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    METHOD FOR DIRECT-OXYGENATION OF ALKANE GASES
    1.
    发明申请
    METHOD FOR DIRECT-OXYGENATION OF ALKANE GASES 审中-公开
    碱性气体直接氧化方法

    公开(公告)号：WO2007133310A3

    公开(公告)日：2008-07-24

    申请号：PCT/US2007004297

    申请日：2007-02-19

    Applicant: GAS TECH LLC ,  PAWLAK NATHAN A ,  CARR ROBERT W ,  GRUNCH ROGER J

    Inventor： PAWLAK NATHAN A ,  CARR ROBERT W ,  GRUNCH ROGER J

    IPC: C07C27/10 ,  C07B41/02

    CPC classification number: B01J19/26 ,  B01F5/04 ,  B01F5/0682 ,  B01J19/02 ,  B01J2219/00006 ,  B01J2219/00063 ,  B01J2219/00119 ,  B01J2219/00123 ,  B01J2219/00166 ,  B01J2219/0209 ,  B01J2219/0245

    Abstract: A method for alkyl oxygenate (e.g., methanol) manufacture via partial oxidation of alkane (methane) uses an injectively-mixed backmixing reaction chamber in fluid communication with a tubular-flow reactor. Alkyl free radicals are induced in the backmixing reaction chamber prior to being fed through a flow-restriction baffle to the tubular-flow reactor. Injective intermixing of feed streams agitates the backmixing reaction chamber. In one embodiment, a variable position flow restriction baffle is axially moved to commensurately modify the backmixing reaction chamber and tubular-flow reactor volumes. In another embodiment, the tubular-flow reactor is quenched with a variable position quenching input. The method further provides for condensing the output stream from the reaction system in a condensing scrubber and also for recycling a portion of the scrubbed output stream to the reactor system.

    Abstract translation: 通过烷烃（甲烷）的部分氧化制备烷基含氧化合物（例如甲醇）的方法使用与管式流动反应器流体连通的注射混合的回混反应室。 在通过流量限制挡板进入管式流动反应器之前，在回混反应室中诱导烷基自由基。 进料流的注入混合搅拌反混合反应室。 在一个实施例中，可变位置流量限制挡板被轴向移动以相应地修改回混反应室和管式流动反应器体积。 在另一个实施例中，管状流动反应器用可变位置淬灭输入淬火。 该方法进一步提供了在冷凝洗涤器中冷凝来自反应系统的输出流，还用于将洗涤的输出流的一部分再循环到反应器系统。

    METHOD FOR DIRECT-OXYGENATION OF ALKANE GASES
    2.
    发明申请
    METHOD FOR DIRECT-OXYGENATION OF ALKANE GASES 审中-公开
    碱性气体直接氧化方法

    公开(公告)号：WO2007133310A2

    公开(公告)日：2007-11-22

    申请号：PCT/US2007/004297

    申请日：2007-02-19

    Applicant: GAS TECHNOLOGIES LLC ,  PAWLAK, Nathan A. ,  CARR, Robert W. ,  GRUNCH, Roger J.

    Inventor： PAWLAK, Nathan A. ,  CARR, Robert W. ,  GRUNCH, Roger J.

    IPC: G09G3/36

    CPC classification number: B01J19/26 ,  B01F5/04 ,  B01F5/0682 ,  B01J19/02 ,  B01J2219/00006 ,  B01J2219/00063 ,  B01J2219/00119 ,  B01J2219/00123 ,  B01J2219/00166 ,  B01J2219/0209 ,  B01J2219/0245

    Abstract: A method for alkyl oxygenate (e.g., methanol) manufacture via partial oxidation of alkane (methane) uses an injectively-mixed backmixing reaction chamber in fluid communication with a tubular-flow reactor. Alkyl free radicals are induced in the backmixing reaction chamber prior to being fed through a flow-restriction baffle to the tubular-flow reactor. Injective intermixing of feed streams agitates the backmixing reaction chamber. In one embodiment, a variable position flow restriction baffle is axially moved to commensurately modify the backmixing reaction chamber and tubular-flow reactor volumes. In another embodiment, the tubular-flow reactor is quenched with a variable position quenching input. The method further provides for condensing the output stream from the reaction system in a condensing scrubber and also for recycling a portion of the scrubbed output stream to the reactor system.

