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公开(公告)号:US20240001318A1
公开(公告)日:2024-01-04
申请号:US18368391
申请日:2023-09-14
申请人: Liang-Yuh Chen
发明人: Liang-Yuh Chen
IPC分类号: B01J8/18 , C01B13/14 , C01B13/34 , B22F9/22 , C01G1/02 , B22F9/08 , B01J8/24 , B01J12/02 , C01B25/45 , H01M4/04 , H01M4/36
CPC分类号: B01J8/18 , C01B13/14 , C01B13/34 , B22F9/22 , C01G1/02 , B22F9/082 , B01J8/1827 , B01J8/24 , B01J12/02 , C01B25/45 , H01M4/04 , H01M4/0471 , H01M4/36 , H01M4/505
摘要: A continuous process for producing a material of a battery cell using a system having a mist generator, a drying chamber, one or more gas-solid separators and a reactor is provided. A mist generated from a liquid mixture of two or more metal precursor compounds in desired ratio is dried inside the drying chamber. Heated air or gas is served as the gas source for forming various gas-solid mixtures and as the energy source for reactions inside the drying chamber and the reactor. One or more gas-solid separators are used in the system to separate gas-solid mixtures from the drying chamber into solid particles mixed with the metal precursor compounds and continuously deliver the solid particles into the reactor for further reaction to obtain final solid material particles with desired crystal structure, particle size, and morphology.
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公开(公告)号:US20230031067A1
公开(公告)日:2023-02-02
申请号:US17963402
申请日:2022-10-11
发明人: Rupa Hiremath Darji , James Newhouse , Vinothan N. Manoharan , Victoria Hwang , Anna B. Stephenson
摘要: Porous metal oxide microspheres are prepared via a process comprising forming a liquid solution or dispersion of polydisperse polymer nanoparticles and a metal oxide; forming liquid droplets from the solution or dispersion; drying the liquid droplets to provide polymer template microspheres comprising polymer nanospheres and metal oxide; and removing the polymer nanospheres from the template microspheres to provide the porous metal oxide microspheres. The porous microspheres exhibit saturated colors and are suitable as colorants for a variety of end-uses.
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公开(公告)号:US11511251B2
公开(公告)日:2022-11-29
申请号:US16104841
申请日:2018-08-17
申请人: Liang-Yuh Chen
发明人: Liang-Yuh Chen
IPC分类号: B01J8/18 , C01B13/14 , C01B13/34 , B22F9/22 , C01G1/02 , B22F9/08 , B01J8/24 , B01J12/02 , C01B25/45 , H01M4/04 , H01M4/36 , H01M4/505 , H01M4/525
摘要: A system and method thereof are provided for multi-stage processing of one or more precursor compounds into a battery material. The system includes a mist generator, a drying chamber, one or more gas-solid separators, and one or more in-line reaction modules comprised of one or more gas-solid feeders, one or more gas-solid separators, and one or more reactors. Various gas-solid mixtures are formed within the internal plenums of the drying chamber, the gas-solid feeders, and the reactors. In addition, heated air or gas is served as the energy source within the processing system and as the gas source for forming the gas-solid mixtures to facilitate reaction rate and uniformity of the reactions therein. Precursor compounds are continuously delivered into the processing system and processed in-line through the internal plenums of the drying chamber and the reaction modules into final reaction particles useful as a battery material.
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公开(公告)号:US11247912B2
公开(公告)日:2022-02-15
申请号:US16306225
申请日:2017-06-02
发明人: Masakazu Enomura , Daisuke Honda
IPC分类号: C01F17/235 , C01G49/06 , C01G9/02 , C09C1/24 , C01B33/02 , C01B33/32 , C01G53/00 , C09C3/06 , C01B13/14 , C01F17/206 , C01G49/02 , C09D7/62 , C09C1/04 , B22F1/00 , C09C3/12 , C01G23/04
摘要: With an aim to provide a method for producing an oxide particle with controlled color characteristics and also provide an oxide particle with controlled color characteristics, the present invention provides a method for producing an oxide particle, wherein the color characteristics of the oxide particle are controlled by controlling a ratio of an M-OH bond between an element (M) and a hydroxide group (OH) or an M-OH bond/M-O bond ratio, where the element (M) is one element or plural different elements other than oxygen or hydrogen included in the oxide particle selected from metal oxide particles and semi-metal oxide particles. According to the present invention, by controlling the M-OH bond or the M-OH bond/M-O bond ratio of the metal oxide particle or the semi-metal oxide particle, the oxide particle with controlled color characteristics of any of reflectance, transmittance, molar absorption coefficient, hue, and saturation can be provided.
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公开(公告)号:US11179694B2
公开(公告)日:2021-11-23
申请号:US16126338
申请日:2018-09-10
发明人: Rupa Hiremath Darji , James Newhouse , Vinothan N. Manoharan , Victoria Hwang , Anna B. Stephenson
摘要: Porous metal oxide microspheres are prepared via a process comprising forming a liquid dispersion of polymer nanoparticles and a metal oxide; forming liquid droplets of the dispersion; drying the droplets to provide polymer template microspheres comprising polymer nanospheres; and removing the polymer nanospheres from the template microspheres to provide the porous metal oxide microspheres. The porous microspheres exhibit saturated colors and are suitable as colorants for a variety of end-uses.
