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    SYNTHESIS OF OLIGOMERIC DIVINYLDIALKYLSILANE CONTAINING COMPOSITIONS
    5.
    发明申请
    SYNTHESIS OF OLIGOMERIC DIVINYLDIALKYLSILANE CONTAINING COMPOSITIONS 审中-公开
    含有低分子二甲基硅氧烷的组合物的合成

    公开(公告)号：WO2015130652A1

    公开(公告)日：2015-09-03

    申请号：PCT/US2015/017247

    申请日：2015-02-24

    Applicant: THE GOVERNMENT OF THE UNITED STATES OF AMERICA, AS REPRESENTED BY THE SECRETARY OF THE NAVY ,  LASKOSKI, Matthew ,  KELLER, Teddy, M. ,  SAAB, Andrew

    Inventor： LASKOSKI, Matthew ,  KELLER, Teddy, M. ,  SAAB, Andrew

    IPC: C08G65/48 ,  C08F290/02 ,  C08F283/06 ,  C08F283/12

    CPC classification number: C08G65/48 ,  C08G65/4012

    Abstract: A method of: providing a solution of: a dichloroaromatic compound having an electron-withdrawing group bound to each aromatic ring containing one of the chloride groups; an excess of a dihydroxyaromatic compound; a base; and a solvent; heating the solution to a temperature at which the dichloroaromatic compound and the dihydroxyaromatic compound react to form an aromatic ether oligomer; and reacting the aromatic ether oligomer with a chlorodialkylvinylsilane to form one or more vinyl-terminated compounds having the formula below. The aromatic ether oligomer is a dihydroxy-terminated compound or a dimetallic salt thereof. Water formed during the heating is concurrently distilled from the solution. Each R is an alkyl group, Ar 1 is a residue from the dichloroaromatic compound, Ar 2 is a residue from the dihydroxyaromatic compound, and n is a non-negative integer.

    Abstract translation: 一种方法：提供以下溶液：具有吸电子基团的二氯芳族化合物与每个含有一个氯基团的芳香环结合; 过量的二羟基芳族化合物; 一个基地 和溶剂; 将溶液加热到二氯芳族化合物和二羟基芳族化合物反应的温度以形成芳族醚低聚物; 并使芳族醚低聚物与氯二烷基乙烯基硅烷反应以形成一种或多种下式的乙烯基封端的化合物。 芳香醚低聚物是二羟基封端的化合物或其二金属盐。 在加热过程中形成的水​​从溶液中同时蒸馏出来。 每个R为烷基，Ar 1为二氯芳族化合物的残基，Ar 2为二羟基芳族化合物的残基，n为非负整数。

    DIVINYLSILANE-TERMINATED AROMATIC ETHER-AROMATIC KETONE-CONTAINING COMPOUNDS
    7.
    发明申请
    DIVINYLSILANE-TERMINATED AROMATIC ETHER-AROMATIC KETONE-CONTAINING COMPOUNDS 审中-公开
    含有芳香木素的芳香酮类含酮化合物

    公开(公告)号：WO2009097252A1

    公开(公告)日：2009-08-06

    申请号：PCT/US2009/032076

    申请日：2009-01-27

    Applicant: THE GOVERNMENT OF THE UNITED STATES OF AMERICA, AS REPRESENTED BY THE SECRETARY OF THE NAVY ,  LASKOSKI, Matthew ,  KELLER, Teddy, M.

    Inventor： LASKOSKI, Matthew ,  KELLER, Teddy, M.

    IPC: B32B9/04 ,  C08G77/00

    CPC classification number: C08G65/48 ,  C08G65/4012

    Abstract: A compound having the formula: (Formula 1), Each Ar is an aromatic group. Each R is an alkyl group. The value n is a positive integer. The values of w, x, y, and z are 0 or 1. If y is 0 than x and z are 0 and w is 1, and if y is 1 than x and z have different values and w equals z. A thermoset made by crosslinking a silane-containing compound with the above compound. A method of making the above compound when y is 1 by: reacting 4,4'-difluorobenzophenone with an aromatic diol to form an oligomer; and reacting the oligomer with a vinyl dialkylsilane. A method of making the below compound by: reacting 4,4'-difluorobenzophcnonc with a vinyl dialkylsilane. Each R is an independently selected alkyl group. (formula 2)

