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    GALLIUM-68 PURIFICATION
    3.
    发明申请
    GALLIUM-68 PURIFICATION 审中-公开
    GALLIUM-68净化

    公开(公告)号：WO2011106846A1

    公开(公告)日：2011-09-09

    申请号：PCT/AU2011/000244

    申请日：2011-03-03

    Applicant: AUSTRALIAN NUCLEAR SCIENCE AND TECHNOLOGY ORGANISATION ,  LE, Van So

    Inventor： LE, Van So

    IPC: C01G15/00 ,  B01D15/10 ,  B01J20/06 ,  B01D15/04 ,  B01D15/26 ,  B01J39/00 ,  B01D15/08 ,  B01D15/38 ,  C22B58/00

    CPC classification number: C22B58/00 ,  B01D15/362 ,  B01J20/06 ,  B01J20/3433 ,  B01J20/3475 ,  B01J39/05 ,  B01J39/18 ,  B01J49/06 ,  B01J49/53 ,  C01G15/003 ,  C22B3/42 ,  Y02P10/234

    Abstract: A method is described for obtaining purified 68 Ga. The method comprises eluting 68 Ga from a sorbent in and/or on which are sorbed 68 Ga and 68 Ge, so as to generate a crude 68 Ga solution. The sorbent should have a higher affinity for 68 Ge than for 68 Ga. The crude 68 Ga solution is then applied to a medium cation exchange resin, and the resin is eluted with an aqueous alcohol so as to retain the 68 Ga on the resin and remove unwanted species from the resin. The resin is then eluted with an eluent, which may be an acidic solution, an alkaline solution or a solution of a species capable of complexing 68 Ga ions, so as to obtain an eluate comprising purified 68 Ga ions.

    Abstract translation: 描述了用于获得纯化的68Ga的方法。 该方法包括从吸附剂和/或其上吸附68Ga和68Ge的吸附剂洗脱68Ga，以产生粗制68Ga溶液。 对于68Ge，吸附剂应该具有比68Ga更高的亲和力。 然后将粗制的68Ga溶液施加到介质阳离子交换树脂上，并用含水醇洗脱树脂，以将68Ga保留在树脂上，并从树脂中除去不需要的物质。 然后用洗脱剂洗脱树脂，洗脱液可以是能够络合68Ga离子的物质的酸性溶液，碱性溶液或溶液，以获得包含纯化的68Ga离子的洗脱液。

    PROCESS FOR SEPARATING AND CONCENTRATING GALLIUM FROM AN AQUEOUS SOLUTION CONTAINING GALLIUM, TOGETHER WITH ALUMINIUM, ZINC AND/OR COPPER
    4.
    发明申请
    PROCESS FOR SEPARATING AND CONCENTRATING GALLIUM FROM AN AQUEOUS SOLUTION CONTAINING GALLIUM, TOGETHER WITH ALUMINIUM, ZINC AND/OR COPPER 审中-公开
    从含有玻璃酸的水溶液中分离和浓缩釉料的方法，与铝，锌和/或铜

    公开(公告)号：WO1991010621A1

    公开(公告)日：1991-07-25

    申请号：PCT/EP1990002321

    申请日：1990-12-27

    Applicant: EUROPÄISCHE WIRTSCHAFTSGEMEINSCHAFT (E.W.G) ,  KIRGIOS, Ioannis ,  SCHÜGERL, Karl ,  DEGENER, Wolfgang

    Inventor： EUROPÄISCHE WIRTSCHAFTSGEMEINSCHAFT (E.W.G)