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公开(公告)号:US11052461B2
公开(公告)日:2021-07-06
申请号:US16306446
申请日:2017-05-25
发明人: Masakazu Enomura , Daisuke Honda
IPC分类号: C09C3/06 , C09C1/24 , B22F1/00 , C01G49/06 , C01G9/02 , C01B33/02 , C01B33/32 , C01G53/00 , C01B13/14 , C01F17/206 , C01G49/02 , C09D7/62 , C09C1/04 , C09C3/12 , C01G23/04
摘要: The present invention is a method of producing silicon compound coated oxide particles in which at least a part of a surface of a metal oxide particle is coated with a silicon compound, wherein wettability and color characteristics are controlled by controlling a ratio of Si—OH bonds contained in the silicon compound coated oxide particles. By the present invention, silicon compound coated oxide particles having controlled wettability such as hydrophilicity, water repellency or oil repellency, and controlled color characteristics of either reflectivity, molar absorption coefficient or transmittance can be provided.
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公开(公告)号:US20210170355A1
公开(公告)日:2021-06-10
申请号:US17133478
申请日:2020-12-23
申请人: eJoule, Inc.
发明人: Liang-Yuh Chen
IPC分类号: B01J8/18 , C01B13/14 , C01B13/34 , B22F9/22 , C01G1/02 , B22F9/08 , B01J8/24 , B01J12/02 , C01B25/45 , H01M4/04 , H01M4/36
摘要: A system and method thereof are provided for multi-stage processing of one or more precursor compounds into a battery material. The system includes a mist generator, a drying chamber, one or more gas-solid separators, and one or more in-line reaction modules comprised of one or more gas-solid feeders, one or more gas-solid separators, and one or more reactors. Various gas-solid mixtures are formed within the internal plenums of the drying chamber, the gas-solid feeders, and the reactors. In addition, heated air or gas is served as the energy source within the processing system and as the gas source for forming the gas-solid mixtures to facilitate reaction rate and uniformity of the reactions therein. Precursor compounds are continuously delivered into the processing system and processed in-line through the internal plenums of the drying chamber and the reaction modules into final reaction particles useful as a battery material.
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公开(公告)号:US11021403B2
公开(公告)日:2021-06-01
申请号:US16390288
申请日:2019-04-22
发明人: Michael David Hill
IPC分类号: C04B35/626 , C04B35/462 , C04B35/468 , C04B35/499 , C01B13/14 , C01G23/00 , H01B3/12 , C01G33/00
摘要: Disclosed are embodiments of tungsten bronze crystal structures that can have both a high dielectric constant and low temperature coefficient, making them advantageous for applications that experience temperature changes and gradients. In particular, tantalum can be substituted into the crystal structure to improve properties. Embodiments of the material can be useful for radiofrequency applications such as resonators and antennas.
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公开(公告)号:US10882109B2
公开(公告)日:2021-01-05
申请号:US16306242
申请日:2017-06-01
发明人: Masakazu Enomura , Daisuke Honda
IPC分类号: B22F1/00 , C09C3/12 , C01G49/06 , C01G9/02 , C09C1/24 , C01B33/02 , C01B33/32 , C01G53/00 , C09C3/06 , C01B13/14 , C01F17/206 , C01G49/02 , C09D7/62 , C09C1/04 , C01G23/04
摘要: The present invention relates to silicon-compound-coated fine metal particles, with which surfaces of fine metal particles, composed of at least one type of metal element or metalloid element, are at least partially coated with a silicon compound and a ratio of Si—OH bonds contained in the silicon-compound-coated fine metal particles is controlled to be 0.1% or more and 70% or less. By the present invention, silicon-compound-coated fine metal particles that are controlled in dispersibility and other properties can be provided by controlling the ratio of Si—OH bonds or the ratio of Si—OH bonds/Si—O bonds contained in the silicon-compound-coated fine metal particles. By controlling the ratio of Si—OH bonds or the ratio of Si—OH bonds/Si—O bonds, a composition that is more appropriate for diversifying applications and targeted properties of silicon-compound-coated fine metal particles than was conventionally possible can be designed easily.
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公开(公告)号:US10800683B2
公开(公告)日:2020-10-13
申请号:US16282094
申请日:2019-02-21
申请人: Calix Ltd
发明人: Mark Sceats , Adam Vincent
IPC分类号: C02F1/68 , C01F5/16 , C01B13/14 , C04B2/04 , B01J19/18 , B01J13/00 , C02F1/52 , C02F1/66 , C02F101/20 , C02F103/00
摘要: A method of manufacture of high-solids hydroxide slurries from caustic calcined carbonate powder is described, whereby the properties of the slurry are its low resistance to shear thinning to facilitate transport, a high stability for transport and storage, ease of reconstitution after long periods of storage, and, as required, a high concentration of chemically reactive species at the particle surface. The method achieves these specifications by mixing caustic calcined carbonate or hydroxide powder with water in an insulated reactor vessel, and agitating the slurry sufficiently such that the hydration reaction causes the water to spontaneously boil, such that the remaining hydration proceeds spontaneously under the fixed conditions of boiling through the water loss. The mixing process is preferably carried out by a shear pump. A viscosity modifier, such as acetic acid, is used to thin the slurry to enable the mixing system to maintain uniform mixing. The reaction is terminated when the boiling has spontaneously ceased and the temperature has spontaneously dropped to a set point though the reactor heat losses, where the processing time is sufficiently long that the slurry meets the desired specifications.
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