method for manufacturing a new disinfectant from sodium hypochlorite that has degraded in quality during storage. A method for manufacturing a novel disinfectant from a solution containing hypochlorite ions, chlorate ions, and chloride ions, wherein the method includes: a first reaction step for adding sulfuric acid to the solution and generating chlorine gas; a step in which, in a recovery liquid A, the generated chlorine gas is caused to react with sodium hydroxide or calcium hydroxide and recovered as hypochlorite ions; a second reaction step for adding, to a reaction mother liquid after the first reaction step, sulfuric acid having a higher concentration than that in the first reaction step, and generating chlorine dioxide gas; a step in which, in a recovery liquid B, the generated chlorine dioxide gas is caused to react with sodium hydroxide and hydrogen peroxide and recovered as chlorite ions; and a step for mixing the recovery liquid A and the recovery liquid B and obtaining a novel disinfectant.
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公开(公告)号：US20210024354A1
公开(公告)日：2021-01-28
申请号：US17043206
申请日：2019-03-19
申请人： OLIN CORPORATION
摘要： Disclosed herein are processes for producing highly concentrated bleach slurries containing a mixture of crystals of solid sodium hypochlorite pentahydrate in a liquid phase saturated in sodium hypochlorite and containing sodium hydroxide or other alkaline stabilizers. Bleach slurries and compositions exhibiting enhanced stability are also disclosed.
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公开(公告)号：US20200172398A1
公开(公告)日：2020-06-04
申请号：US16697054
申请日：2019-11-26
发明人： Bruno LAUNAY , Dimitri KUZNETSOV , Thomas MCNEEL
摘要： A method for producing a haloamine solution with reduced amounts of halogen oxyanions including (a) the on-site generation of a halogen-containing oxidant, such as a solution and (b) reacting on-site the halogen-containing oxidant with a nitrogen source, to thereby produce the haloamine solution.
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公开(公告)号：US20200017359A1
公开(公告)日：2020-01-16
申请号：US16282202
申请日：2019-02-21
发明人： TERRY GEIS , KEN KNIBBS
IPC分类号： C01B11/06
摘要： A process to generate sodium hypochlorite solution from recycled solid oxidizer materials. The process involves preferably two main units: the chlorine generation unit where a wet gaseous chlorine stream will be generated, and a bleach production unit where the chlorine gas will be combined with caustic soda to create a bleach solution.
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公开(公告)号：US20200010320A1
公开(公告)日：2020-01-09
申请号：US16490315
申请日：2018-02-06
发明人： Tomohide OKADA , Hideo SHIMAZU , Hiromichi ITO , Yukihiro SUGIYAMA , Takashi TOYAMA , Kaoru SHIMADA , Hiroshi FUJIHISA , Satoshi TAKEYA , Takehiro MATSUNAGA , Yoshito GOTOH
IPC分类号： C01B11/06
摘要： Provided are sodium hypochlorite pentahydrate crystals capable of long-term storage that have improved stability of sodium hypochlorite pentahydrate, which is effective as an oxidizing agent or bactericide, in the vicinity of normal temperatures, and a method for producing the same.The sodium hypochlorite pentahydrate crystals are such that peaks appear at the locations of the angles of diffraction described in Table 1 of claim 1 over a range of 10°≤2θ (angle of diffraction)≤65° as measured by powder X-ray diffraction using a CuKα radiation source.
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