    IPC: C01G15/00

    CPC classification number: C01G15/003

    Abstract: Process for separating and concentrating gallium from an aqueous solution containing gallium, together with aluminium, zinc and/or copper, characterized by the following combination of features: (a) preparation of a water-in-oil emulsion consisting of a neutral or alkaline aqueous phase and an organic phase containing an oil-soluble reactant in a homogenizer in a volume ratio of aqueous phase to organic phase of 2:2 to 3:2; (b) dispersion of the water-in-oil emulsion in the aqueous solution containing gallium, which is adjusted to at least 4 mol/l of HCl, in an extractor in a volume ratio of aqueous phase to water-in-oil emulsion of 30:1 to 10:1 until droplets of the water-in-oil emulsion with a diameter less than or equal to 1 mm are obtained; (c) separation of the water-in-oil emulsion from the aqueous continuum and splitting of the emulsion in a reactor with coaxial, double-insulated electrodes in a high-voltage kV/cm and a frequency greater than 50 Hz, the unsplit portion of the water-in-oil emulsion being recycled into step (b); (d) separation of the electrocoalesced organic phase of the water-in-oil emulsion in a gravity separator and recycling of the same into step (a).

    PURIFICATION OF 68GE/68GA GENERATOR ELUATE FROM FE(III) INTENDED TO IMPROVE SPECIFIC RADIOACTIVITY OF 68GA-BASED RADIOPHARMACEUTICALS
    6.
    发明申请
    PURIFICATION OF 68GE/68GA GENERATOR ELUATE FROM FE(III) INTENDED TO IMPROVE SPECIFIC RADIOACTIVITY OF 68GA-BASED RADIOPHARMACEUTICALS 审中-公开
    从FE（III）中提取68GE / 68GA发生器配比的改进旨在提高基于68GA的放射性物质的特定放射性

    公开(公告)号：WO2009102378A2

    公开(公告)日：2009-08-20

    申请号：PCT/US2008085095

    申请日：2008-12-01

    Applicant: GE HEALTHCARE LTD ,  MEDI PHYSICS INC ,  LANGSTROM BENGT ,  VELIKYAN IRINA

    Inventor： LANGSTROM BENGT ,  VELIKYAN IRINA

    IPC: A61K51/00

    CPC classification number: C01G15/003 ,  A61K51/02 ,  B01J41/04 ,  C01P2006/80 ,  C01P2006/88

    Abstract: The present invention provides a method of purifying 68Ge/68Ga generator produced 68Ga from Fe (III). The invention further relates to an automated system within an existing Gallea Synthia prototype that provides purification 68Ga from various cations and preconcentrations of 68Ga. In general, the present invention further depicts the use of an automated system for the production of 68Ga-radiolabelled PET tracers with high specific radioactivity and a kit for purifying 68Ge/68Ga generator produced 68Ga from Fe (III).

    Abstract translation: 本发明提供了一种从Fe（III）中纯化68Ge / 68Ga发生器68Ga的纯化方法。 本发明还涉及现有的Gallea Synthia原型中的自动化系统，其提供来自各种阳离子的纯度68Ga和68Ga的预浓缩。 通常，本发明还描述了使用自动化系统来生产具有高比放射性的68Ga放射性标记的PET示踪剂和用于纯化从Fe（III）制备的68Ga的68Ge / 68Ga发生器的试剂盒。

    PROCESS FOR HYDROMETALLURGICAL TREATMENT OF A SOLUTION OF GALLIFEROUS SUBSTANCES
    7.
    发明申请
    PROCESS FOR HYDROMETALLURGICAL TREATMENT OF A SOLUTION OF GALLIFEROUS SUBSTANCES 审中-公开
    高效液相色谱法解决方案

    公开(公告)号：WO1989004878A1

    公开(公告)日：1989-06-01

    申请号：PCT/FR1988000574

    申请日：1988-11-24

    Applicant: METALEUROP S.A. ,  LE QUESNE, Yves

    Inventor： METALEUROP S.A.

    IPC: C22B58/00

    CPC classification number: C22B3/0068 ,  C01G15/003 ,  C22B58/00 ,  Y02P10/234 ,  Y10S423/14

    Abstract: A process for the hydrometallurgical treatment of a solution of galliferous substances containing in addition at least one metalloid from column V of the period classification of the elements comprises the following steps: b) adjustment of the concentration of chloride ions and of the acidity of said solution by addition of hydrochloric acid and alkaline or arkaline earth chloride; c) placing said solution in contact with an organic phase containing at least one neutral pentavalent phosphorous compound containing a phosphorous-oxygen double bond. Application to extractive metallurgy of gallium and accompanying elements.

