摘要:
A method for preparing uniquely sized nanoparticles of CaF 2 by simultaneously spray drying a first NH 4 F and a biocompatible salt solution and a second Ca(OH) 2 and biocompatible salt solution to form CaF 2 solid particles in a soluble salt matrix wherein the salt is more soluble than CaF 2 . The salt matrix may then be dissolved and the separate CaF 2 nanosized particles collected for use as a dental therapeutic material. The technique is useful in the preparation of other discrete, nanoparticle sized compounds and combinations by carefully choosing the solvents and solutes of the two spray dried solutions.
摘要:
The present invention provides an immunogen composition and methods for using the same for the development of immunity, and particularly at mucosal sites in a mammal, thereby providing immunity at the site of entry for many major pathogenic organisms and also systemic immunity. The immunogen composition includes an antigen, a biocompatible polymer, and a liquid vehicle, with the biocompatible polymer and liquid vehicle being present in such proportions and interacting in such a way that the immunogen composition exhibits reverse-thermal viscosity behaviour. A delivery vehicle composition including a drug other than an antigen is also provided. Methods are provided for delivering the compositions of the invention to a host.
摘要:
Highly spherical sorbents of porous hydroxyapatite materials and methods of producing these sorbents are disclosed. The sorbents of the present invention have good mechanical stability and are useful as chromatography media for the separation of biomolecules, such as proteins and nucleic acids.
摘要:
The present invention relates to a method for preparing an electroactive metal polyanion or a mixed metal polyanion comprising forming a slurry comprising a polymeric material, a solvent, a polyanion source or alkali metal polyanion source and at least one metal ion source; heating said slurry at a temperature and for a time sufficient to remove the solvent and form an essentially dried mixture; and heating said mixture at a temperature and for a time sufficient to produce an electroactive metal polyanion or electroactive mixed metal polyanion. In an alternative embodiment the present invention relates to a method for preparing a metal polyanion or a mixed metal polyanion which comprises mixing a polymeric material with a polyanion source or alternatively an alkali metal polyanion source and a source of at least one metal ion to produce a fine mixture and heating the mixture to a temperature higher than the melting point of the polymeric material, milling the resulting material and then heating the milled material. It is another object of the invention to provide electrochemically active materials produced by said methods. The electrochemically active materials so produced are useful in making electrodes and batteries.
摘要:
Disclosed is a method for preparing crystalline small pore molecular sieves, said method comprising (a) preparing a reaction mixture comprising (1) at least one active source of an oxide of a tetravalent element or mixture of tetravalent elements, (2) optionally at least on active source of an oxide of a trivalent element or mixture of trivalent elements, (3) at least one active source of an alkali metal, (4) seed crystals capable of forming the small pore molecular sieve, (5) a structure directing agent capable of forming the small pore molecular sieve, and (6) an amount of water that is not substantially in excess of the amount required to cause and maintain crystallization of the small pore molecular sieve; and (b) heating said reaction mixture at crystallization conditions for sufficient time to form crystallized material containing crystals of the small pore molecular sieve.
摘要:
Disclosed is a process to produce a hypophosphite salt defined as [C + hypophosphite - ] by reacting P4 with a hydroxide salt defined as |[C + OH - ], or a hydroxide salt precursor and a catalyst, wherein C + is the cationic moiety of [C + hypophosphite - ] salt.
摘要翻译:公开了通过使P4与定义为| [C + OH-]的氢氧化物盐或氢氧化物盐前体和催化剂反应生成定义为[C +次磷酸盐 - ]的次磷酸盐的方法,其中C +是[ C +次磷酸盐]盐。
摘要:
The present invention is related to methods for preparing composite materials, which include nanoscale hydroxyapatite, and the composite materials and articles prepared therewith.
摘要:
The present invention is directed to a method for making electrode active materials represented by the general formula: A a (VO) b XO 4l wherein: (a) A is an alkali metal or mixture of alkali metals, and 0
摘要:
The energy density of the entire cell may be improved while retaining high power density by use of an alkali metal transition metal polyanion compound as the cathode (14) and a thin film metal or metalloid anode (16). The thin film anode (16) may be initially unalloyed or partially unalloyed. During use, the thin film anode (16) may be only partially unalloyed relative to the theoretical maximum. The high volumetric capacity of the metal anode (16) makes it possible to use a dense or porous thin film anode (16) in conjunction with a relatively thin particle-based cathode (14) to thereby improve the energy density of the cell.
摘要:
Stable, novel and highly effective peroxyhydrates of condensed phosphates, in particular tetrasodium pyrophosphate tris peroxyhydrates are provided. Said peroxyhydrates may be further stabilised by treatment thereof with an acidic gas or vapour and/or by encapsulation of granules containing the peroxyhydrate with suitable encapsulants including film forming polymers and oils. Additionally, a pH modifier, such as an acid buffer or acid releasing agent may be added to said granules to protect them from excessively alkaline environments as found in most washing powders. The peroxyhydrates provided, are effective oxidising bleaches finding particular application in detergent formulations. Detergent compositions, especially laundry detergent and dishwashing powder compositions containing the peroxyhydrate, are also provided.