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    PROCESS FOR MANUFACTURING HIGHLY SULPHATED FATTY ACIDS AND FATTY ACID DERIVATIVES
    24.
    发明申请
    PROCESS FOR MANUFACTURING HIGHLY SULPHATED FATTY ACIDS AND FATTY ACID DERIVATIVES 审中-公开
    制造高硫脂肪酸和脂肪酸衍生物的方法

    公开(公告)号：WO1990004586A1

    公开(公告)日：1990-05-03

    申请号：PCT/EP1989001257

    申请日：1989-10-20

    Applicant: CHEMISCHE FABRIK STOCKHAUSEN GMBH ,  PEPPMÖLLER, Reinmar ,  DAHMEN, Kurt

    Inventor： CHEMISCHE FABRIK STOCKHAUSEN GMBH

    IPC: C07C303/24

    CPC classification number: C07C303/24 ,  C07C305/06 ,  C07C305/10

    Abstract: To obtain highly sulphated fatty acids, hydroxy fatty acids or oxalkylated hydroxy fatty acids, the reaction mixture obtained from the sulphatation of unsaturated fatty acid esters and/or saturated hydroxy fatty acid esters and/or oxalkylated hydroxy fatty acid esters is neutralized, separated if necessary from the brine, diluted with water and hydrolysed at a temperature between 20°C and 160°C after addition of a quantity of lye whose molar content is not greater than that of the organically bound sulphuric acid. After separation of the phases containing the non-sulphated starting products and the highly sulphated fatty acids, the latter are isolated from the aqueous phase.

    高分子凝胶用单体及高分子凝胶与制备方法
    25.
    发明申请
    高分子凝胶用单体及高分子凝胶与制备方法 审中-公开

    公开(公告)号：WO2022160357A1

    公开(公告)日：2022-08-04

    申请号：PCT/CN2021/074736

    申请日：2021-02-01

    Applicant: 苏州大学

    Inventor： 路建美 ,  徐庆锋

    IPC: C07F7/18 ,  C07C305/26 ,  C07C303/24 ,  C08G75/24 ,  B01J20/26 ,  B01J20/28 ,  B01J20/30

    Abstract: 本发明公开了高分子凝胶用单体及高分子凝胶与制备方法，4,4',4''-三羟基三苯甲烷与叔丁基二甲基氯硅烷反应，得到TPC-OTBS；在三乙胺存在下，4,4',4''-三羟基三苯甲烷与硫酰氟反应，制备TPC-OSO 2F；将TPC-OTBS、TPC-OSO 2F溶解在DMF中，加入DBU超声分散均匀，静置，得到高分子凝胶。本发明获得的凝胶通过静电作用和范德华力可选择性吸附有机溶剂。用SEM和TEM对固体材料的表明和内部形貌进行了表征，发现了其多孔的形貌，且较多为大孔。用红外，核磁表征了交联聚硫酸酯的结构，通过固体核磁氟谱和XPS元素证明了单体磺酰氟基团完全反应，交联聚硫酸酯与溶剂之间的相互作用力使其在吸附方面有较好的应用前景。

    PROCESS FOR SULFONATION OF 2-AMINOETHANOL HYDROGEN SULFATE ESTER TO PRODUCE TAURINE
    26.
    发明申请
    PROCESS FOR SULFONATION OF 2-AMINOETHANOL HYDROGEN SULFATE ESTER TO PRODUCE TAURINE 审中-公开

    公开(公告)号：WO2021248077A1

    公开(公告)日：2021-12-09

    申请号：PCT/US2021/036018

    申请日：2021-06-04

    Applicant: ARCHER DANIELS MIDLAND COMPANY

    Inventor： MA, Chi-Cheng ,  BRAZDIL, James ,  LUO, Hao

    IPC: B01D11/04 ,  C02F1/26 ,  C02F1/66 ,  C07C303/02 ,  C07C303/24

    Abstract: A process comprises continuously adding a first stream and a second stream to a sulfonation vessel, wherein the first stream comprises aminoethanol sulfate ester (AES) and the second stream comprises an aqueous solution of sodium sulfite (Na2SO3). The process comprises continuously mixing the AES and the aqueous solution of Na2SO3 in the sulfonation vessel, thus producing a mixture. The process comprises continuously subjecting the mixture to heat in the presence of an inert gas, thus converting the AES to the taurine via sulfonation. In an aspect, the AES has a residence time of no more than four hours in the sulfonation vessel. In an aspect the heating step is conducted at a temperature of at least 115° C and a pressure of at least 200 psi.

    FLOWABLE, HIGH ACTIVE, AQUEOUS FATTY ALKYL SULFATES
    27.
    发明申请
    FLOWABLE, HIGH ACTIVE, AQUEOUS FATTY ALKYL SULFATES 审中-公开
    可流动，高活性，水性脂肪酸碱金属硫酸盐

    公开(公告)号：WO2014072840A1

    公开(公告)日：2014-05-15

    申请号：PCT/IB2013/052211

    申请日：2013-03-20

    Applicant: GALAXY SURFACTANTS LTD.