    Abstract translation: 具有下式的化合物（式1），每个Ar是芳基。 每个R是烷基。 值n为正整数。 w，x，y和z的值为0或1.如果y为0，z为0且w为1，并且如果y为1，则x和z具有不同的值，w等于z。 通过将含硅烷化合物与上述化合物交联而制得的热固性材料。 当y为1时，通过使4,4'-二氟二苯甲酮与芳族二醇反应形成低聚物而制备上述化合物的方法; 并使低聚物与乙烯基二烷基硅烷反应。 通过以下方法制备下列化合物：使4,4'-二氟苯甲酸与乙烯基二烷基硅烷反应。 每个R是独立选择的烷基。 （式2）

    PHTHALONITRILE PREPOLYMER INTERMEDIATE
    8.
    发明申请
    PHTHALONITRILE PREPOLYMER INTERMEDIATE 审中-公开

    公开(公告)号：WO2015076934A2

    公开(公告)日：2015-05-28

    申请号：PCT/US2014/058229

    申请日：2014-09-30

    Applicant: THE GOVERNMENT OF THE UNITED STATES OF AMERICA, AS REPRESENTED BY THE SECRETARY OF THE NAVY ,  KELLER, Teddy, M. ,  LASKOSKI, Matthew

    Inventor： KELLER, Teddy, M. ,  LASKOSKI, Matthew

    IPC: C08G73/00 ,  C08G63/193 ,  C08G63/44 ,  C08L67/03

    CPC classification number: C08G73/024 ,  C08G65/40 ,  C08G73/02 ,  C08G73/06

    Abstract: A compound having: one or more of the below repeat units, one or more terminating Ar-NH- groups bound to carbon radicals, and one or more terminating -H groups bound to nitrogen radicals. Each R is an organic group and each Ar is an aromatic group. The compound is not a thermoset. A method of: mixing an aromatic amine having the formula Ar-NH2 with a phthalonitrile compound, heating the mixture to form the compound described above (Eq. 1), and cooling the mixture before the onset of gelation.

    Abstract translation: 具有下列重复单元中的一个或多个，与碳基结合的一个或多个终止的Ar-NH-基团以及与氮基团结合的一个或多个终止-H基团的化合物。 每个R是有机基团，每个Ar是芳族基团。 化合物不是热固性物质。 一种方法：将具有式Ar-NH 2的芳族胺与邻苯二甲腈化合物混合，加热混合物以形成上述化合物（式1），并在凝胶化开始之前冷却混合物。

    SYNTHESIS OF AND CURING ADDITIVES FOR PHTHALONITRILES
    9.
    发明申请
    SYNTHESIS OF AND CURING ADDITIVES FOR PHTHALONITRILES 审中-公开
    PHTHALONITRILES的合成与固化添加剂

    公开(公告)号：WO2014021946A1

    公开(公告)日：2014-02-06

    申请号：PCT/US2013/032051

    申请日：2013-03-15

    Applicant: THE GOV. OF THE U.S. OF AMERICA AS REPRESENTED BY THE SECRETARY OF THE NAVY ,  KELLER, Teddy, M. ,  LASKOSKI, Matthew ,  SAAB, Abdrew

    Inventor： KELLER, Teddy, M. ,  LASKOSKI, Matthew ,  SAAB, Abdrew

    IPC: C08G65/00 ,  C08K5/06 ,  C08G73/00 ,  C08G83/00

    CPC classification number: C08G73/024 ,  C08G65/40 ,  C08G65/4012 ,  C08G65/4087 ,  C08G65/4093 ,  C08G65/46 ,  C08G65/48 ,  C08G73/0672 ,  C08G2650/40 ,  Y10T428/2969

    Abstract: A method of: providing a solution of a dichloroaromatic compound having an electron-withdrawing group bound to each aromatic ring containing one of the chloride groups; an excess of a dihydroxyaromatic compound; an organic transition metal complex or a transition metal salt; a base; and a solvent; and heating the solution to a temperature at which the dichloroaromatic compound and the dihydroxyaromatic compound react to form an aromatic ether oligomer that is a dihydroxy-terminated compound or a dimetallic salt thereof. Water formed during the heating is concurrently distilled from the solution. A method of curing a phthalonitrile monomer in the presence of an acid and a curing agent to form a phthalonitrile thermoset.

    Abstract translation: 一种方法：提供具有吸电子基团的二氯芳族化合物与含有一个氯基团的每个芳香环结合的溶液; 过量的二羟基芳族化合物; 有机过渡金属络合物或过渡金属盐; 一个基地 和溶剂; 并将溶液加热到二氯芳族化合物和二羟基芳族化合物反应的温度，以形成作为二羟基封端的化合物或其二金属盐的芳族醚低聚物。 在加热过程中形成的水​​从溶液中同时蒸馏出来。 在酸和固化剂的存在下固化邻苯二甲腈单体以形成邻苯二甲腈热固性的方法。

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