    Abstract translation: 通过烷烃（甲烷）的部分氧化制备烷基含氧化合物（例如甲醇）的方法使用与管式流动反应器流体连通的注射混合回混反应室。 在通过流量限制挡板进入管式流动反应器之前，在回混反应室中诱导烷基自由基。 进料流的注入混合搅拌反混合反应室。 在一个实施例中，可变位置流量限制挡板被轴向移动以相应地修改回混反应室和管式流动反应器体积。 在另一个实施例中，管状流动反应器用可变位置淬灭输入淬火。 该方法进一步提供了在冷凝洗涤器中冷凝来自反应系统的输出流，还用于将洗涤的输出流的一部分再循环到反应器系统。

    TANDEM REACTOR SYSTEM HAVING AN INJECTIVELY-MIXED BACKMIXING REACTION CHAMBER, TUBULAR-REACTOR, AND AXIALLY MOVABLE INTERFACE
    3.
    发明申请
    TANDEM REACTOR SYSTEM HAVING AN INJECTIVELY-MIXED BACKMIXING REACTION CHAMBER, TUBULAR-REACTOR, AND AXIALLY MOVABLE INTERFACE 审中-公开

    公开(公告)号：WO2007133309A3

    公开(公告)日：2007-11-22

    申请号：PCT/US2007/004185

    申请日：2007-02-19

    Applicant: GAS TECHNOLOGIES LLC ,  PAWLAK, Nathan, A. ,  CARR, Robert W. ,  GRUNCH, Roger J.

    Inventor： PAWLAK, Nathan, A. ,  CARR, Robert W. ,  GRUNCH, Roger J.

    IPC: B01J19/26 ,  B01J12/00 ,  C07C29/50

    Abstract: A reactor system for gas phase reacting of at least two fluid feed streams, where the reactor system has an injectively-mixed backmixing reaction chamber in fluid communication with a tubular-flow reactor. The injectively-mixed backmixing reaction chamber has a bulkhead that slides during real-time operation to either diminish or expand the internal volume of the backmixing reaction chamber. In one embodiment, the effective passageway space through the bulkhead is also variably adjustable. In another embodiment, the tubular-flow reactor shares the bulkhead so that axial bulkhead movement commensurately expands one reaction space while diminishing the other reaction space. Input gas streams enter the backmixing reaction chamber with sufficient velocity to turbulently agitate the contents of the injectively-mixed backmixing reaction chamber by injective intermixing of the alkane-containing gas feed stream and the oxygen-containing gas feed stream. A focal application is for direct (partial) oxidative conversion of natural gas to alkyl oxygenates.

    SYSTEM FOR DIRECT-OXYGENATION OF ALKANE GASES
    6.
    发明申请
    SYSTEM FOR DIRECT-OXYGENATION OF ALKANE GASES 审中-公开
    碱性气体直接氧化系统

    公开(公告)号：WO2007133313A1

    公开(公告)日：2007-11-22

    申请号：PCT/US2007/004557

    申请日：2007-02-19

    Applicant: GAS TECHNOLOGIES LLC ,  PAWLAK, Nathan A. ,  CARR, Robert W. ,  GRUNCH, Roger J.

    Inventor： PAWLAK, Nathan A. ,  CARR, Robert W. ,  GRUNCH, Roger J.

    IPC: C07B63/02

    CPC classification number: B01J19/2415 ,  B01D3/14 ,  B01D53/1487 ,  B01D53/18 ,  B01D2257/504 ,  B01D2257/704 ,  B01J4/002 ,  B01J19/006 ,  B01J19/26 ,  B01J2219/00006 ,  B01J2219/00123 ,  B01J2219/00159 ,  B01J2219/00777 ,  B01J2219/182 ,  B01J2219/1943 ,  C07C29/50 ,  Y02P20/152 ,  Y02P70/34 ,  C07C31/04

    Abstract: An apparatus for alkyl oxygenate (e.g., methanol) manufacture via partial oxidation of alkane (methane) has an injectively-mixed backmixing reaction chamber in fluid communication with a tubular-flow reactor. The injectively-mixed backmixing reaction chamber induces alkyl free radicals prior to input to the tubular-flow reactor. lnjective intermixing of feed streams agitates the backmixing reaction chamber. In one embodiment, a variable position bulkhead axially moves to commensurately modify the backmixing reaction chamber and tubular-flow reactor volumes. In another embodiment, the tubular-flow reactor has a variable position quenching input. Both "hairbrush" and conical input inserts facilitate turbulent injective admixing of the input feed streams in the injectively-mixed backmixing reaction chamber. A condensing scrubber is also used for treating the output stream from the reaction system.

