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    PROCESS FOR PREPARING FLUOROCARBOXYLIC ACID
    1.
    发明申请
    PROCESS FOR PREPARING FLUOROCARBOXYLIC ACID 审中-公开
    制备氟代羧酸的方法

    公开(公告)号：WO2010027103A1

    公开(公告)日：2010-03-11

    申请号：PCT/JP2009/065879

    申请日：2009-09-04

    Applicant: DAIKIN INDUSTRIES, LTD. ,  ITATANI, Shuji ,  ICHIDA, Takuya ,  SHIBATA, Noriaki ,  OHNO, Kaori

    Inventor： ITATANI, Shuji ,  ICHIDA, Takuya ,  SHIBATA, Noriaki ,  OHNO, Kaori

    IPC: C07C51/48 ,  C07C53/21 ,  C07C59/135

    CPC classification number: C07C51/48 ,  C07C59/135 ,  C07C53/21

    Abstract: The object of the present invention is to provide a process for industrially preparing a fluorocarboxylic acid in high purity and in high yield. The present invention is a process for preparing a fluorocarboxylic acid, which comprises: a dehydration step of removing from a mixture containing a fluorocarboxylic acid and water at least a part of said water to obtain a dehydrated fluorocarboxylic acid solution; and a purification step of purifying said dehydrated fluorocarboxylic acid solution.

    Abstract translation: 本发明的目的是提供一种以高纯度和高产率工业制备氟代羧酸的方法。 本发明是一种制备氟代羧酸的方法，其包括：脱水步骤，从含有氟代羧酸和水的混合物中除去至少一部分所述水以获得脱水的氟代羧酸溶液; 和纯化所述脱水氟代羧酸溶液的纯化步骤。

    SYNTHESIS OF CARBON-LABELED PERFLUOROALKYL COMPOUNDS
    2.
    发明申请
    SYNTHESIS OF CARBON-LABELED PERFLUOROALKYL COMPOUNDS 审中-公开
    碳标记的全氟烷基化合物的合成

    公开(公告)号：WO2005092820A3

    公开(公告)日：2005-12-15

    申请号：PCT/US2005006652

    申请日：2005-03-02

    Applicant: DU PONT ,  SHTAROV ALEXANDER BORISOVICH ,  HOWELL JON L

    Inventor： SHTAROV ALEXANDER BORISOVICH ,  HOWELL JON L

    IPC: C07B59/00 ,  C07C19/14 ,  C07C19/16 ,  C07C21/18 ,  C07C41/18 ,  C07C43/12 ,  C07C51/15 ,  C07C51/60 ,  C07C51/62 ,  C07C309/06

    CPC classification number: C07B59/001 ,  C07B2200/05 ,  C07C19/16 ,  C07C21/18 ,  C07C41/18 ,  C07C43/123 ,  C07C51/15 ,  C07C51/60 ,  C07C51/62 ,  C07C309/06 ,  C07C53/21 ,  C07C53/50 ,  C07C59/135

    Abstract: Various C and C carbon labeled compounds Rf- CF(U)y(T)z Formula 1A or Rf- CF2 CF(U)y(T)z Formula 1B wherein Rf is a linear or branched perfluoroalkyl radical Z(CmF2m)-, m is 1, 3 to 20, or a mixture thereof; Z is F when m is 1, and Z is F, Cl, or H when m is 3 to 20 or a mixture thereof; b is 13 or 14; y is 1, and z is 0 or 1; and when y and z are each 1, U is F, and T is selected from the group consisting of monovalent radicals -X wherein X is I or Br, -CH2-CH2-X, -CH=CH2, -CH2-CH2-OH, -CH2-COOH, -CH2OH, - CH2OH, -COOH, - COOH, -O-CF(CF3)-C(O)F, -O-CF(CF3)-X, -SO2Y wherein Y is H, F or Cl, and -SO3H; and when y is 1, and z is 0, U is selected from the group consisting of divalent radicals =CH-COOH, =CH-CH2-OH, and =O, are disclosed, and a process for their preparation which selectively introduces C and C carbon labels into a fluoroalkyl chain.