    Inventor： GOPALAKRISHNAN, Ramakrishnan ,  UNNATHAN, Shekhar

    IPC: C07C41/03 ,  C07C303/24

    CPC classification number: A61Q5/02 ,  A61K8/463 ,  C07C41/03 ,  C07C303/24 ,  C07C305/10 ,  C07C43/11

    Abstract: The present invention relates to a process for preparing high-concentration, flowable aqueous fatty alkyl sulfate solution, said process comprises (i) ethoxylation of fatty alcohol with very low of about 0.3 to about 0.8 moles of ethylene oxide, and (ii) sulfating the ethoxylated fatty alcohol with specific reaction conditions, and (iii) neutralizing the sulfation product with an aqueous base. The obtained fatty alkyl sulfate solution contains at least 65% by weight of mixture of fatty alkyl sulfates and fatty alkyl ether sulfates in a weight ratio in the range from about 80:20 to about 50:50 wherein the average number of moles of ethylene oxide (EO) of the mixture is between 0.3 to 0.8; less than 3 ppm of dioxane; and water, and wherein the solution does not contain any antimicrobial or preservatives and is homogeneous, flowable and pumpable at 25°C.

    Abstract translation: 本发明涉及一种制备高浓度，可流动的脂肪族脂肪酸烷基酯水溶液的方法，所述方法包括（i）脂肪醇的乙氧基化，极低的约0.3至约0.8摩尔的环氧乙烷，和（ii）硫酸化 具有特定反应条件的乙氧基化脂肪醇，和（iii）用碱水溶液中和硫酸化产物。 所获得的脂肪烷基硫酸盐溶液含有至少65重量％的脂肪烷基硫酸盐和脂肪烷基醚硫酸盐的混合物，其重量比在约80:20至约50:50的范围内，其中环氧乙烷的平均摩尔数 （EO）为0.3〜0.8; 小于3ppm的二恶烷; 和水，并且其中所述溶液不含任何抗微生物剂或防腐剂，并且在25℃下是均匀的，可流动的和可泵送的。

    PROCESS FOR THE PREPARATION OF ACYLATED SECONDARY ALCOHOL ALKOXYLATES AND SECONDARY ALCOHOL ALKOXYLATES
    29.
    发明申请
    PROCESS FOR THE PREPARATION OF ACYLATED SECONDARY ALCOHOL ALKOXYLATES AND SECONDARY ALCOHOL ALKOXYLATES 审中-公开
    制备二级醇酸二烷基酯和次级醇酸烷基酯的方法

    公开(公告)号：WO2010049465A1

    公开(公告)日：2010-05-06

    申请号：PCT/EP2009/064241

    申请日：2009-10-28

    Applicant: SHELL INTERNATIONALE RESEARCH MAATSCHAPPIJ B.V. ,  VAN DER HEIJDEN, Harry ,  VAN DER MADE, Renata, Helena ,  MEURS, Jan, Hermen, Hendrik ,  ON, Quoc An ,  VAN ZON, Arie

    Inventor： VAN DER HEIJDEN, Harry ,  VAN DER MADE, Renata, Helena ,  MEURS, Jan, Hermen, Hendrik ,  ON, Quoc An ,  VAN ZON, Arie

    IPC: C07C67/26 ,  C07C67/04 ,  C07C69/24 ,  C07C41/26 ,  C07C43/11 ,  C07C303/24 ,  C07C303/10 ,  C08G65/26

    CPC classification number: C07C67/04 ,  C07C41/26 ,  C07C67/26 ,  C07C303/24 ,  C08G65/2615 ,  C08G65/2648 ,  C08G65/2675 ,  C08G65/2678 ,  C08G65/269 ,  C07C305/10 ,  C07C69/14 ,  C07C43/11

    Abstract: A process for the preparation of acylated secondary alcohol alkoxylates, said process comprising : (i) reaction of one or more internal olefins with one or more carboxylic acids in the presence of a catalyst composition in order to form one or more carboxylic acid esters; (ii) reaction of one or more carboxylic acid esters from step (i) with one or more alkylene oxide reactants, in the presence of a catalytically effective amount of a catalyst composition comprising: (a) one or more alkaline earth metal salts of carboxylic and/or hydroxycarboxylic acids and/or hydrates of the former; (b) an oxy-acid selected from sulphuric acid and ortho-phosphoric acid; (c) an alcohol and/or an ester; and/or products of the reciprocal reactions of (a), (b) and/or (c) in order to form one or more acylated secondary alcohol alkoxylates; and optionally (iii) hydrolysis or transesterification of one or more acylated secondary alcohol alkoxylates from step (ii) in order to form one or more secondary alcohol alkoxylates; and a process for making secondary alcohol alkoxy sulphates comprising the steps of: preparing secondary alcohol alkoxylates by the afore-mentioned process; and sulphating the secondary alcohol alkoxylates.

    Abstract translation: 一种制备酰化仲醇烷氧基化物的方法，所述方法包括：（i）在催化剂组合物存在下使一种或多种内烯烃与一种或多种羧酸反应以形成一种或多种羧酸酯; （ii）在催化有效量的催化剂组合物的存在下，将一种或多种来自步骤（i）的羧酸酯与一种或多种烯化氧反应物反应，所述催化剂组合物包含：（a）一种或多种羧酸碱土金属盐 和/或前者的羟基羧酸和/或水合物; （b）选自硫酸和正磷酸的氧酸; （c）醇和/或酯; 和/或（a），（b）和/或（c）的相互反应的产物，以便形成一种或多种酰化的仲醇烷氧基化物; 和任选地（iii）来自步骤（ii）的一种或多种酰化仲醇烷氧基化物的水解或酯交换以形成一种或多种仲醇烷氧基化物; 以及制备仲醇烷氧基硫酸盐的方法，包括以下步骤：通过上述方法制备仲醇烷氧基化物; 并使仲醇烷氧基化物硫酸化。

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