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    METHODS OF HANDLING CHLORINATED COMPOUNDS USED FOR MANUFACTURING HFO-1234YF
    1.
    发明申请
    METHODS OF HANDLING CHLORINATED COMPOUNDS USED FOR MANUFACTURING HFO-1234YF 审中-公开
    用于制造HFO-1234YF的氯化化合物的处理方法

    公开(公告)号：WO2014120865A1

    公开(公告)日：2014-08-07

    申请号：PCT/US2014/013742

    申请日：2014-01-30

    Applicant: HONEYWELL INTERNATIONAL INC.

    Inventor： BEKTESEVIC, Selma ,  WANG, Haiyou ,  TUNG, Hsueh Sung

    IPC: C01B7/03

    CPC classification number: C01B7/01 ,  C07C17/389 ,  C07C17/42 ,  C07C21/04

    Abstract: This invention provides methods for handling, storing and/or transporting reactive chlorinated compounds such as 1230xa whereby decomposition reactions are reduced or eliminated by employing one or more anti-decomposition techniques selected from the group consisting of: (a) providing a 1230xa supply with little or no moisture, HCl, and/or metallic ions, (b) providing a storage and/or transport tank preferably lined and/or coated with one or more suitable materials, (c) transferring 1230xa, preferably stabilized 1230xa, into a storage and/or transportation tank in such a way that no exposure of the 1230xa to air occurs, (d) handling, storing, and/or transporting 1230xa under the protection of a dried inert gas such as nitrogen, (e) optionally providing a device that can remove any HCl generated during the storage and/or transportation of 1230xa; and (f) combinations of two or more of these anti-decomposition techniques.

    Abstract translation: 本发明提供了用于处理，储存和/或运输反应性氯化化合物如1230xa的方法，由此通过使用一种或多种选自以下的抗分解技术来降低或消除分解反应：（a）提供少量的1230xa供应 或没有水分，HCl和/或金属离子，（b）提供优选用一种或多种合适材料衬里和/或涂覆的储存和/或运输罐，（c）将1230xa，优选稳定的1230xa转移到储存器和 /或运输罐，使得不会发生1230xa暴露于空气，（d）在干燥的惰性气体如氮气的保护下处理，储存和/或运输1230xa，（e）可选地提供一种装置， 可以去除在储存和/或运输1230xa期间产生的任何HCl; 和（f）这些抗分解技术中的两种或更多种的组合。

    PROCESS FOR PRODUCING 2,3,3,3-TETRAFLUOROPROPENE
    4.
    发明申请
    PROCESS FOR PRODUCING 2,3,3,3-TETRAFLUOROPROPENE 审中-公开
    生产2,3,3,3-四氯丙烯的方法

    公开(公告)号：WO2013130385A1

    公开(公告)日：2013-09-06

    申请号：PCT/US2013/027606

    申请日：2013-02-25

    Applicant: HONEYWELL INTERNATIONAL INC.

    Inventor： WANG, Haiyou ,  BEKTESEVIC, Selma ,  TUNG, Hsueh S. ,  KOPKALLI, Haluk ,  CHIU, Yuon

    IPC: C07C17/20 ,  C07C21/18

    CPC classification number: C07C17/35 ,  C07C17/206 ,  C07C17/38 ,  Y02P20/582 ,  C07C21/18

    Abstract: The present invention relates, in part, an improved process for the production of certain hydrofluoroolefins, particularly 2,3,3,3-tetrafluoropropene (1234yf). In certain non-limiting embodiments, the invention relates to methods for improving process efficiency during the fluorination of 1,1,2,3-tetrachloropropene, 2,3,3,3-tetrachloropropene, and/or 1,1,1,2,3-pentachloropropane to 2-chloro-3,3,3-trifluoropropene by separating and recycling unreacted HF, unreacted starting materials, and/or certain process intermediates from the 2-chloro-3,3,3-trifluoropropene product stream.

    Abstract translation: 本发明部分地涉及用于生产某些氢氟烯烃，特别是2,3,3,3-四氟丙烯（1234yf）的改进方法。 在某些非限制性实施方案中，本发明涉及在1,1,2,3-四氯丙烯，2,3,3,3-四氯丙烯和/或1,1,1,2,3-四氯丙烯的氟化期间提高工艺效率的方法 通过从2-氯-3,3,3-三氟丙烯产物流中分离和循环未反应的HF，未反应的起始物质和/或某些过程中间体，将3-五氯丙烷加入到2-氯-3,3,3-三氟丙烯中。

    INTEGRATED PROCESS FOR THE MANUFACTURE OF FLUORINATED OLEFINS
    6.
    发明申请
    INTEGRATED PROCESS FOR THE MANUFACTURE OF FLUORINATED OLEFINS 审中-公开
    氟化油制造的综合工艺

    公开(公告)号：WO2012051057A2

    公开(公告)日：2012-04-19

    申请号：PCT/US2011/055198

    申请日：2011-10-07

    Applicant: HONEYWELL INTERNATIONAL INC. ,  BEKTESEVIC, Selma ,  TUNG, Hsueh Sung ,  KOPKALLI, Haluk

    Inventor： BEKTESEVIC, Selma ,  TUNG, Hsueh Sung ,  KOPKALLI, Haluk

    IPC: C07C17/23 ,  C07C21/18 ,  C07C19/08 ,  C07C17/38

    CPC classification number: C07C17/25 ,  C07C17/354 ,  C07C17/38 ,  Y02P20/125 ,  Y02P20/582 ,  C07C21/18 ,  C07C19/08

    Abstract: The instant invention relates, at least in part, to a method increasing the cost efficiency for dehydrohalogenation production of a fluorinated olefin by recovering and recycling spent dehydrohalogenation agent. In one aspect, the present invention relates to dehydrohalogenating a fluorinated alkane (e.g. pentafluoropropane and/or hexafluoropropane) in the presence of a dehydrohalogenating agent to produce a fluorinated olefin (e.g. tetrafluoropropenes and/or pentafluoropropenes). Removal of spent dehydrohalogenating agent from the reactor allows for facile separation of organic and dehydrohalogenating agent, the latter of which is recycled.

