METHOD AND APPARATUS FOR PRODUCING SODIUM HYPOCHLORITE SOLUTION

    公开(公告)号:US20240279821A1

    公开(公告)日:2024-08-22

    申请号:US18563570

    申请日:2022-03-16

    摘要: To provide a production method and a production apparatus of a sodium hypochlorite solution that can produce a sodium hypochlorite solution with a high available chlorine concentration at a low cost using an on-site facility. In production of a sodium hypochlorite solution by feeding secondary salt water as an aqueous sodium chloride solution, in an electrolyzer 10 comparted into an anode chamber 2 and a cathode chamber 3 by an ion-exchange membrane 1, to the anode chamber and, after electrolysis, introducing an anolyte and a generated chlorine gas in the anode chamber and an aqueous sodium hydroxide solution generated in the cathode chamber into a reaction tank 20 to allow the anolyte, the chlorine gas, and the generated aqueous sodium hydroxide solution as a catholyte to react in the reaction tank, a primary salt water generation step of dissolving raw salt G containing sodium chloride as a main component in purified water B to generate primary salt water, and a chelating step of chelating the primary salt water to generate secondary salt water A are included, in which a decomposition rate of salt ranges from 80 to 95%.

    METHOD AND DEVICE FOR MANUFACTURING SODIUM HYPOCHLORITE SOLUTION

    公开(公告)号:US20240218542A1

    公开(公告)日:2024-07-04

    申请号:US18288757

    申请日:2022-03-16

    摘要: To provide a method and an apparatus for producing a sodium hypochlorite solution on-site at a high efficiency and at the initial cost and suppressing operating cost without any problems about impurities derived from raw material water and raw salt. A method of producing a sodium hypochlorite solution on-site in the vicinity of a physical plant where a sodium hypochlorite solution is used. In production of a sodium hypochlorite solution by feeding secondary salt water, in an electrolyzer comparted into an anode chamber and a cathode chamber with an ion-exchange membrane, to the anode chamber and allowing components in the anode chamber and the cathode chamber after electrolysis to react in a reaction tank, there are included respective steps of treating raw material water A with a cation-exchange resin B to generate purified water 5, dissolving raw salt D in the purified water to generate primary salt water E, performing an examination for confirming the presence or absence of a precipitate or suspended solid in the primary salt water, and directly performing chelating in the case of no precipitate or suspended solid contained in the primary salt water, or performing chelating after addition of an acid component for dissolution of the precipitate or suspended solid in the case of the precipitate or suspended solid contained therein, to generate secondary salt water 4.

    Process for preparing concentrated alkali metal hypochlorite solutions
    3.
    发明授权
    Process for preparing concentrated alkali metal hypochlorite solutions 有权
    浓缩碱金属次氯酸盐溶液的制备方法

    公开(公告)号:US09023236B2

    公开(公告)日:2015-05-05

    申请号:US13299599

    申请日:2011-11-18

    IPC分类号: C11D3/395 C01B11/06

    CPC分类号: C01B11/062

    摘要: The present invention relates to a process for preparing concentrated alkali metal hypochlorite solutions. One subject of the invention is more particularly a process for preparing concentrated bleach which may have a chlorine content of greater than 100 chlorometric degrees, and that has a low content of chlorates.

    摘要翻译: 本发明涉及一种制备浓缩碱金属次氯酸盐溶液的方法。 本发明的一个主题更具体地是一种制备浓缩漂白剂的方法,该漂白剂可以具有大于100个氯度的氯含量,并且具有低含量的氯酸盐。

    OPEN-CELL TYPE APPARATUS FOR PREPARING SODIUM HYPOCHLORITE
    5.
    发明申请
    OPEN-CELL TYPE APPARATUS FOR PREPARING SODIUM HYPOCHLORITE 审中-公开
    用于制备SODIUM HYPOCHLORITE的开孔类型设备

    公开(公告)号:US20130313109A1

    公开(公告)日:2013-11-28

    申请号:US13985382

    申请日:2012-03-02

    IPC分类号: C25B15/02 C25B1/26

    摘要: Provided is an open cell-type apparatus for producing sodium hypochlorite based on electrolysis using soft water and salt. The apparatus includes: a sodium hypochlorite generator including a plurality of electrode plates supported by a support, a flow channel for air flow provided above the support and the electrode plates, and an air intake hole and an air exhaust hole which communicate with the flow channel; a cooling unit for lowering a temperature of the flow channel; and a controller for controlling operation of the cooling unit by detecting a temperature of the sodium hypochlorite generator. The apparatus constantly maintains an optimum temperature of the sodium hypochlorite generator in order to produce sodium hypochlorite of a high concentration with high efficiency.