    Abstract translation: 各种13 C和14 C碳标记的化合物Rf-CF（U）y（T）z式1A或Rf-CF 2 CF（U）y（T）z式1B 其中R f为直链或支链全氟烷基Z（C m F 2m） - ，m为1,3-20或其混合物; 当m为1时Z为F，当m为3至20时Z为F，Cl或H或其混合物; b是13或14; y是1，并且z是0或1; 当y和z各自为1时，U为F，且T选自一价基团-X，其中X为I或Br，-CH 2 -CH 2 -X，-CH = CH 2，-CH 2 -CH 2 - OH，-CH 2 -COOH，-CH 2 OH，-CH 2 OH，-COOH，-COOH，-O-CF（CF 3）-C（O）F，-O-CF（CF 3） SO2Y，其中Y是H，F或Cl，和-SO3H; 当y为1且z为0时，U选自二价基团= CH-COOH，= CH-CH 2 -OH和= O，并且公开了它们的制备方法， 13 C和14 C碳标记成氟烷基链。

    METHOD OF TREATING FLUORINE COMPOUND
    4.
    发明申请
    METHOD OF TREATING FLUORINE COMPOUND 审中-公开
    处理氟化合物的方法

    公开(公告)号：WO02010104A1

    公开(公告)日：2002-02-07

    申请号：PCT/JP2001/006451

    申请日：2001-07-26

    IPC: C02F1/52 ,  C02F1/58 ,  C02F1/66 ,  C07C17/38 ,  C07C51/47 ,  C07C303/44 ,  C07C53/21

    CPC classification number: C07C51/47 ,  C02F1/5236 ,  C02F1/5245 ,  C02F1/5254 ,  C02F1/583 ,  C02F1/66 ,  C02F2101/14 ,  C07C53/21

    Abstract: A salt of a divalent metal and a salt of a trivalent metal are added to a solution containing a fluorine compound and a fluoropolymer to precipitate a lamellar composite hydroxide containing the fluorine compound between lamellae and to simultaneously coagulate and precipitate the fluoropolymer suspended in the solution. Thus, a large proportion of the fluorine compound is fixed and separated from the solution together with the fluoropolymer. They are recovered according to need. By this treatment method, a fluorine compound and a fluoropolymer contained in wastewater or the like can be easily separated therefrom and the burden to be imposed on the environment or an ecological system can be lessened.

    Abstract translation: 将二价金属盐和三价金属盐加入到含有氟化合物和含氟聚合物的溶液中，使含有氟化合物的层状复合氢氧化物沉淀在薄片之间，同时使悬浮在溶液中的含氟聚合物凝结并沉淀。 因此，大部分氟化合物与氟聚合物一起固定并与溶液分离。 他们根据需要恢复。 通过该处理方法，可以容易地将废水等中含有的氟化合物和含氟聚合物分离，能够减轻施加在环境或生态系统上的负担。

    PROCESS FOR PREPARING FLUORINATED CARBOXYLIC ACIDS
    8.
    发明申请
    PROCESS FOR PREPARING FLUORINATED CARBOXYLIC ACIDS 审中-公开
    制备氟化羧酸的方法

    公开(公告)号：WO2008033335A3

    公开(公告)日：2008-05-08

    申请号：PCT/US2007019721

    申请日：2007-09-11

    Applicant: HONEYWELL INT INC ,  NAIR HARIDASSAN K ,  BELL SANDRA L

    Inventor： NAIR HARIDASSAN K ,  BELL SANDRA L

    IPC: C07C51/29 ,  C07C53/21

    CPC classification number: C07C51/29 ,  C07C53/21

    Abstract: A process for the preparation of a fluorinated acid of the formula R f COOH, wherein the process includes the step of contacting: (i) a fluorinated alcohol of the formula R f CH 2 OH; and (ii) periodic acid; wherein each R f is independently selected from linear, branched or cyclic hydrocarbyl of 1-12 carbon atoms having 1-25 fluorine atoms and any range there between; and wherein the contacting step is carried out in the presence of a catalyst and optionally in a reaction medium, at a temperature and length of time sufficient to produce the fluorinated acid.

    Abstract translation: 一种制备式R f COOH的氟化酸的方法，其中所述方法包括使以下步骤：（i）式R f F f的氟化醇， CH 2 OH; 和（ii）高碘酸; 其中每个R f独立地选自具有1-25个氟原子的1-12个碳原子的直链，支链或环状烃基，其间的任何范围; 并且其中所述接触步骤在催化剂存在下，任选地在反应介质中，在足以产生氟化酸的温度和时间长度下进行。

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