    Abstract translation: 包含含有元素周期分类的第V列至少一种准金属的含镓物质的溶液的湿法冶金处理方法包括以下步骤：b）调节氯离子的浓度和所述溶液的酸度 通过加入盐酸和碱性碱土金属氯化物; c）将所述溶液与含有至少一种含有磷 - 氧双键的中性五价磷化合物的有机相接触。 应用于镓和伴生元素的萃取冶金。

    PROCESS FOR LIQUID-LIQUID EXTRACTION OF GALLIUM FROM BASIC AQUEOUS SOLUTIONS BY MEANS OF AN ORGANIC EXTRACTION AGENT
    8.
    发明申请
    PROCESS FOR LIQUID-LIQUID EXTRACTION OF GALLIUM FROM BASIC AQUEOUS SOLUTIONS BY MEANS OF AN ORGANIC EXTRACTION AGENT 审中-公开
    通过有机萃取剂从基础水溶液中提取液体液体提取方法

    公开(公告)号：WO1985002171A1

    公开(公告)日：1985-05-23

    申请号：PCT/CH1984000183

    申请日：1984-11-19

    Applicant: GEBRÜDER SULZER AKTIENGESELLSCHAFT

    Inventor： GEBRÜDER SULZER AKTIENGESELLSCHAFT ,  WYNN, Nicholas, Patrick

    IPC: C01G15/00

    CPC classification number: C01G15/003 ,  C22B3/0037 ,  C22B3/0039 ,  Y02P10/234

    Abstract: Process for the liquid-liquid extraction of gallium from basic aqueous solutions, particularly sodium aluminate lye from alumina production according to the Bayer process, by means of an organic extraction agent comprised of a solvent and of substituted hydroxyquinoline, aluminium in addition to gallium being in the organic extraction agent solution. In five successive steps, the organic extraction agent solution containing gallium and aluminium is brought in substance exchange relationship with an aqueous mineral acid solution; the latter lades itself with gallium and aluminium and separates from the organic extraction agent solution. Chloride salt or hydrochloric acid is then dissolved into the solution laden with gallium and aluminium and is placed in substance exchange relationship with an organic solvent, for example an n-butyl acetate solution. The aluminium then remains in the aqueous acid solution while the organic solvent lades itself with gallium. After separation of the aqueous acid solution, the organic solvent is separated from the gallium chloride which is the starting product for the production of pure gallium. A main advantage of the present process is that, in the third step, the aqueous concentrated mineral acid laden with gallium and aluminium may be placed in substance exchange relationship with an organic solvent which, besides the fact that it is less costly, may be more gallium laden than substituted hydroxyquinoline.

    Abstract translation: 根据拜耳法由碱性水溶液，特别是来自氧化铝生产的铝酸钠碱液液提取镓的方法，通过由溶剂和取代的羟基喹啉组成的有机萃取剂，除了镓之外的铝 有机萃取剂溶液。 在连续五个步骤中，含有镓和铝的有机萃取剂溶液与无机酸水溶液形成物质交换关系; 后者用镓和铝自身沉淀，并与有机萃取剂溶液分离。 然后将氯化物盐或盐酸溶解到载有镓和铝的溶液中，并与有机溶剂（例如乙酸正丁酯溶液）物质交换。 然后将铝保留在酸性水溶液中，同时有机溶剂用镓自身沉淀。 在分离酸性水溶液后，将有机溶剂与作为纯镓生产的起始产物的氯化镓分离。 本方法的主要优点是，在第三步中，含有镓和铝的含水浓缩无机酸可以与有机溶剂物质交换关系，除了其成本较低的事实之外，可以更多 富含镓的取代羟基喹啉。

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