    摘要翻译: 本发明提供一种基于使用软水和盐的电解生产次氯酸钠的开孔型设备。 该装置包括:次氯酸钠发生器,其包括由支撑件支撑的多个电极板,设置在支撑件上方的用于气流的流动通道和电极板,以及与流路连通的进气孔和排气孔 ; 用于降低流动通道的温度的冷却单元; 以及控制器,用于通过检测次氯酸钠发生器的温度来控制冷却单元的操作。 该设备不断保持次氯酸钠发生器的最佳温度,以高效率生产高浓度次氯酸钠。

    Deepwater oil recovery process
    7.
    发明申请
    Deepwater oil recovery process 审中-公开
    深水油回收过程

    公开(公告)号:US20120018386A1

    公开(公告)日:2012-01-26

    申请号:US13157143

    申请日:2011-06-09

    摘要: Ozone/oxygen gas is mixed with treated seawater at 30% quality foam and injected to the wellhead at the sea floor. At the seafloor, a tank mixing eductor would be used to mix high pressure oxygen bubbles with the oil contaminated seawater by shearing the oil globs into small oil droplets allowing the new surface area to immediately react with the dissolved ozone/oxygen in the seawater. The ozone/oxygen admixture creating an attraction force between the droplets and the oxygen bubbles. As the droplets and bubble rise, they form larger spherical top-hat bubbles that rise faster in the seawater. In the preferred embodiment, the eductor employs a cone shape flow to direct a significant amount of the oil plume into a predictable area that can then be skimmed mechanically for harvesting or destruction.

    摘要翻译: 将臭氧/氧气与经处理的海水混合,质量为30%的泡沫,并注入海底井口。 在海底,将使用罐混合喷射器将高压氧气泡与油污染的海水混合,通过将油球剪切成小油滴,使新表面积立即与海水中溶解的臭氧/氧气反应。 臭氧/氧气混合物在液滴和氧气泡之间产生吸引力。 随着液滴和气泡的上升,它们形成较大的球形顶帽气泡,其在海水中上升得更快。 在优选实施例中,喷射器采用锥形流将大量油羽引导到可预测的区域中,然后可以机械地撇去油料以进行收获或破坏。

    Chlorohydrin process
    9.
    发明授权
    Chlorohydrin process 失效
    氯醇过程

    公开(公告)号:US6043400A

    公开(公告)日:2000-03-28

    申请号:US765755

    申请日:1996-12-30

    申请人: Edward M. Jorge

    发明人: Edward M. Jorge

    摘要: This invention is a process for preparing chlorohydrins by reacting a chlorinating species, such as hypochlorous acid, with at least one unsaturated organic compound, such as propylene or butylene, at a pH of greater than 6.0. The chlorinating species is formed in a first step by reacting a source of chlorine, such as Cl.sub.2 gas, with an aqueous pH adjusting source, such as aqueous NaOH.

    摘要翻译: 本发明是通过使氯代物质如次氯酸与至少一种不饱和有机化合物如丙烯或丁烯在大于6.0的pH下反应来制备氯代醇的方法。 氯化物质通过使诸如Cl 2气体的氯源与含水pH调节源如NaOH水溶液反应在第一步中形成。

    Hypochlorite bleaching compositions
    10.
    发明授权
    Hypochlorite bleaching compositions 失效
    次氯酸盐漂白组合物

    公开(公告)号:US5914069A

    公开(公告)日:1999-06-22

    申请号:US640968

    申请日:1997-01-17

    IPC分类号: C01B11/06

    CPC分类号: C01B11/062

    摘要: Liquid aqueous bleaching compositions are disclosed which comprise hypochlorite and a specific complexing agent or mixtures thereof selected from the group consisting of polycarboxylic acid derivatives of pyridine or the salts thereof. The compositions have a pH from 11-14 and preferably further comprise a calcium/magnesium precipitation system. The complexing agent counteracts the adverse affect which certain metal ions have on fabric strength and fabric color when hypochlorite bleaches are used in the presence of said ions.

    摘要翻译: PCT No.PCT / US94 / 12746 Sec。 371日期1997年1月17日 102(e)日期1997年1月17日PCT 1994年11月4日PCT PCT。 第WO95 / 13416号公报 日期1995年5月18日公开了含有次氯酸盐和选自吡啶的多元羧酸衍生物或其盐的特定络合剂或其混合物的液态含水漂白组合物。 组合物的pH为11-14,优选还包含钙/镁沉淀体系。 当在所述离子存在下使用次氯酸盐漂白剂时,络合剂抵消某些金属离子对织物强度和织物颜色的不利影响。