    Abstract translation: 本发明至少部分地涉及通过回收和循环使用的脱卤化氢剂来提高氟化烯烃脱卤化氢生产的成本效率的方法。 一方面，本发明涉及在脱卤化氢剂的存在下氟化烷烃（例如五氟丙烷和/或六氟丙烷）脱卤化氢以制备氟化烯烃（例如四氟丙烯和/或五氟丙烯）。 从反应器中除去用过的脱卤化氢剂允许容易地分离有机和脱卤化氢剂，其中后者被再循环。

    A METHOD FOR MITIGATING HCL GENERATION DURING 1,1,2,3-TETRACHLOROPROPENE PURIFICATION
    9.
    发明申请
    A METHOD FOR MITIGATING HCL GENERATION DURING 1,1,2,3-TETRACHLOROPROPENE PURIFICATION 审中-公开
    在1,1,2,3-四氯丙烯纯化过程中缓解HCL生成的方法

    公开(公告)号：WO2014149816A1

    公开(公告)日：2014-09-25

    申请号：PCT/US2014/021023

    申请日：2014-03-06

    Applicant: HONEYWELL INTERNATIONAL INC.

    Inventor： WANG, Haiyou ,  TUNG, Hsueh Sung ,  BEKTESEVIC, Selma

    IPC: C09K5/04 ,  C07C21/04

    CPC classification number: C07C17/42 ,  C07C17/25 ,  C07C17/278 ,  C07C17/38 ,  C07C17/386 ,  C07C21/04

    Abstract: This invention is directed to a method for mitigating HCl generation during 1230xa purification, which comprises the steps of; (a) adding a chelating agent into 1230xa crude, and (b) conducting the 1230xa purification in the presence of said chelating agent at a quantity sufficient to reduce or prevent 1230xa decomposition. Examples of chelating agent include tributyl phosphate (TBP), tripropyl phosphate (TPP), and triethyl phosphate (TEP). The concentration of chelating agent in 1230xa crude can range from 0.001 to 20 wt%, preferably from 0.01 to 10 wt%, and more preferably from 0.1 to 5 wt%.

    Abstract translation: 本发明涉及一种减轻1230xa纯化期间HCl产生的方法，其包括以下步骤： （a）向1230xa粗制品中加入螯合剂，和（b）在所述螯合剂存在下，以足以减少或防止1230×分解的量进行1230xa纯化。 螯合剂的实例包括磷酸三丁酯（TBP），磷酸三丙基酯（TPP）和磷酸三乙酯（TEP）。 1230xa原料中螯合剂的浓度可以为0.001〜20重量％，优选为0.01〜10重量％，更优选为0.1〜5重量％。

    PROCESS FOR PRODUCING 2,3,3,3-TETRAFLUOROPROPENE
    10.
    发明申请
    PROCESS FOR PRODUCING 2,3,3,3-TETRAFLUOROPROPENE 审中-公开
    生产2,3,3,3-四氟丙烯的方法

    公开(公告)号：WO2013049744A2

    公开(公告)日：2013-04-04

    申请号：PCT/US2012/058152

    申请日：2012-09-29

    Applicant: HONEYWELL INTERNATIONAL INC. ,  WANG, Haiyou ,  BEKTESEVIC, Selma ,  TUNG, Hsueh Sung

    Inventor： WANG, Haiyou ,  BEKTESEVIC, Selma ,  TUNG, Hsueh Sung

    CPC classification number: C07C17/20 ,  C07C17/206 ,  C07C17/389 ,  C07C21/04 ,  C07C21/18

    Abstract: The present invention relates, in part, to the discovery that the presence of moisture in 1,1,2,3-tetrachloropropene (HCO-1230xa) results in catalyst deactivation and accelerated corrosion in the reactor during the fluorination of HCO-1230xa to 2-chloro-3,3,3-trifluoropropene. By substantially removing the moisture, it is shown that the catalyst life is extended and results in improved operation efficiency of the fluorination reaction. Such steps similarly result in an overall improvement in the production of certain hydrofluoroolefins, particularly 2,3,3,3-tetrafluoropropene (HFO-1234yf).

    Abstract translation: 本发明部分涉及这样的发现，即1,1,2,3-四氯丙烯（HCO-1230xa）中的水分的存在导致催化剂失活并在反应器中加速腐蚀 将HCO-1230xa氟化为2-氯-3,3,3-三氟丙烯。 通过基本上除去水分，显示出催化剂寿命延长并导致氟化反应的操作效率提高。 这些步骤类似地导致某些氢氟烯烃，特别是2,3,3,3-四氟丙烯（HFO-1234yf）的生产的整体改进。

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