    Abstract translation: 通过烷烃（甲烷）的部分氧化制造烷基含氧化合物（例如甲醇）的装置具有与管式流动反应器流体连通的注射混合的回混反应室。 注入混合的回混反应室在输入管式流动反应器之前引发烷基自由基。 进料流的目标混合搅拌反混合反应室。 在一个实施例中，可变位置隔板轴向移动以相应地修改回混反应室和管式流动反应器体积。 在另一个实施例中，管式流动反应器具有可变位置淬灭输入。 “发刷”和锥形输入插件两者都有助于在喷射混合后混合反应室中的输入进料流的湍流注入混合。 冷凝洗涤器也用于处理来自反应系统的输出流。

    TANDEM REACTOR SYSTEM HAVING AN INJECTIVELY-MIXED BACKMIXING REACTION CHAMBER, TUBULAR-REACTOR, AND AXIALLY MOVABLE INTERFACE
    7.
    发明申请
    TANDEM REACTOR SYSTEM HAVING AN INJECTIVELY-MIXED BACKMIXING REACTION CHAMBER, TUBULAR-REACTOR, AND AXIALLY MOVABLE INTERFACE 审中-公开
    具有混合的反射反应室，管状反应器和轴向可移动接口的TANDEM反应器系统

    公开(公告)号：WO2007133309A2

    公开(公告)日：2007-11-22

    申请号：PCT/US2007004185

    申请日：2007-02-19

    Applicant: GAS TECH LLC ,  PAWLAK NATHAN A ,  CARR ROBERT W ,  GRUNCH ROGER J

    Inventor： PAWLAK NATHAN A ,  CARR ROBERT W ,  GRUNCH ROGER J

    IPC: G11C8/00

    CPC classification number: B01J19/26 ,  B01F5/04 ,  B01F5/0682 ,  B01J19/02 ,  B01J2219/00006 ,  B01J2219/00063 ,  B01J2219/00119 ,  B01J2219/00123 ,  B01J2219/00166 ,  B01J2219/0209 ,  B01J2219/0245

    Abstract: A reactor system for gas phase reacting of at least two fluid feed streams, where the reactor system has an injectively-mixed backmixing reaction chamber in fluid communication with a tubular-flow reactor. The injectively-mixed backmixing reaction chamber has a bulkhead that slides during real-time operation to either diminish or expand the internal volume of the backmixing reaction chamber. In one embodiment, the effective passageway space through the bulkhead is also variably adjustable. In another embodiment, the tubular-flow reactor shares the bulkhead so that axial bulkhead movement commensurately expands one reaction space while diminishing the other reaction space. Input gas streams enter the backmixing reaction chamber with sufficient velocity to turbulently agitate the contents of the injectively-mixed backmixing reaction chamber by injective intermixing of the alkane-containing gas feed stream and the oxygen-containing gas feed stream. A focal application is for direct (partial) oxidative conversion of natural gas to alkyl oxygenates.

    Abstract translation: 一种用于至少两种流体进料流的气相反应的反应器系统，其中反应器系统具有与管式流动反应器流体连通的注射混合的后混合反应室。 喷射混合后混合反应室具有在实时操作期间滑动的隔板，以减小或扩大回混反应室的内部体积。 在一个实施例中，穿过隔板的有效通道空间也是可变的。 在另一个实施例中，管状流动反应器共用舱壁，使得轴向隔板移动相应地扩展一个反应空间，同时减小另一个反应空间。 输入气流以足够的速度进入回混反应室，通过含烷烃气体进料流和含氧气体进料流的注入混合来湍动地搅拌喷射混合回混反应室的内容物。 焦点应用是将天然气直接（部分）氧化转化为烷基含氧化合物。

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